IP Library Granted Patent US 7,214,356
Granted Patent B2
US 7,214,356 · App. 10/677,052 · Granted May 8, 2007

Wet scrubbing apparatus and method for controlling NOx emissions

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Quick Facts
Patent No.
US 7,214,356
App. No.
10/677,052
Granted
May 8, 2007
Kind
B2
Abstract

An apparatus for controlling NOx emissions which includes a chamber having a wall surface and an interior, a flue gas entrance and a flue gas exit for a flue gas to enter and exit the interior of the chamber, a gas quenching zone in which the temperature of the gas can be lowered, an ozone injection and retention zone in the chamber, and a liquid spray zone including at least one spray nozzle for spraying a liquid towards the wall surface.

Claims (39)

1. A method of controlling NOx emissions comprising:

permitting flue gas to enter an interior of a chamber;

quenching flue gas to lower the temperature of the flue gas;

injecting ozone into an ozone injection zone of the interior of the chamber;

spraying a liquid towards the walls of the chamber to capture reaction products of the oxidation process; and

maintaining a portion of the ozone injection zone of the chamber substantially free of droplets of the liquid.

2. The method according to claim 1 , wherein the liquid includes a sodium, calcium, or magnesium reagent.

3. A method according to claim 1 , wherein the injection of ozone into the interior of the chamber occurs below the spraying the liquid, and the entrance of a flue gas is below spraying the liquid.

4. A method according to claim 1 , wherein the spraying of a liquid includes the step of injecting a liquid through 3 or more spray nozzles.

5. A method according to claim 1 , further comprising maintaining a liquid to gas ratio between 5–80 gallons per 1000 feet 3 of gas flow.

6. A method according to claim 1 , further comprising allowing flue gas to travel through the apparatus at a rate from 3–26 feet per second.

7. A method according to claim 1 , wherein NOx emissions are less than 40 ppmdv.

8. A method according to claim 3 , further comprising maintaining a percentage of NOx removal that is greater than or equal to 50%.

9. A method according to claim 1 , further comprising quenching the flue gas to a temperature of between 120°–80° F.

10. A method according to claim 1 , wherein the quenching of the flue gas occurs at the entrance into the interior of the chamber, and includes spraying liquid through the gas as it enters the chamber.

11. A method of controlling NOx emissions comprising the steps of:

introducing a flue gas into a chamber;

quenching flue gas;

injecting ozone into an ozone injection and retention zone in the interior of the chamber;

spraying a liquid towards the walls of the chamber to capture reaction products of the oxidation process so as to maintain a substantially droplet-free chamber interior in the vicinity of the ozone injection and retention zone.

12. A method according to claim 11 , wherein the injecting ozone into the interior of the chamber occurs prior to spraying a liquid.

13. A method according to claim 11 , wherein spraying the liquid comprises spraying the liquid through 3 or more spray nozzles.

14. A method according to claim 11 , further comprising maintaining a liquid to gas ratio between 5–80 gallons per 1000 feet 3 of gas flow.

15. A method according to claim 11 , further comprising allowing flue gas to travel through the apparatus at a rate of from 3–26 feet/second.

16. A method according to claim 11 , wherein NOx emissions are less or equal to 50 ppmdv.

17. A method according to claim 11 , further comprising maintaining a percentage of NOx removal greater than or equal to 50%.

18. A method according to claim 11 , further comprising quenching the flue gas to a temperature of between 140°–160° F.

19. A method of dontrolling NOx emissions comprising:

permitting flue gas to enter an interior of a chamber;

spraying a quenching liquid toward the walls of the chamber to lower the temperature of the flue gas;

injecting ozone into an ozone injection zone of the interior of the chamber; and

maintaining a portion of the ozone injection zone of the chamber substantially free of droplets of the quenching liquid.

20. The method of claim 19 further comprising the step of spraying a product-capturing liquid towards the walls of the chamber to capture reaction products of the oxidation process.

21. A method of controlling NOx emissions comprising:

permitting flue gas to enter an interior of a chamber;

spraying a product-capturing liquid towards the walls of the chamber to capture reaction products of the oxidation process;

injecting ozone into an ozone injection zone of the interior of the chamber; and

maintaining a portion of the ozone injection zone of the chamber substantially free of droplets of the product-capturing liquid.

22. The method of claim 21 further comprising the step of spraying a quenching liquid toward the walls of the chamber to lower the temperature of the flue gas.

Assignments (5)
RELEASE OF SECURITY INTEREST RECORDED AT REEL/FRAME 059594/0190 Recorded May 13, 2025
From: MADISON PACIFIC TRUST LIMITED
To: BELCO TECHNOLOGIES CORPORATION
Reel/Frame 071276/0849 →
IP SECURITY AGREEMENT SUPPLEMENT Recorded Apr 4, 2022
From: BELCO TECHNOLOGIES CORPORATION
To: MADISON PACIFIC TRUST LIMITED, AS SECURITY AGENT
Reel/Frame 059594/0190 →
RELEASE OF SECURITY INTEREST RECORDED AT REEL 28571, FRAME 0141 Recorded Oct 14, 2015
From: WELLS FARGO BANK, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: NEKTAR THERAPEUTICS
Reel/Frame 036866/0700 →
GRANT OF SECURITY INTEREST Recorded Jul 17, 2012
From: NEKTAR THERAPEUTICS
To: WELLS FARGO BANK, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 028571/0141 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 17, 2003
From: HSIEH, JOSEPH; GILMAN, KEVIN R.; PHILIBERT, DOMINIQUE; EAGLESON, SCOTT; MORIN, ANDREW
To: BELCO TECHNOLOGIES CORPORATION
Reel/Frame 014695/0100 →