IP Library Granted Patent US 7,806,077
Granted Patent B2
US 7,806,077 · App. 10/902,435 · Granted Oct 5, 2010

Plasma nozzle array for providing uniform scalable microwave plasma generation

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Quick Facts
Patent No.
US 7,806,077
App. No.
10/902,435
Granted
Oct 5, 2010
Kind
B2
Abstract

Microwave plasma nozzle array systems and methods for configuring the microwave plasma nozzle arrays are disclosed. The microwaves are transmitted to a microwave cavity in a specific manner and form an interference pattern that includes high-energy regions within the microwave cavity. The high-energy regions are controlled by the phases and the wavelengths of the microwaves. A plurality of nozzle elements is provided in the array. Each of the nozzle elements has a portion partially disposed in the microwave cavity and receives a gas for passing therethrough. The nozzle elements receive microwave energy from one of the high-energy regions. Each of the nozzle elements include a rod-shaped conductor having a tip that focuses the microwaves and a plasma is then generated using the received gas.

Claims (52)

1. A method for generating plasma plumes through a microwave plasma nozzle array, comprising the steps of:

directing microwaves into a microwave cavity in opposing directions such that the microwaves interfere with each other and form a standing microwave pattern that is stationary within the microwave cavity;

adjusting a phase of at least one of the microwaves to form high-energy regions in the standing microwave pattern, the high-energy regions having a width where an amplitude of the microwaves exceeds a threshold value;

providing an array of nozzles, each of the nozzles including:

a rod-shaped conductor having a first end and a second end where the first end being a leading end of the rod-shaped conductor, and

a gas flow tube having a first end portion disposed inside the microwave cavity and a second end portion disposed outside of the microwave cavity, the first end portion is made of a substantially microwave transparent material and further the gas flow tube surrounds at least a part of the rod-shaped conductor in such a manner that the second end portion is in proximity to the first end of the rod-shaped conductor, and a portion of the gas flow tube is connected to the microwave cavity at a location where the gas flow tube surrounds the rod-shaped conductor; and

disposing the array of nozzles in the microwave cavity such that a middle portion of the rod-shaped conductor is held with respect to said gas flow tube via a holding member, at least the second end of each of the rod-shaped conductors is disposed in the microwave cavity to receive microwave energy from a corresponding one of the high-energy regions of the standing microwave pattern; the first end is being outside the microwave cavity and the second end is suspended free in the microwave cavity in such a manner that the second end is free from contact with any walls forming the microwave cavity and any members that are in contact with said walls of the microwave cavity so that plasma is formed outside of the microwave cavity.

2. A method as defined in claim 1 , wherein said step of directing microwaves includes the steps of:

transmitting microwaves to the microwave cavity; and

reflecting microwaves using a sliding short circuit operatively connected to the microwave cavity.

3. A method as defined in claim 1 , wherein said step of directing microwaves includes the step of:

transmitting microwaves generated by two microwave power heads to the microwave cavity via respective waveguides, and

introducing the microwaves into the microwave cavity directly from opposite sides of the cavity.

4. A method as defined in claim 1 , wherein said step of adjusting a phase of at least one of the microwaves includes forming the high-energy regions in a striped pattern so that the nozzles are located within the high-energy regions.

5. A method as defined claim 1 , wherein said step of providing an array of nozzles includes providing each of the conductors with a portion for collecting the microwaves and a tapered tip for focusing the microwaves to generate the plasma plumes.

6. A method for generating plasma plumes through a microwave plasma nozzle array as defined in claim 1 ,

wherein each of said nozzles includes an inner shield disposed around the inner surface of the gas flow tube to reduce microwave loss through the gas flow tube.

7. The method as defined in claim 1 , wherein one end of the gas flow tube projects externally from the microwave cavity.

