IP Library Granted Patent US 7,125,907
Granted Patent B2
US 7,125,907 · App. 10/791,278 · Granted Oct 24, 2006

Thiolactones

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Quick Facts
Patent No.
US 7,125,907
App. No.
10/791,278
Granted
Oct 24, 2006
Kind
B2
Abstract

This invention provides new compounds, pharmaceutical compositions and diagnostic kits comprising such compounds, and methods of using such compounds for inhibiting NAALADase enzyme activity, detecting diseases where NAALADase levels are altered, inhibiting angiogenesis, effecting a TGF-β activity or a neuronal activity, and treating a glutamate abnormality, a compulsive disorder, neuropathy, pain, a prostate disease, cancer, Huntington's disease, diabetes, a retinal disorder or glaucoma.

Claims (38)

1. A compound of formula I,

or a pharmaceutically acceptable equivalent, an optical isomer or a mixture of isomers of the compound, wherein:

X is C 1 –C 4 alkylene, C 2 –C 4 alkenylene, C 2 –C 4 alkynylene, C 3 –C 8 cycloalkylene, C 5 –C 7 cycloalkenylene or Ar, wherein the alkylene, alkenylene, alkynylene, cycloalkylene or cycloalkenylene is unsubstituted or substituted with one or more substituent(s);

L is a bond, —CR 1 R 2 —, —O—, —S—, —SO 2 — or —NR 1 —;

Y is —CR 3 R 4 —;

Z is —(CR 5 R 6 ) n —;

n is 2;

Ar is a bivalent aryl or heteroaryl radical that is unsubstituted or substituted with one or more substituent(s);

R 1 , R 2 , R 3 , R 4 , R 5 and R 6 are independently hydrogen, C 1 –C 4 alkyl or C 2 –C 4 alkenyl, wherein the alkyl or alkenyl is unsubstituted or substituted with one or more substituent(s);

R 7 is hydrogen, phenyl, phenylethyl or benzyl wherein the phenyl, phenylethyl or benzyl is unsubstituted or substituted with one or more substituent(s); and

R 8 , R 9 , R 10 and R 11 are independently hydrogen, carboxy, hydroxy, halo, nitro, cyano, C 1 –C 4 alkyl or C 1 –C 4 alkoxy;

provided that when the compound is of formula I, L is a bond and X is ethyl, then Y is not —CR 3 R 4 —.

2. The compound of claim 1 , wherein:

Y is —CR 3 R 4 —; and

n is 2.

3. The compound of claim 2 , wherein:

L is —CR 1 R 2 —, —O—, —S— or NH;

X is C 1 –C 2 alkylene or Ar; and

Ar is phenylene, biphenylene, benzylene or naphthylene, wherein the phenylene, biphenylene, benzylene or naphthylene is unsubstituted or substituted with one or more substituent(s) independently selected from carboxy, halo, nitro, C 1 –C 4 alkyl, C 1 –C 4 alkoxy, phenyl, phenoxy and benzyloxy.

4. The compound of claim 1 , which is 3-[(2-oxotetrahydro-2H-thiopyran-3-yl)methyl]benzoic acid or a pharmaceutically acceptable equivalent, an optical isomer or a mixture of isomers thereof.

5. A method of treating peripheral neuropathy, comprising administering to a mammal in need of such inhibition, treatment, an effective amount of a compound of formula I of claim 1 .

6. A pharmaceutical composition comprising:

(i) an effective amount of a compound of formula I,

or a pharmaceutically acceptable equivalent, an optical isomer or a mixture of isomers of the compound, wherein:

X is C 1 –C 4 alkylene, C 2 –C 4 alkenylene, C 2 –C 4 alkynylene, C 3 –C 8 cycloalkylene, C 5 –C 7 cycloalkenylene or Ar, wherein the alkylene, alkenylene, alkynylene, cycloalkylene or cycloalkenylene is unsubstituted or substituted with one or more substituent(s);

L is a bond, —CR 1 R 2 —, —O—, —S—, —SO 2 — or —NR 1 —;

Y is —CR 3 R 4 ;

Z is —(CR 5 R 6 ) n —;

n is 2;

Ar is a bivalent aryl or heteroaryl radical that is unsubstituted or substituted with one or more substituent(s);

R 1 , R 2 , R 3 , R 4 , R 5 and R 6 are independently hydrogen, C 1 –C 4 alkyl or C 2 –C 4 alkenyl, wherein the alkyl or alkenyl is unsubstituted or substituted with one or more substituent(s);

R 7 is hydrogen, phenyl, phenylethyl or benzyl wherein the phenyl, phenylethyl or benzyl is unsubstituted or substituted with one or more substituent(s); and

R 8 , R 9 , R 10 and R 11 are independently hydrogen, carboxy, hydroxy, halo, nitro, cyano, C 1 –C 4 alkyl or C 1 –C 4 alkoxy; and

(ii) a pharmaceutically acceptable carrier.

7. A compound which is 3-(2-oxo-tetrahydrothiopyran-3-yl)-propionic acid or a pharmaceutically acceptable equivalent, an optical isomer or a mixture of isomers thereof.

8. A pharmaceutical composition comprising:

(i) an effective amount of the compound of claim 7 ; and

(ii) a pharmaceutically acceptable carrier.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 24, 2009
From: EISAI CORPORATION OF NORTH AMERICA
To: EISAI INC.
Reel/Frame 023699/0188 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 19, 2009
From: MGI GP, INC.
To: EISAI CORPORATION OF NORTH AMERICA
Reel/Frame 022277/0779 →
CERTIFICATE OF MERGER OF GRANITE ACQUISITION, INC. WITH AND INTO GUILFORD PHARMACEUTICALS INC. Recorded Dec 23, 2008
From: GRANITE ACQUISITION, INC.; GUILFORD PHARMACEUTICALS INC.
To: MGI GP, INC.
Reel/Frame 022024/0105 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 19, 2004
From: SLUSHER, BARBARA S.; TSUKAMOTO, TAKASHI
To: GUILFORD PHARMACEUTICALS INC.
Reel/Frame 015578/0883 →