IP Library Granted Patent US 7,494,960
Granted Patent B2
US 7,494,960 · App. 10/771,907 · Granted Feb 24, 2009

Lubricant compositions comprising an antioxidant blend

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Quick Facts
Patent No.
US 7,494,960
App. No.
10/771,907
Granted
Feb 24, 2009
Kind
B2
Abstract

A composition is disclosed that comprises a lubricant and at least a first antioxidant and a second antioxidant, the first antioxidant being a hindered phenolic and the second antioxidant being a thioether. Also disclosed is a method of increasing the oxidation stability of a lubricant comprising adding thereto at least a first antioxidant and a second antioxidant, the first antioxidant being a hindered phenolic and the second antioxidant being a thioether.

Claims (31)

1. A composition comprising:

A) a lubricant; and

B) a liquid solution of

(i) butyl-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, and

(ii) ditridecylthiodipropionate;

wherein the ditridecylthiodipropionate comprises greater than 40% by weight of the liquid solution.

2. The composition of claim 1 wherein the lubricant is a lubricating oil.

3. The composition of claim 1 wherein the weight ratio of the butyl-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate to the ditridecylthiodipropionate is 45:55.

4. The composition of claim 1 further comprising:

(c) at least one additional additive selected from the group consisting of dispersants, detergents, rust inhibitors, antioxidants, metal deactivators, antiwear agents, antifoamants, friction modifiers, seal swell agents, demulsifiers, VI improvers, and pour point depressants.

5. A composition comprising a lubricant and a liquid antioxidant blend comprising at least a first antioxidant and a second antioxidant, the first antioxidant being butyl-3-(3,5-di-tert-butyl-4- hydroxyphenyl)propionate and the second antioxidant being a dialkylthiodipropionate of the structure:

wherein R and R′ are independently selected from the group consisting of straight chain and branched chain alkyl groups, and wherein the liquid blend comprises at least 40% by weight of the second antioxidant dissolved in the first antioxidant.

6. The composition of claim 5 wherein the lubricant is a lubricating oil.

7. The composition of claim 5 wherein the second antioxidant is ditridecylthiodipropionate.

8. The composition of claim 5 wherein the weight ratio of the first antioxidant to the second antioxidant is 45:55.

9. The composition of claim 5 further comprising at least one additional additive selected from the group consisting of dispersants, detergents, rust inhibitors, antioxidants, metal deactivators, antiwear agents, antifoamants, friction modifiers, seal swell agents, demulsifiers, VI improvers, and pour point depressants.

10. A method of increasing the oxidation stability of a lubricant comprising the steps of:

(A) dissolving a first antioxidant that is butyl-3-(3,5-di-tert-butyl-4- hydroxyphenyl)propionate in a second antioxidant that is a dialkylthiodipropionate of the structure:

wherein R and R′ are independently selected from the group consisting of straight chain and branched chain alkyl groups to form a liquid antioxidant blend solution comprising greater than 40% by weight of the second antioxidant, and

(B) adding the antioxidant blend solution to the lubricant.

11. The method of claim 10 wherein the lubricant is a lubricating oil.

12. The method of claim 10 wherein the second antioxidant is ditridecylthiodipropionate.

13. The method of claim 10 wherein the weight ratio of the first antioxidant to the second antioxidant is 45:55.

14. The method of claim 10 further comprising at least one additional additive selected from the group consisting of dispersants, detergents, rust inhibitors, antioxidants, metal deactivators, antiwear agents, antifoamants, friction modifiers, seal swell agents, demulsifiers, VI improvers, and pour point depressants.

15. A method of increasing the oxidation stability of a lubricant comprising the steps of:

(A) dissolving butyl-3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate in ditridecylthiodipropionate to form a liquid antioxidant blend solution comprising greater than 40% by weight of the ditridecylthiodipropionate;

(B) adding

the liquid antioxidant blend solution to the lubricant.

16. The method of claim 15 wherein the lubricant is a lubricating oil.

17. The method of claim 15 wherein the weight ratio of the butyl-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate to the ditridecylthiodipropionate is 45:55.

18. The method of claim 15 further comprising adding to the lubricant at least one additional additive selected from the group consisting of dispersants, detergents, rust inhibitors, antioxidants, metal deactivators, antiwear agents, antifoamants, friction modifiers, seal swell agents, demulsifiers, VI improvers, and pour point depressants.

