IP Library Granted Patent US 7,270,876
Granted Patent B2
US 7,270,876 · App. 10/722,951 · Granted Sep 18, 2007

Enhanced adhesion of polyethylene terephthalate to paperboard

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Quick Facts
Patent No.
US 7,270,876
App. No.
10/722,951
Granted
Sep 18, 2007
Kind
B2
Abstract

A unique primer emulsion chemistry yields excellent adhesion of polyethylene terephthalate (PET)resin to clay coated paperboard (with high starch content)at reduced coatweights of the primer emulsion and the resin as compared to other primer and tie-resin chemistries currently employed for moisture barrier applications. A primer used for adhesion enhancement is an ammonium catalyzed, self-crosslinking copolymer of ethylene-vinyl acetate with N-methylol acryl amide functional groups attached to a polymer backbone. Use of the primer in amounts up to about 0.5 pounds per ream permits PET coatweights of as low as 10–12 lbs per ream and lower for some applications.

Claims (21)

1. A package material comprising

a paperboard substrate,

a primer applied to said substrate, wherein the primer is ammoniuxn catalyzed, self-cross linking copolymer of ethylene-vinyl acetate with N-methylol acxyl amide functional groups attached to a polymer backbone wherein said primer has a coat weight of 0.1–0.5 lbs./ream,

a polyester coating applied to said primed substrate, said coating having a coat weight of at least 12 lbs./ream.

2. The packaging material of claim 1 wherein said coating is polyethylene terephthalate.

3. The packaging material of claim 1 , wherein said paperboard substrate is clay coated.

4. The packaging material of claim 1 , wherein said paperboard substrate is clay coated and said polyester coating comprises polyethylene terephthalate.

5. The method of forming a packaging material comprising providing a paperboard substrate,

applying a primer to said substrate, and

applying a polyester coating to said primed substrate with a coat weight of up to 12 lbs/ream,

wherein said polyester coating is extruded onto said substrate at a line speed of 800–1200 feet per minute.

6. The method of claim 5 , wherein said coating is polyethylene terephthalate.

7. The method of claim 5 , wherein said primer is an ammonium catalyzed, self- cross linking copolymer of ethylene-vinyl acetate with N-methylol acryl amide functional group attached to a polymer backbone.

8. The method of claim 5 further comprising flame treating said substrate.

9. The method of claim 5 further comprising water misting said substrate.

10. The method of claim 9 wherein water is misted at 0.01 to 0.1 lbs/ream.

11. The method of claim 5 further comprising a clay coating on said substrate.

12. The method of claim 5 wherein said polyester coating has a coat weight of 10 lbs/ream.

13. The method of claim 5 wherein said coat weight is 10 lbs/ream.

14. The method of claim 4 wherein said primer is epoxy modified polyolefin tie resins.

15. The method of claim 5 , further comprising coating said paperboard substrate with a clay coating and wherein said polyester coating comprises polyethylene terephthalate.

Assignments (9)
RELEASE OF SECURITY INTEREST Recorded Apr 15, 2026
From: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS SUCCESSOR‑IN‑INTEREST TO U.S. BANK NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: GRAPHIC PACKAGING INTERNATIONAL, LLC
Reel/Frame 075415/0575 →
SECURITY INTEREST Recorded Apr 1, 2021
From: GRAPHIC PACKAGING INTERNATIONAL, LLC
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 055811/0676 →
RELEASE OF SECURITY INTEREST Recorded Mar 10, 2021
From: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
To: GRAPHIC PACKAGING INTERNATIONAL, LLC; FIELD CONTAINER QUERETARO (USA), L.L.C.
Reel/Frame 055545/0204 →
SECURITY AGREEMENT Recorded Mar 8, 2021
From: GRAPHIC PACKAGING INTERNATIONAL, LLC
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 055520/0204 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 11, 2018
From: GRAPHIC PACKAGING INTERNATIONAL PARTNERS, LLC
To: GRAPHIC PACKAGING INTERNATIONAL, LLC
Reel/Frame 044591/0681 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 11, 2018
From: INTERNATIONAL PAPER COMPANY
To: GRAPHIC PACKAGING INTERNATIONAL PARTNERS, LLC
Reel/Frame 044591/0640 →
SECURITY AGREEMENT Recorded Jan 8, 2018
From: GRAPHIC PACKAGING INTERNATIONAL, LLC
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 045020/0746 →
SECURITY INTEREST Recorded Jan 5, 2018
From: GRAPHIC PACKAGING INTERNATIONAL, LLC (FORMERLY KNOWN AS GRAPHIC PACKAGING INTERNATIONAL, INC.); FIELD CONTAINER QUERETARO (USA), L.L.C.
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 045009/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 7, 2004
From: ROHATGI, VIVEK; BEDNARIK, LADISLAV; REED, DAVID VERD
To: INTERNATIONAL PAPER COMPANY
Reel/Frame 015422/0245 →