IP Library Granted Patent US 7,429,313
Granted Patent B2
US 7,429,313 · App. 10/834,684 · Granted Sep 30, 2008

Method of producing electrostatically charged gelatin

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Quick Facts
Patent No.
US 7,429,313
App. No.
10/834,684
Granted
Sep 30, 2008
Kind
B2
Abstract

Methods of forming electrostatically charged gelatin are provided. Gelatin is extracted by an acid extraction method ( 12 ) thereby producing a gelatin dispersion ( 14 ), the pH of which is adjusted to the isoelectric point of the gelatin. The pH of the gelatin dispersion ( 14 ) is then further adjusted ( 22 ) so as to cause the gelatin to assume an electrostatic charge.

Claims (35)

1. A method of forming electrostatically charged gelatin comprising the steps of:

(a) providing a collagen-containing raw material;

(b) forming an aqueous slurry with said raw material;

(c) forming a gelatin dispersion by extracting gelatin from said slurry at a pH of from about 2-3;

(d) performing a first pH adjustment to adjust the pH of said gelatin dispersion to the isoelectric point of said gelatin;

(e) removing non-gelatin impurities from said gelatin dispersion formed in step (d); and

(f) performing a second pH adjustment to adjust the pH of said gelatin dispersion from step (e) causing said gelatin to assume an electrostatic charge.

2. The method of claim 1 , said second pH adjustment step comprising adjusting the pH of said gelatin dispersion thereby causing said gelatin to assume a negative electrostatic charge.

3. The method of claim 2 , said second pH adjustment step comprising adjusting the pH of said gelatin dispersion to between about 10-12.

4. The method of claim 1 , said second pH adjustment step comprising adjusting the pH of said gelatin dispersion thereby causing said gelatin to assume a positive electrostatic charge.

5. The method of claim 4 , said second pH adjustment step comprising adjusting the pH of said gelatin dispersion to between about 2-3.

6. The method of claim 1 , the isoelectric point of said gelatin being from about 4.5-5.5.

7. The method of claim 1 , further comprising the step of passing a DC electric current through said gelatin dispersion formed in step (f).

8. The method of claim 1 , further comprising the step of removing moisture from said gelatin dispersion formed in step (f) thereby forming a gelatin concentrate.

9. The method of claim 8 , further comprising the step of sterilizing said gelatin concentrate.

10. The method of claim 1 , further comprising the step of spray drying said gelatin dispersion formed in step (f).

11. The method of claim 1 , said impurities removal step comprising filtering said gelatin dispersion.

12. The method of claim 11 , said filtering step comprising a first filtration to remove insoluble materials from said gelatin dispersion, and a second filtration to remove non-gelatin proteins from said gelatin dispersion.

13. A method of forming electrostatically charged gelatin comprising the steps of:

(a) providing a collagen-containing raw material;

(b) forming an aqueous slurry with said raw material;

(c) forming a gelatin dispersion by extracting gelatin from said slurry;

(d) performing a first pH adjustment to adjust the pH of said gelatin dispersion to the isoelectric point of said gelatin;

(e) performing a second pH adjustment to adjust the pH of said gelatin dispersion from step (d) causing said gelatin to assume an electrostatic charge; and

(f) applying a DC electric current to said gelatin dispersion from step (e).

14. The method of claim 13 , said second pH adjustment step comprising adjusting the pH of said gelatin dispersion thereby causing said gelatin to assume a negative electrostatic charge.

15. The method of claim 14 , said second pH adjustment step comprising adjusting the pH of said gelatin dispersion to between about 10-12.

16. The method of claim 13 , said second pH adjustment step comprising adjusting the pH of said gelatin dispersion thereby causing said gelatin to assume a positive electrostatic charge.

17. The method of claim 16 , said second pH adjustment step comprising adjusting the pH of said gelatin dispersion to between about 2-3.

18. The method of claim 13 , the isoelectric point of said gelatin being from about 4.5-5.5.

19. The method of claim 13 , step (f) comprising applying a positive DC electric current to said gelatin dispersion.

20. The method of claim 13 , step (f) comprising applying a negative DC electric current to said gelatin dispersion.

21. The method of claim 13 , further comprising the step of removing moisture from said gelatin dispersion formed in step (f) thereby forming a gelatin concentrate.

