IP Library Granted Patent US 7,153,534
Granted Patent B2
US 7,153,534 · App. 10/648,660 · Granted Dec 26, 2006

Premix composition for clarifying beer

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Quick Facts
Patent No.
US 7,153,534
App. No.
10/648,660
Granted
Dec 26, 2006
Kind
B2
Abstract

A premix composition for clarifying beverages like beer includes, by weight, (a) about 40 to 90%, preferably 60–85%, of silica xerogel having less than 10% water therein, preferably 5% or less, and a particle size, as defined by its mean volume average diameter MV, in both the dry state and as a 10% aqueous slurry, of less than 50μ, preferably about 5–30μ, and (b) about 10 to 60%, preferably 15–40%, of crosslinked polyvinylpyrrolidone having a particle size as defined, in the dry state, of about 10 to 50μ, and about 30–60μ in a 10% aqueous slurry, and a process of obtaining, chill-haze stabilized beer with substantial reduction in high molecular weight proteins, as well as polyphenols, flavanoids and tannins, in an efficient and effective single-step process at a rapid filter-flow rate, with undetectable residual soluble plyvinylpyrrolidone thereafter, and no microbiological growth in the premix, effective haze stability after time, and advantageous redispersibility of the premix used in the process.

Claims (5)

1. A premix composition for clarifying beer effectively in a single-step process, without compactation, consisting essentially of, by weight,

(a) about 70% of silica xerogel having less than 5% water therein, and a particle size in the dry state as defined by its mean volume average diameter, Mv, of about 5 to about 30μ, and

(b) about 30% of crosslinked polyvinylpyrrolidone having a particle size in the dry state of about 10 to about 50μ, wherein the particle size of (a) is less than the particle size of (b) and the particle size of a water slurry of 10 wt. % of the premix composition is about 50μ.

2. A stable, flocculated aqueous slurry for homogeneously dosing and clarifying beer effectively in a single-step process, without compactation, consisting essentially of, by weight, (a) about 5% to about 20% of a premix composition of about 70% of silica xerogel having less than 5% water therein, and having a particle size in the dry state as defined by its mean volume average diameter, Mv, of 5 to 30μ, and (b) about 30% of crosslinked polyvinylpyrrolidone, having a particle size in the dry state of about 10 to about 50μ; wherein the particle size of (a) is less than the particle size of (b) and the particle size of a water slurry of 10 wt. % of the premix composition is about 50μ; and 80% to 95% water.

3. A process of stabilizing beer which comprises treating beer with the aqueous flocculated slurry of claim 2 and filtering the thus-treated beer.

Assignments (5)
RELEASE OF SECURITY INTEREST Recorded Jan 10, 2020
From: THE BANK OF NOVA SCOTIA
To: AVOCA LLC; HERCULES LLC; ISP INVESTMENTS LLC; PHARMACHEM LABORATORIES LLC
Reel/Frame 051557/0504 →
SECURITY AGREEMENT Recorded Jul 3, 2017
From: AVOCA, INC.; HERCULES LLC; ISP INVESTMENTS LLC; PHARMACHEM LABORATORIES, INC.
To: THE BANK OF NOVA SCOTIA, AS ADMINISTRATIVE AGENT
Reel/Frame 043084/0753 →
RELEASE OF PATENT SECURITY AGREEMENT Recorded Mar 18, 2013
From: THE BANK OF NOVA SCOTIA
To: ASHLAND LICENSING AND INTELLECTUAL PROPERTY LLC; AQUALON COMPANY; ISP INVESTMENTS INC.; HERCULES INCORPORATED
Reel/Frame 030025/0320 →
PATENT RELEASE Recorded Sep 19, 2011
From: JPMORGAN CHASE BANK, N.A. (F/K/A THE CHASE MANHATTAN BANK)
To: ISP CAPITAL, INC.; ISP CHEMICAL PRODUCTS, INC.; VERONA, INC.
Reel/Frame 026930/0774 →
SECURITY AGREEMENT Recorded Sep 16, 2011
From: ASHLAND LICENSING AND INTELLECTUAL PROPERTY LLC; HERCULES INCORPORATED; AQUALON COMPANY; ISP INVESTMENT INC.
To: THE BANK OF NOVA SCOTIA, AS ADMINISTRATIVE AGENT
Reel/Frame 026918/0052 →