Glycerine foots salt separation system
View Patent ↗The present invention provides a method and apparatus for the recovery of salt from a glycerine process, allowing the salt to be used in a brine solution. A salt settling tank is positioned inline between the foots from a crude still bottom and a foot still. Salt settles to the bottom of the settling tank and into a salt receiver positioned below, while clarified liquid overflows to the foot still. Salt from the salt receiver is then semi-continuously transferred into a salt extractor where the salt is removed from the mother liquor. A condensate is then circulated into the salt extractor and the salt slurry is then stored in a brine storage tank.
1. A method for recovering salt from a glycerine refining process residue, comprising:
a) providing a settling tank with an upper inlet through which liquid residue from a glycerine refining process is introduced into said settling tank, a conical shaped bottom onto which salt in the residue falls, and an overflow outlet positioned between the upper inlet and the bottom through which liquid is discharged;
b) providing a receiving tank located below the settling tank which is arranged to receive salt from the settling tank, and
c) providing a salt extractor located below the receiving tank which is arranged to receive solid material from the receiving tank and water from another source and to discharge the mixture;
d) a first step of directing liquid obtained from the glycerine refining process containing salt into the upper inlet of the settling tank;
e) a second step of allowing the liquid to settle in the settling tank then discharging the liquid obtained through the overflow outlet and transferring salt collected at the bottom of the settling tank to the receiving tank;
f) a third step of transferring salt from the receiving tank to the extractor; and
g) a fourth step of introducing water into the extractor to dilute the salt received from the receiving tank and then discharge the diluted mixture for collection.
2. The method of claim 1 further comprising:
a) providing said salt settling tank with a sidewall outlet in a sidewall for overflow of a clear liquid fraction;
b) adding a first step between the directing and allowing steps of directing the clear liquid fraction through the sidewall outlet for overflow.
3. The method of claim 2 further comprising:
a) providing a foots still and connection from said sidewall outlet to said foots still; and
b) adding a step between the first step and the third step comprising overflowing said clear liquid fraction through said sidewall outlet.
4. The method of claim 3 further comprising:
a) providing apparatus to automatically provide salt from said salt receiving tank to said salt extractor; and
b) adding a step between the overflowing step and the third step of automatically providing salt from said salt settling tank to said salt extractor.
5. The method of claim 4 further comprising:
a) providing the salt receiver with a sight glass; and
b) adding a step between the automatically providing step and the third step of determining the salt level using said sight glass.