Method of forming aluminide diffusion coatings
View Patent ↗Method of forming an outwardly grown aluminide diffusion coating on a superalloy substrate disposed in a coating retort including the steps of heating the substrate to a temperature of 900 to 1200 degrees C., flowing a coating gas comprising aluminum trichloride and a carrier gas through the coating retort at a flow rate of the coating gas of about 100 to about 450 standard cubic feet per hour, providing a concentration of aluminum trichloride in the retort of less than 1.4% by volume of the coating gas, and providing a total pressure of the coating gas in the coating retort of about 100 to about 450 Torr.
1. A method of forming an outwardly grown aluminide diffusion coating on a superalloy substrate disposed in a coating chamber, comprising heating the substrate to a temperature of 900 to 1200 degrees C., flowing a coating gas mixture comprising aluminum trichloride and a carrier gas through the chamber at a flow rate of the coating gas of about 100 to about 450 standard cubic feet per hour, providing a concentration of aluminum trichloride of less than about 1.4% by volume of the coating gas mixture in the chamber, and providing a total pressure of the coating gas mixture in the chamber of about 100 to about 450 Torr to increase coating rate of the outwardly grown aluminide diffusion coating on the substrate.
2. The method of claim 1 wherein the flow rate of coating gas mixture through the chamber is 200 to 400 standard cubic feet per hour, the concentration of aluminum trichloride is about 0.6 to about 1.2% by volume of the coating gas mixture in the chamber, and the total pressure of the coating gas mixture in the chamber of about 100 to about 300 Torr.
3. The method of claim 2 wherein the flow rate of coating gas mixture through the chamber is 300 standard cubic feet per hour, the concentration of aluminum trichloride is about 1.0% by volume of the coating gas mixture in the chamber, and the total pressure of the coating gas mixture in the chamber is about 200 Torr.
4. The method of clam 1 including before forming the coating on the substrate, depositing a layer comprising platinum on the substrate.
5. The method of claim 1 wherein the coating gas mixture comprises aluminum trichloride and balance hydrogen.
6. The method of claim 1 wherein the substrate is heated to a temperature of about 1080 degrees C.