IP Library Granted Patent US 7,727,482
Granted Patent B2
US 7,727,482 · App. 10/541,432 · Granted Jun 1, 2010

Method for carrying out chemical reactions in pseudo-isothermal conditions

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 7,727,482
App. No.
10/541,432
Granted
Jun 1, 2010
Kind
B2
Abstract

Method for controlling the reaction temperature in a catalytic bed ( 24 ) of a reactor ( 1 ) in which a chemical reaction takes place in pseudo-isothermal conditions by means of at least one heat exchanger ( 12 ), crossed by a respective operating fluid, immersed in the catalytic bed ( 24 ).

Claims (13)

1. A method for controlling the reaction temperature in a catalytic bed of a reactor in which a chemical reaction takes place in pseudo-isothermal conditions by means of at least one heat exchanger, crossed by a respective operating fluid immersed in said catalytic bed, comprising the step of:

setting the velocity of said heat exchange fluid inside the respective heat exchanger within predetermined values, so that the heat transfer coefficient inside said heat exchanger is less than the heat transfer coefficient in the catalytic bed.

2. The method according to claim 1 , wherein said velocity of said heat exchange fluid inside the respective heat exchanger is regulated within values such that the heat transfer coefficient inside the heat exchangers is equal to or less than ⅔ the heat transfer coefficient inside the catalytic bed.

3. The method according to claim 1 , wherein said reactor comprises at least two heat exchangers immersed in the catalytic bed and wherein the method further comprises the steps of:

continuously detecting in said catalytic bed the temperature difference ΔT between the temperature of the catalytic bed at said heat exchangers and a limit temperature T 1 , at a middle point between said heat exchangers; and

varying the velocity of said heat exchange fluid inside said heat exchangers, according to the aforementioned temperature difference ΔT, obtaining a corresponding variation of the heat transfer coefficient inside said heat exchangers.

4. A pseudo-isothermal chemical reactor comprising:

a catalytic bed;

at least two heat exchangers immersed in said catalytic bed; and

an apparatus for adjusting the temperature inside a reaction zone of said catalytic bed defined between said heat exchangers, comprising

a probe for continuously measuring the temperature difference ΔT between the temperature in a central position of said zone and the temperature of said reaction zone at said heat exchangers,

a control unit, in data communication with said probe, and

a feeding velocity regulator for an operating fluid (F o ) in said heat exchangers, in data communication with said control unit.

Assignments (2)
MERGER Recorded Dec 4, 2014
From: AMMONIA CASALE SA; UREA CASALE SA; METHANOL CASALE SA; CASALE CHEMICALS SA
To: CASALE SA
Reel/Frame 034533/0456 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 14, 2010
From: FILIPPI, ERMANNO; RIZZI, ENRICO; TAROZZO, MIRCO
To: METHANOL CASALE S.A.
Reel/Frame 024228/0770 →