IP Library Granted Patent US 7,268,174
Granted Patent B2
US 7,268,174 · App. 10/618,111 · Granted Sep 11, 2007

Homogeneous alumoxane-LCT-epoxy polymers and methods for making the same

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 7,268,174
App. No.
10/618,111
Granted
Sep 11, 2007
Kind
B2
Abstract

The present invention relates to homogeneous alumoxane-LCT-epoxy polymers and methods for making the same. The homogeneous alumoxane-LCT-epoxy polymers comprise alumoxane-containing sub-structures evenly dispersed and essentially completely co-reacted with the LCT-epoxy sub-structures. The alumoxane sub-structures are organically bonded to the LCT-epoxy sub-structures. This produces homogeneous alumoxane-LCT-epoxy polymers that are substantially free of particle wetting and micro-void formation, with improved thermal conductivity properties without compromising on other desired structural integrities.

Claims (7)

1. A method of increasing the thermal conductivity of an electrically insulating epoxy material without compromising the electrical insulating properties of the material, the method comprising:

stirring an LCT-epoxy resin comprising a crystalline microstructure having a layered nature with an anhydriding agent at approximately 60° C. until a clear LCT-epoxy anhydride solution is formed;

after the solution is clear, adding a boehmite material into the clear solution and stirring at approximately 60° C., until the solution is again clear to form a uniform dissolution of the boehmite material substantially free of particle wetting and with essentially complete co-reactivity of the boehmite material with the LCT-epoxy anhydride; and

adding an accelerator and curing the solution;

the method effective to produce homogeneous alumoxane-LCT-epoxy-anhydride polymers that retain the layered nature of the LCT-epoxy resin and are substantially free of micro-void formation and that exhibit a dielectric strength of at least 1.2 kV/mil while at the same time exhibiting thermal conductivity of at least 0.50 W/mK in a transverse direction and at least 0.99 W/mK in a thickness direction in an environment of 25° C.

2. The method of claim 1 , further comprising dissolving zinc naphthenate into the solution as the accelerator.

3. A homogeneous alumoxane-LCT-epoxy anhydride polymer produced by the method of claim 1 and comprising a crystalline microstructure having a layered nature and exhibiting a dielectric strength of at least 1.2 kV/mil while at the same time exhibiting thermal conductivity of at least 0.50 W/mK in a direction transverse to layers of the microstructure and at least 0.99 W/mK in a thickness direction across the layers of the microstructure in an environment of 25° C.

Assignments (3)
CHANGE OF NAME Recorded Mar 31, 2009
From: SIEMENS POWER GENERATION, INC.
To: SIEMENS ENERGY, INC.
Reel/Frame 022482/0740 →
CHANGE OF NAME Recorded Sep 15, 2005
From: SIEMENS WESTINGHOUSE POWER CORPORATION
To: SIEMENS POWER GENERATION, INC.
Reel/Frame 017000/0120 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 11, 2003
From: SMITH, JAMES D.B.
To: SIEMENS WESTINGHOUSE POWER CORPORATION
Reel/Frame 014283/0969 →