IP Library Granted Patent US 7,641,736
Granted Patent B2
US 7,641,736 · App. 10/545,306 · Granted Jan 5, 2010

Method of manufacturing SiC single crystal wafer

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Quick Facts
Patent No.
US 7,641,736
App. No.
10/545,306
Granted
Jan 5, 2010
Kind
B2
Abstract

A method of manufacturing an SiC single crystal wafer according to the present invention includes the steps of: (a) preparing an SiC single crystal wafer 10 with a mirror-polished surface; (b) oxidizing the surface of the SiC single crystal wafer 10 with plasma, thereby forming an oxide layer 12 on the surface of the SiC single crystal wafer; and (c) removing at least a portion of the oxide layer 12 by a reactive ion etching process. Preferably, the surface of the wafer is planarized by repeatedly performing the steps (b) and (c) a number of times.

Claims (20)

1. A method of manufacturing an SiC single crystal wafer, the method comprising the steps of:

(a) preparing an SiC single crystal wafer with a mirror-polished surface;

(b) after step (a), oxidizing the surface of the SiC single crystal wafer with plasma, thereby forming an oxide layer under the surface of and within the SiC single crystal wafer; and

(c) after step (b), removing at least a portion of the oxide layer by a reactive ion etching process; wherein

the step of removing at least a portion of the oxide layer by a reactive ion etching process includes removing substantially the entire oxide layer.

2. The method of claim 1 , wherein the steps (b) and (c) are repeatedly performed a number of times.

3. The method of claim 2 , wherein the oxidation in the step (b) and the etching process in the step (c) are each carried out for one to ten minutes.

4. The method of claim 2 , further comprising, after repeatedly performing the steps (b) and (c) a number of times and finishing the step (b) for the last time, the step (d) of polishing the surface of the SiC single crystal wafer by a chemical mechanical polishing process.

5. The method of claim 1 , wherein the step (b) includes using either oxygen or a mixture of oxygen and an inert gas.

6. The method of claim 1 , wherein the step (c) includes using a gas including F.

7. The method of claim 1 , wherein the step (c) includes defining conditions of the reactive ion etching process such that SiC and the oxide layer are etched at the same rate.

8. The method of claim 1 , wherein the step (a) includes preparing an SiC single crystal wafer that has an offset angle of substantially zero degrees with respect to C-axis.

9. The method of claim 1 , wherein the steps (b) and (c) are carried out in the same system with gases changed.

10. A method of manufacturing an SiC single crystal wafer, comprising the steps of:

planarizing the surface of the SiC single crystal wafer by repeatedly performing, a number of times, the step of oxidizing the surface of the SiC single crystal wafer, thereby forming an oxide layer under the surface of and within the SiC single crystal wafer; and

after the step of oxidizing, performing the step of etching away an oxide layer produced by the step of oxidizing; wherein

the step of etching away the oxide layer includes etching away substantially the entire oxide layer.

11. The method of claim 2 , wherein the number of times is at least five.

12. The method of claim 1 , wherein the step of oxidizing the surface of the SiC single crystal wafer includes forming the oxide layer over substantially the entire surface of the SiC single crystal wafer.

13. The method of claim 10 , wherein the step of oxidizing the surface of the SiC single crystal wafer includes forming the oxide layer on substantially the entire surface of the SiC single crystal wafer.

Assignments (4)
CORRECTIVE ASSIGNMENT TO CORRECT THE INCORRECT APPLICATION NO. "11545306" TO CORRECTLY READ "10545306" PREVIOUSLY RECORDED ON REEL 020960 FRAME 0162. ASSIGNOR(S) HEREBY CONFIRMS THE MERGER. Recorded Mar 6, 2017
From: NEOMAX CO., LTD.
To: HITACH METALS, LTD.
Reel/Frame 042041/0090 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 29, 2008
From: NEOMAX CO., LTD.
To: HITACHI METALS, LTD.
Reel/Frame 021015/0213 →
MERGER Recorded Apr 30, 2008
From: NEOMAX CO., LTD.
To: HITACHI METALS, LTD.
Reel/Frame 020960/0162 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 11, 2005
From: HIROOKA, TAISUKE
To: NEOMAX CO., LTD.
Reel/Frame 018089/0957 →