IP Library Granted Patent US 8,198,302
Granted Patent B2
US 8,198,302 · App. 10/790,662 · Granted Jun 12, 2012

Compositions and methods with enhanced therapeutic activity

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 8,198,302
App. No.
10/790,662
Granted
Jun 12, 2012
Kind
B2
Abstract

Novel quinone and catechol compositions, compositions containing prodrugs of quinone and catechol compositions, and methods of use for the treatment of solid tumor cancers and other vascular proliferative disorders. The disclosure particularly relates to the discovery of dual activity agents capable of generating both a vascular targeting effect and direct tumor cell cytotoxicity in order to achieve an enhanced anti-tumor response in a patient.

Claims (47)

1. A composition of the following formula (V):

wherein

a. Z is an ethylene (—CH═CH—) bridge in the cis (Z) isomeric configuration;

b. R 1 and R 2 are OH or a prodrug form thereof;

c. R 3 is selected from the group consisting of

i) a C 1 , C 2 , C 3 , C 4 or C 5 branched or straight-chain lower alkoxy, cycloalkoxy, heterocycloalkoxy, aryloxy, or lower alkanoyloxy;

ii) a halogen or trihaloalkyl;

iii) a C 1 , C 2 , C 3 , C 4 or C 5 branched or straight chain lower alkyl, allyl, allyloxy, vinyl, or vinyloxy;

iv) a C 1 , C 2 , C 3 , C 4 or C 5 primary, secondary, or tertiary alcohol; and

v) oxo, lower alkanoyl, thio, sulfonyl, sulfonamide, nitro, nitrosyl, cyano, carboxy, carbamyl, aryl, or heterocycle;

d. R 4 , R 5 , and R 9 are hydrogen,

e. R 6 and R 8 are the same or different and selected from the group consisting of hydrogen and

i) a C 1 , C 2 , C 3 , C 4 or C 5 branched or straight-chain lower alkoxy, cycloalkoxy, heterocycloalkoxy, aryloxy, or lower alkanoyloxy;

ii) a halogen or trihaloalkyl;

iii) a C 1 , C 2 , C 3 , C 4 or C 5 branched or straight chain lower alkyl, allyl, allyloxy, vinyl, or vinyloxy; or

iv) a C 1 , C 2 , C 3 , C 4 or C 5 primary, secondary, or tertiary alcohol; and

v) nitro;

f. R 7 , is selected from the group consisting of

i) a C 1 , C 2 , C 3 , C 4 or C 5 branched or straight-chain lower alkoxy, cycloalkoxy, heterocycloalkoxy, aryloxy, or lower alkanoyloxy;

ii) a halogen or trihaloalkyl;

iii) a C 1 , C 2 , C 3 , C 4 or C 5 branched or straight chain lower alkyl, allyl, allyloxy, vinyl, or vinyloxy;

iv) a C 1 , C 2 , C 3 , C 4 or C 5 primary, secondary, or tertiary alcohol; and

v) nitro;

provided that said compound is not combretastatin A1 or prodrug thereof.

2. The composition of claim 1 , wherein R 6 , R 7 , and R 8 are not hydrogen.

3. The composition of claim 2 , wherein R 6 , R 7 and R 8 are the same.

4. The composition of claim 3 , wherein R 6 , R 7 and R 8 are methoxy.

5. The composition of claim 4 , wherein R 3 is —CH 3 , —CH 2 CH 3 , —OCH 2 CH 3 , —F, —Br, —CF 3 , —CBr 3 , —O—CH 2 —CH═CH 2 , —CH 2 —CH═CH 2 , —NO 2 , -cyano, or -carboxy.

6. The composition of claim 3 , wherein R 6 , R 7 , and R 8 are F.

7. The composition of claim 6 , wherein R 3 is —CH 3 , —CH 2 CH 3 , —OCH 2 CH 3 , —F, —Br, —CF 3 , —CBr 3 , —O—CH 2 —CH═CH 2 , —CH 2 —CH═CH 2 , —NO 2 , -cyano, -carboxy, or -benzyl.

8. A composition selected from the group consisting of

3-Ethyl-6-[(Z)-2-(3,4,5-trimethoxyphenyl)vinyl]-1,2-dihydroxybenzene,

3-Methyl-6-[(Z)-2-(3,4,5-trimethoxyphenyl)vinyl]-1,2-dihydroxybenzene,

4-Bromo-6-[(Z)-2-(3,4,5-trimethoxyphenyl)vinyl]-1,2-dihydroxybenzene,

4-Phenyl-6-[(Z)-2-(3,4,5-trimethoxyphenyl)vinyl]-1,2-dihydroxybenzene,

3-Allyl-6-[(Z)-2-(3,4,5-trimethoxyphenyl)vinyl]-1,2-dihydroxybenzene,

4-Fluoro-6-[(Z)-2-(3,4,5-trimethoxyphenyl)vinyl]-1,2-dihydroxybenzene,

2,3,4-Trihydroxy-6-[(Z)-2(3,4,5-trimethoxyphenyl)vinyl]-benzene,

2,3-Dihydroxy-4-ethoxy-6-[(Z)-2-(3,4,5-trimethoxyphenyl)vinyl]-benzene,

2,3-Dihydroxy-4-allyloxy-6-[(Z)-2-(3,4,5-trimethoxyphenyl)vinyl]-benzene,

4-Nitro-6-[(Z)-2-(3,4,5-trimethoxyphenyl)vinyl]-2,3-dihydroxybenzene,

2′,3′ dihydroxy-3,5 dichloro-4,4′-dimethoxy-(Z)-stilbene,

2′,3′ dihydroxy-4′-methoxy-3,4,5-trifluoro-(Z)stilbene,

2,3-Dihydroxy-4-methoxy-[(Z)-2-(3,4,5-trimethoxyphenyl) Beta-lactam]-benzene,

2′,3′ diphosphate-3,4,5-trimethoxy-(Z)-stilbene, tetrasodium salt;

3′,4′ diphosphate-3,4,5-trimethoxy-(Z)-stilbene, tetrasodium salt;

and combinations thereof.

Assignments (4)
CHANGE OF NAME Recorded Jul 26, 2016
From: OXIGENE, INC.
To: MATEON THERAPEUTICS, INC.
Reel/Frame 039264/0377 →
CORRECTIVE ASSIGNMENT TO CORRECT THE EXECUTION DATE FOR DAVID CHAPLIN FROM 05/26/2004 TO 03/26/2004 PREVIOUSLY RECORDED ON REEL 015573 FRAME 0353. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jun 22, 2016
From: CHAPLIN, DAVID; EDVARDSEN, KLAUS; PREZIOSO, JOSEPH; WOOD, MARK
To: OXIGENE, INC.
Reel/Frame 039119/0587 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 16, 2004
From: PINNEY, KEVIN
To: BAYLOR UNIVERSITY
Reel/Frame 015572/0753 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 16, 2004
From: CHAPLIN, DAVID; EDVARDSEN, KLAUS; PREZIOSO, JOSEPH; WOOD, MARK
To: OXIGENE, INC.
Reel/Frame 015573/0353 →