IP Library Granted Patent US 7,163,358
Granted Patent B2
US 7,163,358 · App. 10/644,488 · Granted Jan 16, 2007

Injection grouting

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Quick Facts
Patent No.
US 7,163,358
App. No.
10/644,488
Granted
Jan 16, 2007
Kind
B2
Abstract

The invention relates to the use of a composition for injection grouting obtainable by mixing an alkali metal silicate or an organic silicate, colloidal silica particles, and at least one gelling agent, wherein the weight ratio of colloidal silica to silicate is from about 2:1 to about 100:1. The invention also relates to a method of sealing a leaking part or cavity, and method of cutting off a liquid flow in a leaking part or cavity. The invention further relates to a composition for injection grouting and a method for preparing such composition.

Claims (16)

1. A method of sealing a leaking part or cavity comprising injecting into said leaking part or cavity a grouting composition comprising an alkali metal silicate or an organic silicate, colloidal silica particles dispersed in a solvent in a concentration from about 10 to about 70 wt % counted as dry weight silica, and at least one gelling agent, wherein the composition has a weight ratio of silica to silicate from about 2:1 to about 100:1.

2. A method according to claim 1 , wherein the colloidal silica particles are present in a silica sol having an S-value from about 30 to about 90.

3. A method according to claim 1 , wherein the composition further comprises a hydraulic binder.

4. A method according to claim 1 , wherein the weight ratio of silica to silicate is from about 3:1 to about 70:1.

5. A method according to claim 1 , wherein the weight ratio of silica to silicate is from about 6:1 to about 20:1.

6. A method according to claim 1 , wherein the silica particles have a relative standard deviation of the particle size distribution lower than about 15% by numbers.

7. A method according to claim 1 , wherein the gelling agent is an alkali metal salt.

8. A method according to claim 1 , wherein the gelling agent is added resulting in an amount of from about 1 to about 30 wt % of the total dry weight of silicate and silica particles.

9. A method of sealing a leaking part or cavity comprising injecting into said leaking part or cavity a grouting composition comprising an alkali metal silicate or an organic silicate, colloidal silica particles dispersed in a solvent in a concentration from about 10 to about 70 wt % counted as dry weight silica, and at least one gelling agent in an amount effective to result in a gelling time from about 1 minute to about 24 hours, wherein the composition has a weight ratio of silica to silicate from about 2:1 to about 100:1.

10. A method according to claim 9 , wherein the colloidal silica particles are present in a silica sol having an S-value from about 30 to about 90.

11. A method according to claim 9 , wherein the composition further comprises a hydraulic binder.

12. A method according to claim 9 , wherein the weight ratio of silica to silicate is from about 3:1 to about 70:1.

13. A method according to claim 9 , wherein the weight ratio of silica to silicate is from about 6:1 to about 20:1.

14. A method according to claim 1 , wherein the silica particles have a relative standard of deviation of the particle size distribution lower than about 15% by numbers.

15. A method according to claim 9 , wherein the gelling agent is an alkali metal salt.

16. A method according to claim 9 , wherein the gelling agent is added resulting in an amount of from about 1 to about 30% of the total dry weight of the silicate and silica particles.

Assignments (3)
SECURITY INTEREST Recorded Oct 1, 2018
From: STARFRUIT US MERGER SUB 1 LLC; STARFRUIT US MERGER SUB 2 LLC; AKZO NOBEL SURFACE CHEMISTRY LLC; AKZO NOBEL CHEMICALS B.V.; AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
To: WILMINGTON TRUST (LONDON) LIMITED, AS COLLATERAL AGENT
Reel/Frame 047231/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 13, 2017
From: AKZO NOBEL N.V.
To: AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
Reel/Frame 044427/0759 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 20, 2003
From: GREENWOOD, PETER; JANSSON, INGER; SKARP, ULF
To: AKZO NOBEL N.V.
Reel/Frame 014425/0211 →