Assignments (12)
CHANGE OF NAME Recorded Sep 25, 2018
From: CROMPTON CORPORATION
To: CHEMTURA CORPORATION
Reel/Frame 047141/0152 →
RELEASE OF FIRST LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded May 11, 2017
From: BANK OF AMERICA, N.A.
To: CHEMTURA CORPORATION; BIOLAB FRANCHISE COMPANY, LLC; BIO-LAB, INC.; CROMPTON COLORS INCORPORATED; CROMPTON HOLDING CORPORATION; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; LAUREL INDUSTRIES HOLDINGS, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC
Reel/Frame 042447/0508 →
RELEASE OF SECOND LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded May 11, 2017
From: BANK OF AMERICA, N.A.
To: CHEMTURA CORPORATION; BIOLAB FRANCHISE COMPANY, LLC; BIO-LAB, INC.; CROMPTON COLORS INCORPORATED; CROMPTON HOLDING CORPORATION; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; LAUREL INDUSTRIES HOLDINGS, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC
Reel/Frame 042449/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 21, 2013
From: MIGDAL, CYRIL A.; SIKORA, DAVID J.
To: CHEMTURA CORPORATION
Reel/Frame 031052/0663 →
SECDOND LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 21, 2011
From: CHEMTURA CORPORATION; BIOLAB FRANCHISE COMPANY, LLC; BIO-LAB, INC.; CROMPTON COLORS INCORORATED; CROMPTON HOLDING CORPORATION; CLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; HAOMECARE LABS, INC.; LAUREL INDUSTRIES HOLDINGS, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC
To: BANK OF AMERICA, N. A.
Reel/Frame 027881/0347 →
FIRST LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT. Recorded Mar 21, 2011
From: CHEMTURA CORPORATION; BIOLAB FRANCHISE COMPANY, LLC; BIO-LAB, INC.; CROMPTON COLORS INCORPORATED; CROMPTON HOLDING CORPORATION; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; LAUREL INDUSTRIES HOLDINGS, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC
To: BANK OF AMERICA, N.A.
Reel/Frame 026028/0622 →
INTELLECTUAL PROPERTY SECURITY RELEASE AGREEMENT Recorded Mar 21, 2011
From: CITIBANK, N.A.
To: CHEMTURA CORPORATION; A & M CLEANING PRODUCTS, LLC; ASCK, INC; BIOLAB COMPANY STORE, LLC; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIOLAB TEXTILES ADDITIVES, LLC; BIOLAB, INC.; CROMPTON COLORS INCORPORATED; CROMPTON MONOCHEM, INC.; CNK CHEMICAL REALTY CORPORATION; CROMPTON HOLDING CORPORATION; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GT SEED TREATMENT, INC.; ISCI, INC; GREAT LAKES CHEMICAL GLOBAL, INC.; HOMECARE LABS, INC.; KEM MANUFACTURING CORPORATION; LAUREL INDUSTRIES HOLDINGS, INC.; NAUGATUCK TREATMENT COMPANY; UNIROYAL CHEMICAL COMPANY LIMITED (DELAWARE); MONOCHEM, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC; WRL OF INDIANA, INC.; BIOLAB FRANCHISE COMPANY, LLC
Reel/Frame 026039/0142 →
AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Feb 22, 2010
From: CHEMTURA CORPORATION; A & M CLEANING PRODUCTS, LLC; AQUA CLEAR INDUSTRIES, LLC; ASCK, INC.; ASEPSIS, INC.; BIOLAB COMPANY STORE, LLC; BIOLAB FRANCHISE COMPANY, LLC; BIOLAB TEXTILE ADDITIVES, LLC; BIO-LAB, INC.; CNK CHEMICAL REALTY CORPORATION; CROMPTON COLORS INCORPORATED; CROMPTON HOLDING CORPORATION; CROMPTON MONOCHEM, INC.; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; ISCI, INC.; KEM MANUFACTURING CORPORATION; LAUREL INDUSTRIES HOLDINGS, INC.; MONOCHEM, INC.; NAUGATUCK TREATMENT COMPANY; RECREATIONAL WATER PRODUCTS, INC.; UNIROYAL CHEMICAL COMPANY LIMITED (DELAWARE); WEBER CITY ROAD LLC; WRL OF INDIANA, INC.
To: CITIBANK, N.A.
Reel/Frame 023998/0001 →
CHANGE OF NAME Recorded Sep 15, 2008
From: CROMPTON CORPORATION
To: CHEMTURA CORPORATION
Reel/Frame 021528/0364 →
RELEASE OF LIEN IN PATENTS Recorded Jul 13, 2005
From: DEUTSCHE BANK AG, NEW YORK BRANCH
To: CROMPTON CORPORATION
Reel/Frame 016513/0745 →
SECURITY AGREEMENT Recorded Nov 10, 2004
From: CROMPTON CORPORATION
To: DEUTSCHE BANK AG NEW YORK BRANCH
Reel/Frame 015370/0467 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 10, 2004
From: MIGDAL, CYRIL A.; SIKORA, DAVID J.
To: CROMPTON CORPORATION
Reel/Frame 015306/0800 →