22. The method of claim 21 , further comprising the step of sterilizing said gelatin concentrate.

23. The method of claim 13 , further comprising the step of spray drying said gelatin dispersion formed in step (f).

Assignments (20)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 25, 2016
From: BIG HEART PET BRANDS, LLC
To: BIG HEART PET, INC.
Reel/Frame 038810/0086 →
CHANGE OF NAME Recorded May 13, 2016
From: BIG HEART PET BRANDS
To: BIG HEART PET BRANDS, LLC
Reel/Frame 038687/0149 →
RELEASE OF SECURITY INTEREST Recorded Mar 23, 2015
From: JPMORGAN CHASE BANK, N.A.
To: BIG HEART PET BRANDS
Reel/Frame 035231/0235 →
RELEASE OF SECURITY INTEREST Recorded Mar 23, 2015
From: JPMORGAN CHASE BANK, N.A.
To: BIG HEART PET BRANDS (F/K/A DEL MONTE CORPORATION)
Reel/Frame 035231/0696 →
CORRECTIVE ASSIGNMENT TO CORRECT THE REMOVE INCORRECT PATENT NO. 6648163 FROM CHANGE OF NAME PREVIOUSLY RECORDED ON REEL 032472 FRAME 0782. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF NAME FROM DEL MONTE CORPORATION TO BIG HEART PET BRANDS. Recorded Oct 3, 2014
From: DEL MONTE CORPORATION
To: BIG HEART PET BRANDS
Reel/Frame 033888/0631 →
SECURITY INTEREST Recorded Mar 31, 2014
From: BIG HEART PET BRANDS
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 032565/0323 →
CORRECTIVE ASSIGNMENT TO CORRECT THE REMOVE INCORRECT PATENT NOS. 6254920 AND 6350485 FROM CHANGE OF NAME PREVIOUSLY RECORDED ON REEL 032472 FRAME 0782. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF NAME FROM DEL MONTE CORPORATION TO BIG HEART PET BRANDS. Recorded Mar 21, 2014
From: DEL MONTE CORPORATION
To: BIG HEART PET BRANDS
Reel/Frame 032561/0003 →
CHANGE OF NAME Recorded Mar 19, 2014
From: DEL MONTE CORPORATION
To: BIG HEART PET BRANDS
Reel/Frame 032472/0782 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENT RIGHTS Recorded Mar 19, 2014
From: BANK OF AMERICA, N.A.
To: BIG HEART PET BRANDS F/K/A DEL MONTE CORPORATION
Reel/Frame 032479/0915 →
SECURITY AGREEMENT Recorded Apr 8, 2011
From: DEL MONTE CORPORATION
To: JPMORGAN CHASE BANK, NA, AS COLLATERAL AGENT
Reel/Frame 026100/0771 →
SECURITY AGREEMENT Recorded Mar 28, 2011
From: DEL MONTE CORPORATION
To: BANK OF AMERICA, N.A.
Reel/Frame 026029/0157 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENT RIGHTS Recorded Mar 17, 2011
From: BANK OF AMERICA, N.A.
To: DEL MONTE FOODS COMPANY; DEL MONTE CORPORATION
Reel/Frame 025969/0967 →
SECURITY AGREEMENT Recorded Feb 8, 2010
From: DEL MONTE CORPORATION
To: BANK OF AMERICA, N.A.
Reel/Frame 023905/0643 →
RELEASE OF SECURITY INTEREST Recorded Feb 8, 2010
From: BANK OF AMERICA, N.A.
To: DEL MONTE CORPORATION
Reel/Frame 023905/0799 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT SUPPLEMENT Recorded Aug 17, 2006
From: DEL MONTE CORPORATION
To: BANK OF AMERICA, N.A.
Reel/Frame 018120/0805 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 1, 2006
From: THE MEOW MIX COMPANY
To: DEL MONTE CORPORATION
Reel/Frame 018039/0084 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT SUPPLEMENT Recorded Jul 28, 2006
From: MEOW MIX HOLDINGS, INC.; THE MEOW MIX COMPANY; MEOW MIX DECATUR PRODUCTION I LLC
To: BANK OF AMERICA, N.A.
Reel/Frame 018018/0826 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENT RIGHTS AT REEL/FRAME 016283/0001 Recorded May 19, 2006
From: UBS, AG, STAMFORD BRANCH
To: THE MEOW MIX COMPANY
Reel/Frame 017636/0725 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 9, 2006
From: LIN, CHARLES; DAHLGREN, JAY; MORRIS, SCOTT; THOMPSON, RICHARD
To: THE MEOW MIX COMPANY
Reel/Frame 017592/0966 →
SECURITY AGREEMENT Recorded Jul 19, 2005
From: THE MEOW MIX COMPANY
To: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
Reel/Frame 016283/0001 →