IP Library Granted Patent US 6,843,282
Granted Patent B2
US 6,843,282 · App. 10/802,244 · Granted Jan 18, 2005

Densification of aerated powders using positive pressure

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Quick Facts
Patent No.
US 6,843,282
App. No.
10/802,244
Granted
Jan 18, 2005
Kind
B2
Abstract

A process for increasing the bulk density of an aerated powder is provided. The powder is placed in a container. The container is then closed and the gas pressure within the container is increased to a level above atmospheric pressure and at a rate sufficient to cause the powder to compact before a substantial portion of said pressurization gas diffuses into said powder. In one embodiment, the process is utilized to increase the bulk density of an aerated, free-flowing titanium dioxide pigment. Apparatus for carrying out the process is also provided.

Claims (12)

1. A process for preparing a slurry, comprising:

processing a powder, in a fluid energy mill;

prior to allowing said powder to fully settle, increasing the bulk density of said powder by deaerating said powder by placing said powder in a container; and injecting a pressurization gas into the area of said container containing said powder such that the gas pressure in the area of said container is increased to a level above atmospheric pressure at a rate sufficient to cause said powder to compact before a substantial portion of said pressurization gas diffuses into said powder;

removing said compacted powder from said container, and

dispersing said densified powder into a liquid medium.

2. The process of claim 1 wherein said powder is titanium dioxide pigment, and said liquid medium is water.

3. A process for preparing a concentrated titanium dioxide pigment slurry, comprising:

milling a titanium dioxide pigment;

prior to allowing said titanium dioxide pigment to fully settle, increasing the bulk density of said pigment by:

placing said pigment in a container; and

injecting a pressurization gas into the area of said container containing said pigment such that the gas pressure is increased to a level above atmospheric pressure at a rate sufficient to cause said pigment to compact before a substantial portion of said pressurization gas diffuses into said pigment; and

removing said compacted titanium dioxide pigment from said container; and dispersing said deaerated pigment in a liquid medium.

Assignments (12)
ASSIGNMENT OF SECURITY INTEREST IN PATENT COLLATERAL RECORDED AT REEL/FRAME 044100/0339 Recorded Mar 12, 2021
From: BANK OF AMERICA, N.A.
To: HSBC BANK USA, NATIONAL ASSOCIATION, AS THE SUCCESSOR ADMINISTRATIVE AGENT AND COLLATERAL AGENT
Reel/Frame 055578/0880 →
PATENT SECURITY AGREEMENT Recorded Oct 2, 2017
From: TRONOX LLC
To: BANK OF AMERICA, N.A., AS COLLATERAL AGENT
Reel/Frame 044100/0339 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY COLLATERAL AT REEL/FRAME NOS. 027682/0086 AND 030047/0422 Recorded Sep 26, 2017
From: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
To: TRONOX LLC
Reel/Frame 044018/0893 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Sep 25, 2017
From: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
To: TRONOX LLC; TRONOX WORLDWIDE LLC
Reel/Frame 043993/0306 →
PATENT SECURITY AGREEMENT Recorded Jul 18, 2012
From: TRONOX LLC; TRONOX WORLDWIDE LLC
To: UBS AG, STAMFORD BRANCH
Reel/Frame 028582/0669 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 12, 2012
From: WELLS FARGO CAPITAL FINANCE, LLC
To: TRONOX LLC; TRONOX WORLDWIDE LLC
Reel/Frame 028535/0362 →
RELEASE OF SECURITY INTEREST Recorded Feb 9, 2012
From: GOLDMAN SACHS LENDING PARTNERS LLC
To: TRONOX LLC
Reel/Frame 027682/0064 →
SECURITY AGREEMENT Recorded Feb 9, 2012
From: TRONOX LLC
To: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
Reel/Frame 027682/0086 →
BANKRUPTCY COURT NOTICE CONFIRMING RELEASE OF LIENS EFFECTIVE 2/14/2011 Recorded Mar 24, 2011
From: LEHMAN COMMERCIAL PAPER, INC.
To: TRONOX LLC
Reel/Frame 026010/0684 →
SECURITY AGREEMENT Recorded Feb 15, 2011
From: TRONOX LLC
To: GOLDMAN SACHS LENDING PARTNERS LLC, AS COLLATERAL AGENT
Reel/Frame 025795/0130 →
SECURITY AGREEMENT Recorded Aug 21, 2008
From: TRONOX LLC F/K/A KERR-MCGEE CHEMICAL LLC
To: LEHMAN COMMERCIAL PAPER INC.
Reel/Frame 021411/0792 →
CHANGE OF NAME Recorded Aug 15, 2008
From: KERR-MCGEE CHEMICAL LLC
To: TRONOX LLC
Reel/Frame 021411/0498 →