Process for producing magnetic recording medium
View Patent ↗A process for producing a magnetic recording medium having at least one magnetic layer formed above a support is provided. The process includes a step of providing, on at least one side of the support, a smoothing coating layer having a thickness of 0.10 to 1 μm, a surface roughness of at most 5 nm, a number of projections having a height of 20 nm or higher measured by atomic force microscopy (AFM) of at most 20 projections/900 μm 2 , and an amount of residual solvent of less than 10 mg/m 2 , and a step of forming at least one magnetic layer on or above the smoothing coating layer without winding up.
1. A process for producing a magnetic recording medium having at least one magnetic layer formed above a support, the process comprising:
a step of providing, on at least one side of the support, a smoothing coating layer having a thickness of 0.10 to 1 μm, a surface roughness of at most 5 nm, a number of projections having a height of 20 nm or higher measured by atomic force microscopy (AFM) of at most 20 projections/900 μm 2 , and an amount of residual solvent of less than 10 mg/m 2 ; and
a step of forming at least one magnetic layer on or above the smoothing coating layer without winding up.
2. The process for producing a magnetic recording medium according to claim 1 , wherein the smoothing coating layer is formed by coating with a polymer solution and drying.
3. The process for producing a magnetic recording medium according to claim 2 , wherein in the polymer solution, a polymer compound having a number average molecular weight of 10,000 to 100,000 is used.
4. The process for producing a magnetic recording medium according to claim 1 , wherein the smoothing coating layer is formed by coating with a coating solution containing a compound having a radiation curing functional group in the molecule, and then irradiating with radiation so as to cure the compound.
5. The process for producing a magnetic recording medium according to claim 4 , wherein the compound having the radiation curing functional group is a di- or higher-functional acrylate compound having a molecular weight of 200 to 4,000.
6. The process for producing a magnetic recording medium according to claim 1 , wherein the smoothing coating layer is formed by coating with a coating solution containing a compound having a ultraviolet-curing functional group in the molecule, and then irradiating with ultraviolet rays so as to cure the compound.
7. The process for producing a magnetic recording medium according to claim 1 , wherein the smoothing coating layer has a thickness of 0.2 to 0.7 μm.
8. The process for producing a magnetic recording medium according to claim 1 , wherein the smoothing coating layer has a surface roughness of 0.5 to 4.0 nm.
9. The process for producing a magnetic recording medium according to claim 1 , wherein the smoothing coating layer has an amount of residual solvent of at most 5 mg/m 2 .
10. The process for producing a magnetic recording medium according to claim 1 , wherein the smoothing coating layer has an amount thereof that dissolves in a methyl ethyl ketone/cyclohexanone mixed solution (1:1) of 0.0 to 0.4 mg/cm 2 .
11. The process for producing a magnetic recording medium according to claim 1 , wherein the support has a thickness of 3.0 to 6.5 μm.
12. The process for producing a magnetic recording medium according to claim 1 , wherein the magnetic layer has a thickness of 20 to 500 nm.
13. The process for producing a magnetic recording medium according to claim 1 , wherein a non-magnetic layer containing a non-magnetic powder and a binder and having a thickness of 0.5 to 3.0 μm is provided between the magnetic layer and the smoothing coating layer.
14. The process for producing a magnetic recording medium according to claim 13 , wherein the non-magnetic layer and the magnetic layer are provided by wet-on-wet coating.
15. The process for producing a magnetic recording medium according to claim 1 , wherein the process comprises a step of drying with drying air at 60° C. or higher after the step of forming the magnetic layer.
16. The process for producing a magnetic recording medium according to claim 1 , wherein the magnetic layer employs a ferromagnetic metal powder.
17. The process for producing a magnetic recording medium according to claim 1 , wherein the magnetic layer employs a hexagonal ferrite powder.