IP Library Granted Patent US 7,473,372
Granted Patent B2
US 7,473,372 · App. 10/518,248 · Granted Jan 6, 2009

Oxidation of organic compounds

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Quick Facts
Patent No.
US 7,473,372
App. No.
10/518,248
Granted
Jan 6, 2009
Kind
B2
Abstract

An improved method for treating organic compounds present in soil, groundwater and other environments is disclosed. The method involves the use of a peroxygen compound and a chelated transition metal.

Claims (16)

1. A method of oxidizing an organic compound present in soil, groundwater, process water or wastewater said method comprising contacting the organic compound with a composition comprising a persulfate, and a chelated metal catalyst composed of divalent or trivalent cationic species of iron.

2. A method as in claim 1 , wherein the organic compound is present in soil, groundwater, or wastewater.

3. A method as in claim 1 , wherein the organic compound is selected from the group consisting of volatile organic compounds, semi-volatile organic compounds, polyaromatic hydrocarbons, polychlorobiphenyls, pesticides and herbicides.

4. The method as in claim 1 , wherein the persulfate is a dipersulfate.

5. The method as in claim 4 , wherein the dipersulfate is selected from sodium, potassium or ammonium persulfate or a combination thereof.

6. The method as in claim 1 , wherein the persulfate is a monopersulfate.

7. The method as in claim 6 , wherein the monopersulfate is selected from sodium and potassium monopersulfate.

8. The method as in claim 1 , wherein the persulfate is a combination of a dipersulfate and monopersulfate.

9. The method as in claim 1 , wherein the iron is divalent.

10. The method as in claim 1 , wherein the iron is trivalent.

11. The method as in claim 1 , wherein the metal catalyst is chelated with ethylenediaminetetraacetic acid.

12. The method as in claim 1 , wherein the amount of chelated metal catalyst is sufficient to deliver an equivalent amount of transition metal in the range of 1-1000 ppm.

13. The method as in claim 1 , wherein the amount of persulfate is sufficient to satisfy the soil oxidant and to oxidize substantially all of the organic compound.

14. The method as in claim 1 , wherein the chelated metal catalyst and the persulfate are added in combination.

15. The method as in claim 1 , wherein the chelated metal catalyst and the persulfate are added sequentially.

16. The method as in claim 1 , wherein the metal catalyst is chelated with citrate.

Assignments (11)
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE'S ADDRESS PREVIOUSLY RECORDED AT REEL: 061398 FRAME: 0889. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded May 11, 2023
From: PEROXYCHEM LLC
To: EVONIK ACTIVE OXYGENS, LLC
Reel/Frame 063628/0835 →
CHANGE OF ADDRESS Recorded May 10, 2023
From: EVONIK ACTIVE OXYGENS, LLC
To: EVONIK ACTIVE OXYGENS, LLC
Reel/Frame 063602/0685 →
CHANGE OF NAME Recorded Sep 8, 2022
From: PEROXYCHEM LLC
To: EVONIK ACTIVE OXYGENS, LLC
Reel/Frame 061398/0889 →
RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT R/F 050605/0305 Recorded Feb 3, 2020
From: BARCLAYS BANK PLC, AS ADMINISTRATIVE AGENT
To: PEROXYCHEM LLC
Reel/Frame 051777/0957 →
RELEASE OF SECURITY INTEREST Recorded Oct 2, 2019
From: BANK OF AMERICA, N.A., AS AGENT
To: PEROXYCHEM LLC
Reel/Frame 050606/0329 →
SECURITY INTEREST Recorded Oct 2, 2019
From: PEROXYCHEM LLC
To: BARCLAYS BANK PLC, AS ADMINISTRATIVE AGENT
Reel/Frame 050605/0305 →
RELEASE OF SECURITY INTEREST Recorded Nov 4, 2015
From: MACQUARIE US TRADING LLC, AS COLLATERAL AGENT
To: PEROXYCHEM LLC
Reel/Frame 036953/0766 →
SECURITY INTEREST Recorded Oct 21, 2015
From: PEROXYCHEM LLC
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 036847/0594 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 31, 2014
From: FMC CORPORATION
To: PEROXYCHEM LLC
Reel/Frame 032558/0681 →
SHORT FORM PATENT SECURITY AGREEMENT Recorded Mar 3, 2014
From: PEROXYCHEM LLC
To: MACQUARIE US TRADING LLC
Reel/Frame 032379/0931 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 27, 2005
From: BLOCK, PHILIP A.; SETHI, DALBIR S.; BROWN, RICHARD A.; ROBINSON, DAVID S.
To: FMC CORPORATION
Reel/Frame 016314/0415 →