IP Library Granted Patent US 6,957,623
Granted Patent B2
US 6,957,623 · App. 10/796,445 · Granted Oct 25, 2005

Critical temperature indicator

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Quick Facts
Patent No.
US 6,957,623
App. No.
10/796,445
Granted
Oct 25, 2005
Kind
B2
Abstract

A critical temperature indicator according to the present invention produces a visual, irreversible indication that the indicator has been subjected to a selected critical temperature. The critical temperature indicator includes a transparent housing, and a temperature sensitive transformable material operably contained within the transparent housing which includes mixture of water, nucleating agent (preferably ice nucleating active (INA) microorganisms), latex, and stabilizer which is translucent prior to exposure of a predetermined temperature and is transformed upon being subjected to the predetermined temperature to render a substantially consistent opaque material thus precluding visibility therethrough and thereby providing a sure visual sign that the indicator has been subjected to the predetermined temperature.

Claims (38)

1. A critical temperature indicator which provides an irreversible visual indication that the indicator has been exposed to a predetermined critical temperature, which includes:

a transparent housing; and

a temperature sensitive transformable material operably contained within said transparent housing which includes mixture of water, latex, and ice nucleating active (INA) microorganism which is translucent prior to exposure of a predetermined temperature and is transformed upon being subjected to said predetermined temperature to render a substantially consistent opaque material thus precluding visibility therethrough and thereby providing a sure visual sign that said indicator has been subjected to said predetermined temperature.

2. The critical temperature indicator of claim 1 , wherein said latex includes particles having a diameter of less than about 0.05 microns.

3. The critical temperature indicator of claim 1 , wherein said latex is present in said material in an amount of from about 5 to 35 weight percent.

4. The critical temperature indicator of claim 1 , wherein said INA microorganism is present in said material in an amount of from about 0.01 to 1.0 weight percent.

5. The critical temperature indicator of claim 1 , wherein said INA microorganism includes ice nucleating active (NA) microorganisms which contain a molecular structure to attract said water and which upon reaching said predetermined temperature interacts with said latex to form said opaque material.

6. The critical temperature indicator of claim 1 , wherein said latex includes one of acrylic, nitrite, polychloroprene, paraffin, polyethylene, waxes, styrene-butadiene, vinyl pyridine based, styrene polymers, styrene/butadiene copolymers, styrene/acrylic acid copolymers, vinyltoluene/tertiarybutyl styrene copolymers, vinylidene chloride/vinyl chloride copolymers or mixtures thereof.

7. The critical temperature indicator of claim 1 , which further includes a colored substrate operably disposed with respect to said housing such that said colored substrate can be seen through said housing while said material is substantially transparent and is substantially invisible when said material is opaque.

8. The critical temperature indicator of claim 7 , wherein said colored substrate forms part of backing to which said housing is sealably connected.

9. The critical temperature indicator of claim 7 , wherein said backing has an exposed surface having a self adhesive material applied thereto.

10. The critical temperature indicator of claim 7 , wherein said substrate is a colored strip contained within said housing.

11. The critical temperature indicator of claim 1 , which further includes a stabilizer for said INA microorganism.

12. A critical temperature indicator which provides an irreversible visual indication that the indicator has been exposed to a predetermined critical temperature, which includes:

a transparent housing; and

a temperature sensitive transformable material operably contained within said transparent housing which includes mixture of water, latex, and ice nucleating active (INA) microorganism which is translucent prior to exposure of a predetermined temperature and is transformed upon being subjected to said predetermined temperature to render a substantially consistent opaque material thus precluding visibility therethrough and thereby providing a sure visual sign that said indicator has been subjected to said predetermined temperature, wherein said INA microorganism includes INA microorganisms which contain a molecular structure to attract said water and which upon reaching said predetermined temperature interacts with said latex to form said opaque material.

13. The critical temperature indicator of claim 12 , wherein said latex includes particle size having a diameter of less than about 0.05 microns.

14. The critical temperature indicator of claim 12 , wherein said latex is present in said material in an amount of from about 5 to 35 weight percent.

15. The critical temperature indicator of claim 12 , wherein said INA microorganism is present in said material in an amount of from about 0.01 to 1.0 weight percent.

16. The critical temperature indicator of claim 12 , wherein said latex includes one of acrylic, natural, nitrile, polychloroprene, paraffin, polyethylene, waxes, styrene-butadiene, vinyl pyridine based, styrene polymers, styrene/butadiene copolymers, styrene/acrylic acid copolymers, vinyltoluene/tertiarybutyl styrene copolymers, vinylidene chloride/vinyl chloride copolymers or mixtures thereof.

