IP Library Granted Patent US 7,259,195
Granted Patent B2
US 7,259,195 · App. 10/759,804 · Granted Aug 21, 2007

Pigments treated with organo-phosphoric acids and their salts

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Quick Facts
Patent No.
US 7,259,195
App. No.
10/759,804
Granted
Aug 21, 2007
Kind
B2
Abstract

A unique treatment for pigments is provided. This treatment, which uses certain organo-phosphoric acids and/or their salts, imparts improved physical and chemical qualities including lacing resistance, improved dispersion and decreased chemical reactivity when these treated pigments are incorporated into polymeric matrices.

Claims (27)

1. A polymer film comprising:

(i) a treated pigment, wherein said treated pigment comprises titanium dioxide and an organo-phosphoric acid compound having the formula:

R′ n —P (n−2) O 4+[3(n−3)]

wherein n=4-14, and each R′ is an organic group having from 2 to 22 carbon atoms or hydrogen and within any one molecule, any two or more R′ groups may be the same provided that at least one of the R′ groups is not hydrogen; and

(ii) a polymer,

wherein said organo-phosphoric acid compound is present in an amount from about 0.01 percent to about 5 percent by weight, based on the weight of the titanium dioxide, and said treated pigment is present in an amount of about 20 wt. % based on the weight of the polymer film.

2. The polymer film of claim 1 , wherein said polymer is polyethylene.

3. The polymer film of claim 1 , further comprising an additional metal oxide selected from the group consisting of aluminum oxide, silicon dioxide and zirconium oxide.

4. A polymer film comprising:

(i) a treated pigment, wherein said treated pigment comprises titanium dioxide and an organo-phosphoric acid compound having the formula:

R′ n —P (n−2) O 4+[3(n−3)]

wherein n=4-14, and each R′ is an organic group having from 2 to 22 carbon atoms or hydrogen and within any one molecule, any two or more R′ groups may be the same provided that at least one of the R′ groups is not hydrogen; and

(ii) a polymer, wherein said polymer comprises polyethylene,

wherein said organo-phosphoric acid compound is present in an amount from about 0.01 percent to about 5 percent by weight, based on the weight of the titanium dioxide, and wherein said treated pigment is present in an amount of about 20 wt. % based on the weight of the polymer film.

5. A polymer film comprising:

(i) a treated pigment, wherein said treated pigment comprises titanium dioxide and an organometaphosphate compound having the formula:

(R″PO 3 ) m

wherein m=1-14, and each R″ is an organic group having from 2 to 22 carbon atoms or hydrogen and within any one molecule, any two or more R″ groups may be the same provided that at least one of the R″ groups is not hydrogen; and

(ii) a polymer,

wherein said organometaphosphate compound is present in an amount from about 0.01 percent to about 5 percent by weight, based on the weight of the titanium dioxide, and said treated pigment is present in an amount of about 20 wt. % based on the weight of the polymer film.

6. The polymer film of claim 5 , wherein said polymer is polyethylene.

7. The polymer film of claim 5 , further comprising an additional metal oxide selected from the group consisting of aluminum oxide, silicon dioxide and zirconium oxide.

8. A polymer film comprising:

(i) a treated pigment, wherein said treated pigment comprises titanium dioxide and an organometaphosphate compound having the formula:

(R″PO 3 ) m

wherein m=1-14, and each R″ is an organic group having from 2 to 22 carbon atoms or hydrogen and within any one molecule, any two or more R″ groups may be the same provided that at least one of the R′ groups is not hydrogen; and

(ii) a polymer, wherein said polymer comprises polyethylene, wherein said organometaphosphate compound is present in an amount from about 0.01 percent to about 5 percent by weight, based on the weight of the titanium dioxide, and wherein said treated pigment is present in an amount of about 20 wt. % based on the weight of the polymer film.

Assignments (7)
RELEASE OF SECURITY INTEREST Recorded Apr 7, 2022
From: WILMINGTON TRUST, NATIONAL ASSOCIATION
To: TRONOX LLC
Reel/Frame 059629/0581 →
SECURITY INTEREST Recorded Mar 12, 2021
From: TRONOX LLC
To: HSBC BANK USA, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 055579/0619 →
SECURITY INTEREST Recorded May 1, 2020
From: TRONOX LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 052554/0529 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 10, 2019
From: CRISTAL USA INC.
To: TRONOX LLC
Reel/Frame 049148/0729 →
RELEASE OF SECURITY INTEREST Recorded Mar 19, 2014
From: HSBC BANK USA, NATIONAL ASSOCIATION
To: MILLENNIUM INORGANIC CHEMICALS INC.
Reel/Frame 032478/0788 →
RELEASE OF SECURITY INTEREST Recorded Mar 19, 2014
From: HSBC BANK USA, NATIONAL ASSOCIATION
To: MILLENNIUM INORGANIC CHEMICALS INC.
Reel/Frame 032480/0232 →
CHANGE OF NAME Recorded Aug 9, 2013
From: MILLENNIUM INORGANIC CHEMICALS, INC.
To: CRISTAL USA INC.
Reel/Frame 030982/0732 →