IP Library Granted Patent US 6,962,963
Granted Patent B2
US 6,962,963 · App. 10/688,582 · Granted Nov 8, 2005

Enzymatic synthesis of polymers

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Quick Facts
Patent No.
US 6,962,963
App. No.
10/688,582
Granted
Nov 8, 2005
Kind
B2
Abstract

The invention relates to new methods of enzymatic synthesis of polymers such as polyorganosilicones and polyesters, and new polymers made by these methods.

Claims (33)

1. A polyorganosilicone of the formula:

wherein

each R′, independently is a hydroxy or alkoxy; each R″, independently is a hydrogen, alkyl, alkoxy, aryl, or aryloxy;

each x, independently, is an integral of 1 to 10;

y is an integral of 1 to 1,000;

n is an integral of 1 to 10,000;

A is O or NH; and

B is alkylene, arylene, or oxaalkylene.

2. A polyorganosilicone of claim 1 , wherein x is ten; y is 1000; and n is 10000.

3. A method of synthesizing a polyorganosilicone polymer of claim 1 , the method comprising:

mixing linear or cyclic monomers, oligomers, macromers, or a combination thereof to form a monomer mixture;

adding a lipase, esterase, or protease to the monomer mixture to form a reaction mixture; and

reacting the reaction mixture for a time and under polymerizing conditions suitable to obtain the polyorganosilicone polymer.

4. The method of claim 3 , further comprising mixing the polymer with a fire-retardant.

5. A method of retarding fire, the method comprising using the polyorganosilicone polymer of claim 1 as a fire-retardant.

6. A method of controlled drug delivery, the method comprising using the polyorganosilicone polymer of claim 1 as a carrier for controlled drug delivery.

7. A method of delivering bio-implants, the method comprising using the polyorganosilicone polymer of claim 1 as a carrier for bio-implants.

8. A method of tissue engineering, the method comprising using the polyorganosilicone polymer of claim 1 as a biodegradable matrix for tissue engineering.

9. A packaging material comprising the polyorganosilicone polymer of claim 1 .

10. A thermal insulator comprising the polyorganosilicone polymer of claim 1 .

11. An antioxidant agent comprising the polyorganosilicone polymer of claim 1 , and free phenolic groups.

12. A photovoltaic device comprising a polyorganosilicone polymer of claim 1 , and conjugated polymers.

13. A biosensor device comprising a polyorganosilicone polymer of claim 1 , and conjugated polymers.

14. A composition or structure comprising a polyorganosilicone of the formula:

wherein

each R′, independently is a hydroxy or alkoxy; each R″, independently is a hydrogen, alkyl, alkoxy, aryl, or aryloxy;

each x, independently, is an integral of 1 to 10;

y is an integral of 1 to 1,000;

n is an integral of 1 to 10,000;

A is O or NH; and

B is alkylene, arylene, or oxaalkylene.

15. The composition of claim 14 , further comprising a fire retardant.

16. A method of retarding fire, the method comprising using the composition or structure of claim 15 as a fire-retardant.

Assignments (4)
CORRECTIVE ASSIGNMENT TO CORRECT THE NAMED ASSIGNEE FROM THE SECRETARY OF THE NAVY TO THE U.S. GOVERNMENT AS REPRESENTED BY THE SECRETARY OF THE ARMY PREVIOUSLY RECORDED ON REEL 017105 FRAME 0238. ASSIGNOR(S) HEREBY CONFIRMS THE "1. ASSIGN TO THE GOVERNMENT OF THE UNITED STATES, AS REPRESENTED BY THE SECRETARY OF THE ARMY". Recorded Dec 1, 2010
From: SAMUELSON, LYNNE A., MS
To: GOVERNMENT OF THE UNITED STATES, AS REPRESENTED BY THE SECRETARY OF THE ARMY
Reel/Frame 025434/0295 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 5, 2009
From: SAMUELSON, LYNNE A.
To: ARMY, UNITED STATES OF AMERICA, THE, AS REPRESENTED BY THE SECRETARY
Reel/Frame 022214/0692 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 9, 2005
From: SAMUELSON, LYNNE ANN
To: SECRETARY OF THE NAVY, USA AS REPRESENTED BY THE
Reel/Frame 017105/0238 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 9, 2004
From: KUMAR, RAJESH; WATTERSON, ARTHUR C.; PARMAR, VIRINDER SINGH; KUMAR, JAYANT
To: UNIVERSITY OF MASSACHUSETTS
Reel/Frame 014509/0300 →