Pulsed vapor desorber
View Patent ↗Vapor concentrators are used to provide a higher concentration of trace target vapor than would normally be available in the environment. This is accomplished by allowing the trace target vapor to adsorb onto a concentrating surface and subsequently releasing the trace target vapor by heating the surface. An improved desorbing method is providing by a fast pulse of photons, which only heats the near surface region, rather than the entire mass of the substrate on which the concentrating surface resides. Since all of the trace target vapor is released in a short time interval, the vapor is less diluted by carrier gas than would occur during the slower temperature ramp that results when the entire substrate mass is heated. A more highly concentrated target vapor is produced with less input of energy.
1. A method for the rapid desorption of adsorbed gases in a vapor concentrator system comprising:
providing a chamber with at least one entrance orifice and at least one exit orifice for the passage of vapor;
providing a carrier gas moved by a gas pump to assist the passage of trace target vapor into and out of said chamber;
providing at least one substrate with a surface for the concentration of said trace target vapor within said chamber;
providing at least one lamp that emits photons in optical communication with said surface of said substrate;
providing an electronic circuit that energizes said lamp, wherein the lamp is induced to produce a main pulse of photons with a duration less than 100 milliseconds;
passing gas containing said trace target vapor over said substrate to accumulate said target vapor through adsorption on said surface;
emitting said main pulse of photons to induce said trace target vapor to rapidly desorb from said surface of said substrate; and
passing said carrier gas over said substrate to assist said desorbed trace target vapor in being swept from said chamber through said exit orifice.
2. A method for rapid desorption as in claim 1 wherein said carrier gas is at least one of air, nitrogen, an inert gas, carbon dioxide, hydrogen, ammonia, and water vapor.
3. A method for rapid desorption as in claim 1 wherein the surface of said substrate is coated with an adsorption-enhancing chemical.
4. A method for rapid desorption as in claim 1 wherein said lamp contains an inert gas.
5. A method for rapid desorption as in claim 1 wherein said main pulse of photons includes wavelengths in at least one of infrared, visible, and ultraviolet.
6. A method for rapid desorption as in claim 1 wherein said chamber includes at least one component that is heated to reduce adsorption of said trace target vapor on the surface of said component.
7. A method for rapid desorption as in claim 1 wherein said lamp is in optical communication with at least one optically reflecting surface to concentrate and contain a photon flux from the main pulse.