17. The critical temperature indicator of claim 12 , which further includes a colored substrate operably disposed with respect to said housing such that said colored substrate can be seen through said housing while said material is in said transparent state and is substantially invisible when said material is opaque.

18. The critical temperature indicator of claim 17 , wherein said colored substrate forms part of backing to which said housing is sealably connected.

19. The critical temperature indicator of claim 17 , wherein said backing has an exposed surface having a self adhesive material applied thereto.

20. The critical temperature indicator of claim 17 , wherein said substrate is a colored strip contained within said housing.

21. The critical temperature indicator of claim 12 , which further includes a stabilizer for said INA microorganism.

22. A critical temperature indicator which provides an irreversible visual indication that the indicator has been exposed to a predetermined critical temperature, which includes:

a transparent housing;

a temperature sensitive transformable material operably contained within said transparent housing which includes mixture of water, latex, and ice nucleating active (INA) microorganism which is translucent prior to exposure of a predetermined temperature and is transformed upon being subjected to said predetermined temperature to render a substantially consistent opaque material thus precluding visibility therethrough and thereby providing a sure visual sign that said indicator has been subjected to said predetermined temperature; and

a colored substrate operably disposed with respect to said housing such that said colored substrate can be seen through said housing while said material is in said transparent state and is substantially invisible when said material is opaque.

23. The critical temperature indicator of claim 22 , wherein said latex includes particle size having a diameter of less than about 0.05 microns.

24. The critical temperature indicator of claim 22 , wherein said latex is present in said material in an amount of from about 5 to 35 weight percent.

25. The critical temperature indicator of claim 22 , wherein said INA microorganism is present in said material in an amount of from about 0.01 to 1.0 weight percent.

26. The critical temperature indicator of claim 22 , wherein said INA microorganism includes INA microorganisms which contain a molecular structure to attract said water and which upon reaching said predetermined temperature interacts with said latex to form said opaque material.

27. The critical temperature indicator of claim 22 , wherein said latex includes one of acrylic, natural, nitrile, polychloroprene, paraffin, polyethylene, waxes, styrene-butadiene, vinyl pyridine based, styrene polymers, styrene/butadiene copolymers, styrene/acrylic acid copolymers, vinyltoluene/tertiarybutyl styrene copolymers, vinylidene chloride/vinyl chloride copolymers or mixtures thereof.

28. The critical temperature indicator of claim 22 , wherein said colored substrate forms part of backing to which said housing is sealably connected.

29. The critical temperature indicator of claim 22 , wherein said backing has an exposed surface having a self adhesive material applied thereto.

30. The critical temperature indicator of claim 22 , wherein said substrate is a colored strip contained within said housing.

31. The critical temperature indicator of claim 22 , which further includes a stabilizer for said INA microorganism.

Assignments (6)
RELEASE OF SECURITY INTEREST - 364 - DAY Recorded Mar 5, 2021
From: JPMORGAN CHASE BANK, N.A.
To: ZEBRA TECHNOLOGIES CORPORATION; LASER BAND, LLC; TEMPTIME CORPORATION
Reel/Frame 056036/0590 →
SECURITY INTEREST Recorded Sep 1, 2020
From: ZEBRA TECHNOLOGIES CORPORATION; LASER BAND, LLC; TEMPTIME CORPORATION
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 053841/0212 →
SECURITY INTEREST Recorded Apr 25, 2019
From: TEMPTIME CORPORATION
To: JPMORGAN CHASE BANK, N.A, AS COLLATERAL AGENT
Reel/Frame 048995/0241 →
RELEASE OF SECURITY INTEREST Recorded Feb 28, 2019
From: ARES CAPITAL CORPORATION, AS COLLATERAL AGENT
To: TEMPTIME CORPORATION
Reel/Frame 048462/0163 →
SECURITY AGREEMENT Recorded Sep 13, 2013
From: TEMPTIME CORPORATION
To: ARES CAPITAL CORPORATION, AS COLLATERAL AGENT
Reel/Frame 031265/0599 →
NOTICE OF SECURED INSTRUMENT Recorded Dec 15, 2009
From: KLT TECHNOLOGY INC
To: TEMPTIME CORPORATION
Reel/Frame 023649/0837 →