IP Library Granted Patent US 7,160,845
Granted Patent B2
US 7,160,845 · App. 10/815,579 · Granted Jan 9, 2007

Dithiocarbamate derivatives useful as lubricant and fuel additives

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Quick Facts
Patent No.
US 7,160,845
App. No.
10/815,579
Granted
Jan 9, 2007
Kind
B2
Abstract

Dithiocarbamate derivative compounds, useful as multifunctional additives for lubricating oils and fuels, are provided and are derived from a reaction product obtained from (a) a di(hydrocarbyl)thiocarbamate intermediate derived from the reaction of a dihydrocarbylamine and carbon disulfide; (b) an amide of the general formula R 7 CONH 2 wherein R 7 is an alkylene group having 2 to about 30 carbon atoms; and (c) an effective amount of a carbonyl-containing compound.

Claims (43)

1. A dithiocarbamate derivative compound of the general formula:

wherein R 1 , R 2 , R 5 and R 6 are each independently C 1 –C 30 n-alkyl, C 3 –C 30 branched alkyl, C 3 –C 12 cycloalkyl, C 5 –C 12 aryl, or C 6 –C 12 alkylaryl; R 3 are each independently C 2 –C 20 alkylene and R 4 is C 1 –C 20 alkylene substituted with a compound selected from the group consisting of

2. The dithiocarbamate derivative compound of claim 1 , wherein R 1 , R 2 , R 5 and R 6 are each independently a straight-chained, branched or cyclic alkyl group of from about 2 to about 30 carbon atoms; R 3 is a divalent alkylene group of from about 2 to about 12 carbon atoms; and the alkylene group of R 4 is a divalent alkylene group of from 1 to about 12 carbon atoms.

3. The dithiocarbamate derivative compound of claim 1 , wherein R 1 , R 2 , R 5 and R 6 are each independently a straight-chained, branched or cyclic alkyl group of from about 4 to about 24 carbon atoms; R 3 is a divalent alkylene group of from 2 to about 6 carbon atoms; and the alkylene group of R 4 is a divalent alkylene group of from 1 to about 6 carbon atoms.

4. The dithiocarbamate derivative compound of claim 2 , wherein the alkylene group of R 4 is substituted with

5. The dithiocarbamate derivative compound of claim 3 , wherein the alkylene group of R 4 is substituted with

6. The dithiocarbamate derivative compound of claim 2 , wherein the alkylene group of R 4 is substituted with

7. The dithiocarbamate derivative compound of claim 3 , wherein the alkylene group of R 4 is substituted with

8. The dithiocarbamate derivative compound of claim 2 , wherein the alkylene group of R 4 is substituted with

9. The dithiocarbamate derivative compound of claim 3 , wherein the alkylene group of R 4 is substituted with

10. A lubricating oil composition comprising (a) an oil of lubricating viscosity and (b) a functional property-improving effective amount of at least one dithiocarbamate derivative compound of claim 1 .

11. A lubricating oil composition comprising (a) an oil of lubricating viscosity and (b) an antiwear-improving effective amount of at least one dithiocarbamate derivative compound of claim 1 .

12. A lubricating oil composition comprising (a) an oil of lubricating viscosity and (b) a friction reducing effective amount of at least one dithiocarbamate derivative compound of claim 1 .

13. A lubricating oil composition comprising (a) an oil of lubricating viscosity and (b) an antioxidant-improving effective amount of at least one dithiocarbamate derivative compound of claim 1 .

14. A method for improving at least one functional property of a lubricating oil which comprises adding to the lubricating oil a functional property-improving effective amount of at least one dithiocarbamate derivative compound of claim 1 .

15. A method for improving the anti-wear property of a lubricating oil which comprises adding to the lubricating oil an anti-wear-improving effective amount of at least one dithiocarbamate derivative compound of claim 1 .

16. A method for improving the friction reducing property of a lubricating oil which comprises adding to the lubricating oil a friction reducing effective amount of at least one dithiocarbamate derivative compound of claim 1 .

17. A method for improving the antioxidant property of a lubricating oil which comprises adding to the lubricating oil an antioxidant-improving effective amount of at least one dithiocarbamate derivative compound of claim 1 .

18. A reaction product obtained from (a) a di(hydrocarbyl)thiocarbamate intermediate derived from the reaction of a dihydrocarbylamine and carbon disulfide; (b) an amide of the general formula R 7 CONH 2 wherein R 7 is an alkylene group having 2 to about 30 carbon atoms; and (c) an effective amount of a carbonyl-containing compound.

19. The reaction product of claim 18 wherein the amide is acrylamide and the carbonyl-containing compound is a dialdehyde.

