Process for the granulation of an animal feedstuff additive
View Patent ↗The invention relates to a process for the granulation of an animal feedstuffs additive comprising amino acids or vitamins in a circulating fluidized bed, wherein the additive is preferably a fermentation product and optionally comprises further constituents from the fermentation broth.
1. A process for granulation of L-threonine from a solution comprising the steps of:
(a) spraying a superheated aqueous suspension or an aqueous solution of L-threonine in the granulation chamber, the aqueous solution of L-threonine being superheated to a temperature ranging from 100° C. to 160° C.;
(b) granulating L-threonine into solid particles in a circulating fluidized bed of a granulation chamber;
(c) discharging at least 30% weight of the solid particles with a drying gas stream from the granulation chamber;
(d) separating the discharged solid particles from the drying gas stream of step (c);
(e) removing granulated particles within the size range of greater than 100 μm to 2,000 μm from the granulation chamber at a rate such that the amount of solid L-threonine remains constant in the granulation chamber; and
(f) recycling the solid particles of step (d), which have not reached the desired size range of greater than 100 μm to 2,000 μm, back into the circulating fluidized bed of steps (a)-(b).
2. The process of claim 1 , wherein the drying gas stream is passed into the granulation chamber through an inflow base and is allowed to flow upwards through the circulating fluidized bed against the force of gravity.
3. The process according to claim 2 , wherein the drying gas stream from the inflow base flows at an inflow speed that is 1 to 10 times the speed necessary to allow the desired particle size to circulate out of the granulation chamber with the drying gas stream.
4. The process according to claim 3 , wherein the inflow speed is 1 to 3 times the speed necessary to allow the desired particle size to circulate out of the granulation chamber with the drying gas stream.
5. The process of claim 1 , wherein the solid particles in the granulation chamber are discharged upwards in a continuous manner with the drying gas stream.
6. The process according to claim 1 , wherein the circulation rate per hour of the fluidized bed is 2 to 100 times the mass remaining in the granulation chamber.
7. The process according to claim 1 , wherein the drying gas stream flows through an inflow base into the granulation chamber at a temperature ranging from 100 to 450° C.
8. The process according to claim 1 , wherein an aqueous solution of L-threonine is sprayed into the granulation chamber using pneumatic nozzles or pressure nozzles.
9. The process according to claim 8 , wherein the nozzle is positioned in the middle and bottom of the granulation chamber yet above the inflow base wherein the aqueous solution of L-threonine is sprayed in an upward direction.
10. The process according to claim 1 , wherein the superheated aqueous solution or suspension is sprayed through the nozzle using a feed-line that is under 1 to 5 bars of pressure.
11. The process according to claim 10 , wherein the nozzle is a two component pressure nozzle operated with compressed air that further comprises an extended liquid insert with a triple-groove whirling body wherein a drop of up to 5 bars of pressure is achieved when the superheated aqueous solution or suspension of L-threonine is sprayed through the two component pressure nozzle.
12. The process according to claim 1 , wherein mechanical energy is introduced in the fluidized bed in order to achieve uniform granulated particles and an increase in bulk density in the granulated particles.
13. The process according to claim 12 , wherein the mechanical energy is introduced into the fluidized bed by a movable flat structure.
14. The process according to claim 13 , wherein the movable flat structure is selected from the group consisting of rotating knives, vanes, blade surfaces, flat iron bars or compacters.
15. The process according to claim 1 , wherein the L-threonine has a purity of 80-99.5%.
16. The process according to claim 1 , wherein step (e) comprises removing granulated particles within the size range of 300 μm to 800 μm from the granulation chamber at a rate such that the amount of solid L-threonine remains constant in the granulation chamber.
17. The process according to claim 1 , wherein step (e) comprises removing granulated particles within the size range of 500 μm to 1,200 μm from the granulation chamber at a rate such that the amount of solid L-threonine remains constant in the granulation chamber.