8. A method for generating plasma plumes through a microwave plasma nozzle array, comprising the steps of:

directing a first pair of microwaves into a microwave cavity in opposing directions along a first axis;

directing a second pair of microwaves into the microwave cavity in opposing directions along a second axis, the first axis being normal to the second axis such that the first and the second pairs of microwaves cross and interfere with each other to form high-energy regions that are arranged in a matrix pattern and are stationary within the microwave cavity;

adjusting a phase of at least one of the microwaves to control the high-energy regions, the high-energy regions having a width where an amplitude of the microwaves exceeds a threshold value;

providing a plurality of nozzles, each of the nozzles including:

a rod-shaped conductor having a first end and a second end where the first end being a leading end of the rod-shaped conductor, and

a gas flow tube having a first end portion disposed inside the microwave cavity and a second end portion

disposed outside of the microwave cavity, the first end portion is made of a material which is substantially transparent to microwaves and further the gas flow tube surrounds at least part of the rod-shaped conductor in such a manner that the second end portion is in proximity to the first end of the rod-shaped conductor, and a portion of the gas flow tube is connected to the microwave cavity at a location where the gas flow tube surrounds the rod-shaped conductor; and

disposing a plurality of nozzle arrays in the microwave cavity such that a middle portion of the rod-shaped conductor is held with respect to said gas flow tube via a holding member, at least the second end of each of the rod-shaped conductors in each nozzle is disposed in the microwave cavity so that each nozzle element of the nozzle arrays is configured to receive microwave energy from a corresponding one of the high-energy regions; the first end is being outside the microwave cavity and the second end is suspended free in the microwave cavity in such a manner that the second end is free from contact with any walls forming the microwave cavity and any members that are in contact with said walls of the microwave cavity so that plasma is formed outside of the microwave cavity.

9. A method as defined in claim 8 , wherein said step of directing the first pair of microwaves includes the steps of:

transmitting microwaves to the microwave cavity; and

reflecting microwaves using a sliding short circuit operatively connected to the microwave cavity.

10. A method as defined in claim 8 , wherein each of said step of directing the first pair of microwaves and said step of directing the second pair of microwaves includes the step of:

transmitting microwaves generated by two microwave power heads to the microwave cavity, via respective waveguides, and

introducing the microwaves into the microwave cavity directly from opposite sides of the cavity.

11. A method as defined in claim 8 , further comprising the steps of:

generating the microwaves by a microwave power head; and

providing a power splitter connected to the microwave power head.

12. A method as defined in claim 8 , wherein said step of adjusting a phase of at least one of the microwaves includes adjusting phases of the first pair of microwaves.

13. A method as defined in claim 8 , wherein said step of adjusting a phase of at least one of the microwaves includes adjusting phases of the second pair of microwaves.

14. A method as defined in claim 8 , wherein said step of adjusting a phase of at least one of the microwaves includes adjusting phases of both the first pair and the second pair of microwaves.

15. A method for generating plasma plumes through a microwave plasma nozzle array as defined in claim 8 ,

wherein each of said nozzles includes an inner shield disposed around the inner surface of the gas flow tube to reduce microwave loss through the gas flow tube.

16. The method as defined in claim 8 , wherein one end of the gas flow tube projects externally from the microwave cavity.

17. A method for generating plasma plumes through a microwave plasma nozzle array, comprising the steps of:

directing microwaves into a microwave cavity in opposing directions through separate waveguides such that the microwaves are injected into the microwave cavity via two opposite openings formed on a wall of the microwave cavity, interfere and form a standing microwave pattern that is stationary within the microwave cavity;

adjusting a phase of at least one of the microwaves to control high-energy regions generated by the standing microwave pattern, the high-energy regions having a width where an amplitude of the microwaves exceeds a threshold value;

providing a plurality of nozzles, each of the nozzles including:

a rod-shaped conductor having a first end and a second end where the first end being a leading end of the rod-shaped conductor, and

a gas flow tube having a first end portion disposed inside the microwave cavity and a second end portion disposed outside of the microwave cavity, the first end portion is made of a material substantially transparent to microwaves and further the gas flow tube surrounds at least part of the rod-shaped conductor in such a manner that the second end portion is in proximity to the first end of the rod-shaped conductor, and a portion of the gas flow tube is connected to the microwave cavity at a location where the gas flow tube surrounds the rod-shaped conductor; and

disposing the nozzle array at least partially in the microwave cavity so that a middle portion of the rod-shaped conductor is held with respect to said gas flow tube via a holding member, at least the second end of the rod-shaped conductor is disposed in the microwave cavity to receive microwave energy from a corresponding one of the high-energy regions of the standing microwave pattern; the first end is being outside the microwave cavity and the second end is suspended free in the microwave cavity in such a manner that the second end is free from contact with any walls forming the microwave cavity and any members that are in contact with said walls of the microwave cavity so that plasma is formed outside of the microwave cavity.

