Densification of aerated powders using positive pressure
View Patent ↗A process for increasing the bulk density of an aerated powder is provided. The powder is placed in a container. The container is then closed and the gas pressure within the container is increased to a level above atmospheric pressure and at a rate sufficient to cause the powder to compact before a substantial portion of said pressurization gas diffuses into said powder. In one embodiment, the process is utilized to increase the bulk density of an aerated, free-flowing titanium dioxide pigment. Apparatus for carrying out the process is also provided.
1. A process for preparing a slurry, comprising:
processing a powder, in a fluid energy mill;
prior to allowing said powder to fully settle, increasing the bulk density of said powder by deaerating said powder by placing said powder in a container; and injecting a pressurization gas into the area of said container containing said powder such that the gas pressure in the area of said container is increased to a level above atmospheric pressure at a rate sufficient to cause said powder to compact before a substantial portion of said pressurization gas diffuses into said powder;
removing said compacted powder from said container, and
dispersing said densified powder into a liquid medium.
2. The process of claim 1 wherein said powder is titanium dioxide pigment, and said liquid medium is water.
3. A process for preparing a concentrated titanium dioxide pigment slurry, comprising:
milling a titanium dioxide pigment;
prior to allowing said titanium dioxide pigment to fully settle, increasing the bulk density of said pigment by:
placing said pigment in a container; and
injecting a pressurization gas into the area of said container containing said pigment such that the gas pressure is increased to a level above atmospheric pressure at a rate sufficient to cause said pigment to compact before a substantial portion of said pressurization gas diffuses into said pigment; and
removing said compacted titanium dioxide pigment from said container; and dispersing said deaerated pigment in a liquid medium.