IP Library Granted Patent US 7,423,046
Granted Patent B2
US 7,423,046 · App. 10/524,820 · Granted Sep 9, 2008

3-hydroxy-6-phenylphenanthridines as pde-4 inhibitors

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Quick Facts
Patent No.
US 7,423,046
App. No.
10/524,820
Granted
Sep 9, 2008
Kind
B2
Abstract

Compounds of formula (I), in which R1, R2, R3, R4, R5, R6 and R7 have the meaning indicated in the description, are novel effective PDE4 inhibitors.

Claims (43)

1. A compound of the formula I

in which

R1 is methoxy or difluoromethoxy,

R2 is methoxy difluoromethoxy or ethoxy,

R3 is hydrogen,

R31 is hydrogen,

R4 is hydrogen or acetyl,

R5 hydrogen,

R6 is cyano or cyclopropylmethoxy,

R7 is hydrogen or cyclopropylmethoxy, or a salt of this compound, an N-oxide of this compound, or a salt of an N-oxide of this compound.

2. A compound of the formula I as claimed in claim 1 , in which

R1 is methoxy,

R2 is methoxy,

R3 is hydrogen,

R31 is hydrogen,

R4 is hydrogen or acetyl,

R5 is hydrogen,

R6 is cyano or cyclopropylmethoxy,

R7 is hydrogen or cyclopropylmethoxy, or a salt of this compound, an N-oxide of this compound, or a salt of an N-oxide of this compound.

3. A compound of the formula I as claimed in claim 1 , in which

R1 is methoxy,

R2 is methoxy,

R3 is hydrogen,

R31 is hydrogen,

R4 is hydrogen or acetyl,

R5 is hydrogen,

R6 is cyclopropylmethoxy,

R7 is cyclopropylmethoxy, or a salt of this compound, an N-oxide of this compound, or a salt of an N-oxide of this compound.

4. A compound as claimed in claim 1 , selected from the group consisting of

(±)-acetic acid (3RS,4aRS,10bRS)-6-(3,4-bis-cyclopropylmethoxyphenyl)-8,9-dimethoxy-(1,2,3,4,4a,10b)-hexahydrophenanthridin-3-yl ester,

(±)-acetic acid (3SR,4aRS,10bRS)-6-(3,4-bis-cyclopropylmethoxyphenyl)-8,9-dimethoxy-(1,2,3,4,4a,10b)-hexahydrophenanthridin-3-yl ester,

(±)-(3RS,4aRS,10bRS)-6-(3,4-bis-cyclopropylmethoxyphenyl)-8,9-dimethoxy-(1,2,3,4,4a,10b)-hexahydrophenanthridin-3-ol,

(±)-(3SR,4aRS,10bRS)-6-(3,4-bis-cyclopropylmethoxyphenyl)-8,9-dimethoxy-1,2,3,4,4a,10b-hexahydrophenanthridin-3-ol,

(±)-acetic acid (3SR,4aRS,10bRS)-6-(4-cyanophenyl)-8,9-dimethoxy-(1,2,3,4,4a,10b)-hexahydrophenanthridin-3-yl ester,

(±)-4-((3SR,4aRS,10bRS)-3-hydroxy-8,9-dimethoxy-(1,2,3,4,4a,10b)-hexahydrophenanthridin-6-yl)-benzonitrile, and the salts of these compounds, the N-oxides of these compounds, and the salts of the N-oxides of these compounds.

5. A compound of the formula I according to claim 1 , in which the hydrogen atoms in positions 4a and 10b are in the cis position relative to one another, or a salt of this compound, an N-oxide of this compound, or a salt of an N-oxide of this compound.

6. A compound of the formula I according to claim 1 , which has with respect to the positions 4a and 10b, the configuration shown in the formula I*:

or a salt of this compound, an N-oxide of this compound, or a salt of an N-oxide of this compound.

7. A compound of the formula I according to claim 1 , which has with respect to the positions 3, 4a and 10b, the configuration shown either in formula I**, I*** or I****:

or a salt of this compound, an N-oxide of this compound, or a salt of an N-oxide of this compound.

8. A compound of the formula I according to claim 1 , which has with respect to the positions 3, 4a and 10b, the configuration shown in formula I*****:

or a salt of this compound, an N-oxide of this compound, or a salt of an N-oxide of this compound.

9. A pharmaceutical composition comprising one or more compounds of the formula I as claimed in claim 1 , or a pharmaceutically acceptable salt of this compound, a pharmaceutically acceptable N-oxide of this compound, or a salt of said N-oxide,together with a pharmaceutical auxiliary and/or excipient.

Assignments (4)
CHANGE OF NAME Recorded Jul 29, 2015
From: NYCOMED GERMANY HOLDING GMBH
To: TAKEDA GMBH
Reel/Frame 036205/0192 →
MERGER Recorded Jul 28, 2015
From: TAKEDA GMBH
To: NYCOMED ASSET MANAGEMENT GMBH
Reel/Frame 036193/0178 →
MERGER Recorded Jul 28, 2015
From: NYCOMED ASSET MANAGEMENT GMBH
To: NYCOMED GERMANY HOLDING GMBH
Reel/Frame 036201/0261 →
CHANGE OF NAME Recorded Sep 4, 2007
From: ALTANA PHARMA AG
To: NYCOMED GMBH
Reel/Frame 019783/0625 →