18. A method for generating plasma plumes through a microwave plasma nozzle array as defined in claim 17 ,

wherein each of said nozzles includes an inner shield disposed around the inner surface of the gas flow tube to reduce microwave loss through the gas flow tube.

19. The method as defined in claim 17 , wherein one end of the gas flow tube projects externally from the microwave cavity.

Assignments (41)
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: CLAPP, DAVID
To: NOXILIZER, INC.
Reel/Frame 072667/0406 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: SUZANNE P. MURPHY TRUST, A TRUST
To: NOXILIZER, INC.
Reel/Frame 072668/0664 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: ALJ INVESTMENTS LLC
To: NOXILIZER, INC.
Reel/Frame 072666/0927 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: JOHNSON, BLANCHE M.; LASCELLE, WILLIAM A.
To: NOXILIZER, INC.
Reel/Frame 072667/0034 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: ANDERSON, M. JEAN
To: NOXILIZER, INC.
Reel/Frame 072667/0165 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: GRAY, C. BOYDEN
To: NOXILIZER, INC.
Reel/Frame 072667/0204 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: SAMUEL, MATHIAS
To: NOXILIZER, INC.
Reel/Frame 072667/0264 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: MCDONALD, CAPERS W.
To: NOXILIZER, INC.
Reel/Frame 072667/0277 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: THE ABELL FOUNDATION, INC.
To: NOXILIZER, INC.
Reel/Frame 072666/0620 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: GORDAN GRAY TRUST FBO C. BOYDEN GRAY, A TRUST
To: NOXILIZER, INC.
Reel/Frame 072667/0533 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: EUGENE C. PULLIAM TRUST FBO SUZANNE P. MURPHY
To: NOXILIZER, INC.
Reel/Frame 072667/0776 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: EUGENE C. PULLIAM TRUST FBO SUZANNE P. MURPHY
To: NOXILIZER, INC.
Reel/Frame 072667/0884 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: GORDAN GRAY TRUST FBO C. BOYDEN GRAY, A TRUST
To: NOXILIZER, INC.
Reel/Frame 072667/0988 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: SHEETS, JOHN RICHARD
To: NOXILIZER, INC.
Reel/Frame 072668/0046 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: PENSCO TRUST COMPANY, CUSTODIAN FBO CHARLES T. HALTER, IRA, A TRUST
To: NOXILIZER, INC.
Reel/Frame 072668/0057 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: PENSCO TRUST COMPANY, CUSTODIAN FBO JERRY L. PARROTT, IRA
To: NOXILIZER, INC.
Reel/Frame 072668/0098 →
RELEASE OF SECURITY INTEREST Recorded Oct 24, 2025
From: PENSCO TRUST COMPANY, CUSTODIAN FBO JERRY L. PARROTT, IRA
To: NOXILIZER, INC.
Reel/Frame 072668/0599 →
SECURITY INTEREST Recorded Jul 6, 2017
From: NOXILIZER, INC.
To: GORDON GRAY TRUST FBO C. BOYDEN GRAY
Reel/Frame 042915/0581 →
SECURITY INTEREST Recorded Jul 6, 2017
From: NOXILIZER, INC.
To: EUGENE C. PULLIAM TRUST FBO SUZANNE P. MURPHY
Reel/Frame 042915/0613 →
SECURITY INTEREST Recorded Jun 30, 2017
