IP Library Granted Patent US 7,186,389
Granted Patent B2
US 7,186,389 · App. 10/648,894 · Granted Mar 6, 2007

Method for carrying out chemical reactions in pseudo-isothermal conditions

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Quick Facts
Patent No.
US 7,186,389
App. No.
10/648,894
Granted
Mar 6, 2007
Kind
B2
Abstract

Method for carrying out in continuous, under so-called pseudo-isothermal conditions and in a predetermined reaction environment, such as a catalytic bed, a selected chemical reaction, comprising the steps of providing in the reaction environment at least one tubular heat exchanger fed with a first flow of a heat exchange operating fluid at a respective predetermined inlet temperature, the fluid passing through the at least one tubular heat exchanger according to a respective inlet/outlet path, which method also provides the step of feeding into the at least one tubular heat exchanger and at one or more intermediate positions of said path, a second flow of operating fluid having a respective predetermined inlet temperature.

Claims (18)

1. A method for carrying out in continuous, under pseudo-isothermal conditions and in a predetermined reaction environment, a selected chemical reaction, comprising the steps of:

feeding a first flow of a heat exchange operating fluid at a respective predetermined inlet temperature in at least one tubular heat exchanger provided in said reaction environment, said fluid passing through said at least one tubular heat exchanger according to a respective inlet/outlet path, and

feeding into said at least one tubular heat exchanger and at one or more intermediate positions of said path, a second flow of operating fluid having a respective predetermined inlet temperature.

2. A heat exchanger comprising:

a tubular element,

a chamber defined within said tubular element for being passed through by a first flow of a heat exchange operating fluid,

a fluid distributor duct, and

a fluid collector duct connected to said tubular element and in fluid communication with said chamber,

an additional distributor of a second flow of said operating fluid in fluid communication with said chamber, and

a feeding duct of said second flow of operating fluid in fluid communication with said additional distributor.

3. The heat exchanger according to claim 2 , wherein said additional distributor is supported within said tubular element and is provided with a least a hole in fluid communication with said chamber at a predetermined distance between said fluid distributor duct and said fluid collector duct.

4. The heat exchanger according to claim 3 , wherein said additional distributor is tubular shaped, closed at one end thereof and connected to said feeding duct at an opposite end thereof.

5. The heat exchanger according to claim 4 , wherein said feeding duct is supported within said fluid distributor duct or said fluid collector duct.

6. The heat exchanger according to claim 3 , wherein said additional distributor extends for substantially the entire length of said tubular exchanger.

7. The heat exchanger according to claim 3 , wherein said additional distributor is provided with a plurality of said holes arranged in rows at respective predetermined distances between said fluid distributor duct and said fluid collector duct.

8. The heat exchanger according to claim 4 , wherein the diameter of said additional distributor varies along its length.

9. The heat exchange unit for pseudo-isothermal reactors, comprising at least one tubular heat exchanger according to claim 2 .

10. A pseudo-isothermal chemical reactor comprising a catalytic bed and a heat exchange unit according to claim 9 provided therein.

Assignments (3)
MERGER Recorded Dec 4, 2014
From: AMMONIA CASALE SA; UREA CASALE SA; METHANOL CASALE SA; CASALE CHEMICALS SA
To: CASALE SA
Reel/Frame 034533/0456 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 18, 2003
From: FILIPPI, ERMANNO; RIZZI, ENRICO; TAROZZO, MIRCO
To: METHANOL CASALE S.A.
Reel/Frame 014208/0489 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 25, 2003
From: EBATA, ATSUSHI; KAWAMOTO, SHINICHI
To: HITACHI, LTD.
Reel/Frame 014435/0813 →