20. The reaction product of claim 19 wherein the dialdehyde is selected from the group consisting of glyoxal and glutaraldehyde.

21. The reaction product of claim 18 wherein the amide is acrylamide and the carbonyl-containing compound is glyoxal.

22. The reaction product of claim 18 wherein the dihydrocarbylamine is a dialkylamine in which each alkyl group contains from about 2 to about 30 carbon atoms.

23. A lubricating oil compositions comprising (a) an oil of lubricating viscosity and (b) a functional property-improving effective amount of the reaction product of claim 18 .

24. A lubricating oil compositions comprising (a) an oil of lubricating viscosity and (b) a functional property-improving effective amount of the reaction product of claim 19 .

25. A lubricating oil compositions comprising (a) an oil of lubricating viscosity and (b) a functional property-improving effective amount of the reaction product of claim 21 .

26. A lubricating oil composition comprising (a) an oil of lubricating viscosity and (b) an antiwear-improving effective amount of the reaction product claim 18 .

27. A lubricating oil composition comprising (a) an oil of lubricating viscosity and (b) a friction reducing effective amount of the reaction product claim 18 .

28. A lubricating oil composition comprising (a) an oil of lubricating viscosity and (b) an antioxidant-improving effective amount of the reaction product claim 18 .

29. A method for improving at least one functional property of a lubricating oil which comprises adding to the lubricating oil a functional property-improving amount of the reaction product claim 18 .

30. A method for improving the anti-wear property of a lubricating oil which comprises adding to the lubricating oil an anti-wear-improving amount of the reaction product claim 18 .

31. A method for improving the friction reducing property of a lubricating oil which comprises adding to the lubricating oil a friction reducing amount of the reaction product claim 18 .

32. A method for improving the antioxidant property of a lubricating oil which comprises adding to the lubricating oil an antioxidant-improving amount of the reaction product claim 18 .

33. A fuel composition comprising a major amount of a hydrocarbon fuel and a minor effective amount of the dithiocarbamate derivative compound of claim 1 .

34. A fuel composition comprising a major amount of a hydrocarbon fuel and a minor effective amount of the dithiocarbamate derivative compound of claim 3 .

35. A fuel composition comprising a major amount of a hydrocarbon fuel and a minor effective amount of the reaction product of claim 18 .

36. A fuel composition comprising a major amount of a hydrocarbon fuel and a minor effective amount of the reaction product of claim 19 .

37. A fuel composition comprising a major amount of a hydrocarbon fuel and a minor effective amount of the reaction product of claim 21 .