From: NOXILIZER, INC.
To: SHEETS, JOHN RICHARD
Reel/Frame 042877/0459 →
SECURITY INTEREST Recorded Jun 30, 2017
From: NOXILIZER, INC.
To: THE ABELL FOUNDATION, INC.
Reel/Frame 042877/0611 →
SECURITY INTEREST Recorded May 26, 2017
From: NOXILIZER, INC.
To: PENSCO TRUST COMPANY, CUSTODIAN, FBO JERRY L. PARROTT, IRA
Reel/Frame 042517/0141 →
SECURITY INTEREST Recorded May 26, 2017
From: NOXILIZER, INC.
To: PENSCO TRUST COMPANY, CUSTODIAN, FBO JERRY L. PARROTT, IRA
Reel/Frame 042517/0273 →
SECURITY INTEREST Recorded May 25, 2017
From: NOXILIZER, INC.
To: EUGENE C. PULLIAM TRUST FBO SUZANNE P. MURPHY
Reel/Frame 042508/0093 →
SECURITY INTEREST Recorded May 24, 2017
From: NOXILIZER, INC.
To: SUZANNE P. MURPHY TRUST
Reel/Frame 042488/0307 →
SECURITY INTEREST Recorded May 23, 2017
From: NOXILIZER, INC.
To: SAMUEL, MATHIAS
Reel/Frame 042479/0490 →
SECURITY INTEREST Recorded May 23, 2017
From: NOXILIZER, INC.
To: MCDONALD, CAPERS W.
Reel/Frame 042477/0699 →
SECURITY INTEREST Recorded May 23, 2017
From: NOXILIZER, INC.
To: PENSCO TRUST COMPANY, CUSTODIAN FBO CHARLES T. HALTER, IRA
Reel/Frame 042478/0130 →
SECURITY INTEREST Recorded May 23, 2017
From: NOXILIZER, INC.
To: GRAY, C. BOYDEN
Reel/Frame 042478/0306 →
SECURITY INTEREST Recorded May 23, 2017
From: NOXILIZER, INC.
To: GORDON GRAY TRUST FBO C. BOYDEN GRAY
Reel/Frame 042478/0598 →
SECURITY INTEREST Recorded May 23, 2017
From: NOXILIZER, INC.
To: ANDERSON, M. JEAN
Reel/Frame 042478/0841 →
SECURITY INTEREST Recorded May 23, 2017
From: NOXILIZER, INC.
To: JOHNSON, BLANCHE M.; LASCELLE, WILLIAM A.
Reel/Frame 042479/0084 →
SECURITY INTEREST Recorded May 23, 2017
From: NOXILIZER, INC.
To: CLAPP, DAVID
Reel/Frame 042479/0255 →
SECURITY INTEREST Recorded Mar 30, 2017
From: NOXILIZER, INC.
To: ALJ INVESTMENTS LLC
Reel/Frame 041803/0157 →
CORRECTIVE ASSIGNMENT TO CORRECT THE NAME OF THE ASSIGNEE WHICH WAS MISPELLED PREVIOUSLY RECORDED ON REEL 030902 FRAME 0276. ASSIGNOR(S) HEREBY CONFIRMS THE NAME OF THE ASSIGNEE TO BE CORRECTED. Recorded Sep 9, 2013
From: SAIAN CORPORATION
To: NOXILIZER, INC.
Reel/Frame 031188/0797 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 30, 2013
From: AMARANTE TECHNOLOGIES, INC.
To: RECARBON, INC.
Reel/Frame 030902/0216 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 30, 2013
From: SAIAN CORPORATION
To: NOXILIXER, INC.
Reel/Frame 030902/0276 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 10, 2010
From: NORITSU KOKI CO., LTD.
To: SAIAN CORPORATION
Reel/Frame 024812/0226 →
CHANGE OF ASSIGNEE'S ADDRESS Recorded Jan 9, 2007
From: AMARANTE TECHNOLOGIES, INC.
To: AMARANTE TECHNOLOGIES, INC.
Reel/Frame 018756/0793 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 7, 2005
From: IMAGINEERING, INC.
To: NORITSU KOKI CO., LTD.; AMARANTE TECHNOLOGIES, INC.
Reel/Frame 016669/0985 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 20, 2004
From: LEE, SANG HUN; KIM, JAY JOONGSOO
To: NORITSU KOKI CO., LTD.; AMARANTE TECHNOLOGIES, INC.; IMAGINEERING, INC.
Reel/Frame 015907/0817 →