IP Library Granted Patent US 7,247,725
Granted Patent B2
US 7,247,725 · App. 10/528,329 · Granted Jul 24, 2007

Gamma-aminoamide modulators of chemokine receptor activity

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Quick Facts
Patent No.
US 7,247,725
App. No.
10/528,329
Granted
Jul 24, 2007
Kind
B2
Abstract

The present invention is directed to compounds of the formula (I), wherein R 1 , R 2 , R 3 , R 4 , R 5 , R 6 , R 7 , R 8 , R 11 , R 12 , W, X, and n are defined herein, which are useful as modulators of chemokine receptor activity. In particular, these compounds are useful as modulators of the chemokine receptor CCR-2.

Claims (84)

1. A compound of the formula Ib:

wherein the dashed line represents a single or a double bond and wherein

R 1 is selected from:

and positional and stereo isomers thereof;

R 2 is selected from: (C 0-6 alkyl)-phenyl and (C 0-6 alkyl)-heterocycle, where the alkyl is unsubstituted or substituted with 1–7 substituents where the substituents are independently selected from:

(a) halo,

(b) hydroxy,

(c) —O—C 1-3 alkyl,

(d) trifluoromethyl,

(e) —C 1-3 alkyl,

(f) —CO 2 R 9 , and

(g) oxo;

and where the phenyl and the heterocycle may be unsubstituted or substituted with 1–5 substituents where the substituents are independently selected from:

(a) halo,

(b) trifluoromethyl

(c) trifluoromethoxy,

(d) hydroxy,

(e) C 1-6 alkyl,

(f) C 3-7 cycloalkyl,

(g) —O—C 1-6 alkyl,

(h) —O—C 3-7 cycloalkyl,

(i) —SCF 3 ,

(j) —S—C 1-6 alkyl,

(k) —SO 2 —C 1-6 alkyl,

(l) phenyl,

(m) hetreocycle,

(n) —CO 2 R 9 ,

(o) —CN,

(p) —NR 9 R 10 ,

(q) —NR 9 —SO 2 —R 10 ,

(r) —SO 2 —NR 9 R 10 ,

(s) —ONR 9 R 10 , and

(t) —O -phenyl;

R 5 is selected from:

(a) hydrogen,

(b) hydroxy,

(c) C 1-6 alkyl,

(d) C 1-6 alkyl-hydroxy,

(e) —O—C 1-3 alkyl,

(f) oxo, and

(g) halo,

(h) C 0-4 CO 2 R 9 , and

(i) CF 3 ,

R 15 and R 16 are independently selected from:

(a) hydrogen,

(b) halo,

(c) trifluoromethyl,

(d) hydroxy,

(e) C 1-3 alkyl,

(f) —O—C 1-3 alkyl,

(g) —CO 2 H,

(h) –CO 2 C 1-3 alkyl,

(i) —CN, and

(j) heterocycle;

and pharmaceutically acceptable salts and individual diastereomers thereof.

2. The compound of claim 1 wherein R 2 is selected from:

(1) —CH 2 -(phenyl),

(2) —CH 2 -(4-bromophenyl),

(3) —CH 2 -(3-chlorophenyl),

(4) —CH 2 -(3,5-difluorophenyl),

(5) —CH 2 -((2-trifluoromethyl)phenyl),

(6) —CH 2 -((3-trifluoromethyl)phenyl),

(7) —CH 2 -((4-trifluoromethyl)phenyl),

(8) —CH 2 -((3-trifluoromethoxy)phenyl),

(9) —CH 2 -((3-trifluoromethylthio)phenyl),

(10) —CH 2 -((3-trifluoromethoxy-5-thiomethyl)phenyl),

(11) —CH 2 -((3-trifluoromethoxy-5-methoxy)phenyl),

(12) —CH 2 -((3-trifluoromethoxy-5-methanesulfonyl)phenyl),

(13) —CH 2 -((3-trifluoromethoxy-5-amino)phenyl),

(14) —CH 2 -((3-trifluoromethoxy-5-aminomethanesulfonyl)phenyl),

(15) —CH 2 -((3-trifluoromethoxy-5-sulfonylamino)phenyl),

(16) —CH 2 -((3,5-bis-trifluoromethyl)phenyl),

(17) —CH 2 -((3-fluoro-5-trifluoromethyl)phenyl),

(18) —CH(CH 3 )-((3,5-bis-trifluoromethyl)phenyl),

(19) —C(CH 3 )2-((3,5-bis-trifluoromethyl)phenyl),

(20) —CH 2 -(4-(2-trifluoromethyl)pyridyl),

(21) —CH 2 -(5-(3-trifluoromethyl)pyridyl),

(22) —CH 2 -(5-(3-trifluoromethyl)pyridazinyl),

(23) —CH 2 -(4-(2-trifluoromethyl)pyridyl-N-oxide), and

(24) —CH 2 -(5-(3-trifluoromethyl)pyridyl-N-oxide).

3. The compound of claim 1 of the formula:

wherein the dashed line represents a single or a double bond,

R 5 is hydrogen or methyl;

and pharmaceutically acceptable salts and individual diastereomers thereof.

Assignments (2)
CHANGE OF NAME Recorded Jan 29, 2010
From: MERCK & CO., INC.
To: MERCK SHARP & DOHME CORP.
Reel/Frame 023861/0910 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 6, 2006
From: BUTORA, GABOR; PASTERNAK, ALEXANDER; YANG, LIHU; ZHOU, CHANGYOU
To: MERCK & CO., INC.
Reel/Frame 017312/0569 →