38. The fuel composition of claim 33 wherein the hydrocarbon fuel is gasoline or diesel fuel.

39. The fuel composition of claim 34 wherein the hydrocarbon fuel is gasoline or diesel fuel.

40. The fuel composition of claim 35 wherein the hydrocarbon fuel is gasoline or diesel fuel.

41. The fuel composition of claim 36 wherein the hydrocarbon fuel is gasoline or diesel fuel.

42. The fuel composition of claim 37 wherein the hydrocarbon fuel is gasoline or diesel fuel.

Assignments (11)
CHANGE OF NAME Recorded Sep 25, 2018
From: CROMPTON CORPORATION
To: CHEMTURA CORPORATION
Reel/Frame 047141/0152 →
RELEASE OF FIRST LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded May 11, 2017
From: BANK OF AMERICA, N.A.
To: CHEMTURA CORPORATION; BIOLAB FRANCHISE COMPANY, LLC; BIO-LAB, INC.; CROMPTON COLORS INCORPORATED; CROMPTON HOLDING CORPORATION; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; LAUREL INDUSTRIES HOLDINGS, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC
Reel/Frame 042447/0508 →
RELEASE OF SECOND LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded May 11, 2017
From: BANK OF AMERICA, N.A.
To: CHEMTURA CORPORATION; BIOLAB FRANCHISE COMPANY, LLC; BIO-LAB, INC.; CROMPTON COLORS INCORPORATED; CROMPTON HOLDING CORPORATION; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; LAUREL INDUSTRIES HOLDINGS, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC
Reel/Frame 042449/0001 →
SECDOND LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 21, 2011
From: CHEMTURA CORPORATION; BIOLAB FRANCHISE COMPANY, LLC; BIO-LAB, INC.; CROMPTON COLORS INCORORATED; CROMPTON HOLDING CORPORATION; CLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; HAOMECARE LABS, INC.; LAUREL INDUSTRIES HOLDINGS, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC
To: BANK OF AMERICA, N. A.
Reel/Frame 027881/0347 →
FIRST LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT. Recorded Mar 21, 2011
From: CHEMTURA CORPORATION; BIOLAB FRANCHISE COMPANY, LLC; BIO-LAB, INC.; CROMPTON COLORS INCORPORATED; CROMPTON HOLDING CORPORATION; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; LAUREL INDUSTRIES HOLDINGS, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC
To: BANK OF AMERICA, N.A.
Reel/Frame 026028/0622 →
INTELLECTUAL PROPERTY SECURITY RELEASE AGREEMENT Recorded Mar 21, 2011
From: CITIBANK, N.A.
To: CHEMTURA CORPORATION; A & M CLEANING PRODUCTS, LLC; ASCK, INC; BIOLAB COMPANY STORE, LLC; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIOLAB TEXTILES ADDITIVES, LLC; BIOLAB, INC.; CROMPTON COLORS INCORPORATED; CROMPTON MONOCHEM, INC.; CNK CHEMICAL REALTY CORPORATION; CROMPTON HOLDING CORPORATION; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GT SEED TREATMENT, INC.; ISCI, INC; GREAT LAKES CHEMICAL GLOBAL, INC.; HOMECARE LABS, INC.; KEM MANUFACTURING CORPORATION; LAUREL INDUSTRIES HOLDINGS, INC.; NAUGATUCK TREATMENT COMPANY; UNIROYAL CHEMICAL COMPANY LIMITED (DELAWARE); MONOCHEM, INC.; RECREATIONAL WATER PRODUCTS, INC.; WEBER CITY ROAD LLC; WRL OF INDIANA, INC.; BIOLAB FRANCHISE COMPANY, LLC
Reel/Frame 026039/0142 →
AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Feb 22, 2010
From: CHEMTURA CORPORATION; A & M CLEANING PRODUCTS, LLC; AQUA CLEAR INDUSTRIES, LLC; ASCK, INC.; ASEPSIS, INC.; BIOLAB COMPANY STORE, LLC; BIOLAB FRANCHISE COMPANY, LLC; BIOLAB TEXTILE ADDITIVES, LLC; BIO-LAB, INC.; CNK CHEMICAL REALTY CORPORATION; CROMPTON COLORS INCORPORATED; CROMPTON HOLDING CORPORATION; CROMPTON MONOCHEM, INC.; GLCC LAUREL, LLC; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; ISCI, INC.; KEM MANUFACTURING CORPORATION; LAUREL INDUSTRIES HOLDINGS, INC.; MONOCHEM, INC.; NAUGATUCK TREATMENT COMPANY; RECREATIONAL WATER PRODUCTS, INC.; UNIROYAL CHEMICAL COMPANY LIMITED (DELAWARE); WEBER CITY ROAD LLC; WRL OF INDIANA, INC.
To: CITIBANK, N.A.
Reel/Frame 023998/0001 →
SECURITY AGREEMENT Recorded May 12, 2009
From: CHEMTURA CORPORATION; A & M CLEANING PRODUCTS, LLC; AQUA CLEAR INDUSTRIES, LLC; ASCK, INC.; ASEPSIS, INC.; BIOLAB TEXTILE ADDITIVES, LLC; BIO-LAB, INC.; CNK CHEMICAL REALTY CORPORATION; CROMPTON HOLDING CORPORATION; CROMPTON COLORS INCORPORATED; CROMPTON MONOCHEM, INC.; GREAT LAKES CHEMICAL CORPORATION; GREAT LAKES CHEMICAL GLOBAL, INC.; GT SEED TREATMENT, INC.; HOMECARE LABS, INC.; ISCI, INC.; KEM MANUFACTURING CORPORATION; LAUREL INDUSTRIES HOLDINGS, INC.; MONOCHEM, INC.; NAUGATUCK TREATMENT COMPANY; RECREATIONAL WATER PRODUCTS, INC.; UNIROYAL CHEMICAL COMPANY LIMITED (DELAWARE); WEBER CITY ROAD LLC; WRL OF INDIANA, INC.; BIOLAB COMPANY STORE, LLC; BIOLAB FRANCHISE COMPANY, LLC; GLCC LAUREL, LLC
To: CITIBANK, N.A.
Reel/Frame 022668/0658 →
RELEASE OF LIEN IN PATENTS Recorded Jul 13, 2005
From: DEUTSCHE BANK AG, NEW YORK BRANCH
To: CROMPTON CORPORATION
Reel/Frame 016513/0745 →
SECURITY AGREEMENT Recorded Nov 10, 2004
From: CROMPTON CORPORATION
To: DEUTSCHE BANK AG NEW YORK BRANCH
Reel/Frame 015370/0467 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 31, 2004
From: BARANSKI, JOHN R.; NALESNIK, THEODORE E.
To: CROMPTON CORPORATION
Reel/Frame 015179/0800 →