IP Library Granted Patent US 7,364,826
Granted Patent B2
US 7,364,826 · App. 10/902,818 · Granted Apr 29, 2008

Electrostatic latent image developing toner, and method for manufacturing electrostatic latent image developer and electrostatic latent image developing toner

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Quick Facts
Patent No.
US 7,364,826
App. No.
10/902,818
Granted
Apr 29, 2008
Kind
B2
Abstract

There is provided an electrostatic latent image developing toner including a binder resin, a colorant, and a release agent, wherein the shape factor SF1 of the toner is within the range from 110 to 140, the volume average particle size of the toner is within the range from 1.2 μm to 4.8 μm, and the crystallinity of the release agent within the toner is within the range from 35 to 80. There is also provided a method for manufacturing such a toner.

Claims (35)

1. An electrostatic latent image developing toner including a binder resin, a colorant, and a release agent, wherein:

shape factor SF1 of the toner is within a range from 110 to 140, where SF1=(ML 2 /A)·(π/4)·100, ML denoting an absolute maximum length of a toner particle and A denoting a projected area of a toner particle;

volume average particle size of the toner is within a range from 1.2 pm to 4.8 μm;

crystallinity of the release agent within the toner is within a range from 35 to 80; and

R/D is within a range from 0.2 to 0.6, where R denotes a domain average longitudinal diameter of the release agent within the toner and D denotes the volume average particle size of the toner.

2. An electrostatic latent image developing toner as defined in claim 1 , wherein the crystallinity is within a range from 40 to 75.

3. An electrostatic latent image developing toner as defined in claim 1 , wherein the crystallinity is within a range from 50 to 70.

4. An electrostatic latent image developing toner as defined in claim 1 , wherein particle size distribution GSD of the toner is no greater than 1.26, where GSD=[(d16/d84)] 0.5 , volume d16 denotes a particle size where an accumulated volume in an accumulation distribution from larger size reaches 16% and volume d84 denotes a particle size where the accumulated volume in the accumulation distribution from larger size reaches 84%.

5. An electrostatic latent image developing toner as defined in claim 1 , wherein glass transition temperature of the binder resin is within a range from 40° C. to 70° C.

6. An electrostatic latent image developing toner as defined in claim 1 , wherein weight average molecular weight Mw of the binder resin is within a range from 6000 to 45000.

7. An electrostatic latent image developing toner as defined in claim 1 , wherein the binder resin is a vinyl-based resin.

8. An electrostatic latent image developing toner as defined in claim 1 , wherein content of the release agent within the toner is within a range of 6 to 25 wt % of the toner weight.

9. An electrostatic latent image developing toner as defined in claim 1 , wherein the shape factor SF1 of the toner is within a range from 115 to 135.

10. An electrostatic latent image developing toner as defined in claim 1 , wherein the shape factor SF1 of the toner is within a range from 115 to 130.

11. An electrostatic latent image developing toner as defined in claim 1 , wherein the volume average particle size of the toner is within a range from 2.0 μm to 4.5 μm.

12. An electrostatic latent image developing toner as defined in claim 1 , wherein the volume average particle size of the toner is within a range from 2.5 μm to 4.0 μm.

13. An electrostatic latent image developer comprising an electrostatic latent image developing toner including a binder resin, a colorant, and a release agent, wherein: shape factor SF1 of the toner is within a range from 110 to 140, where SF1=(ML 2 /A)·(π/4)·100, ML denoting an absolute maximum length of a toner particle and A denoting a projected area of a toner particle;

volume average particle size of the toner is within a range from 1.2 μm to 4.8 μm;

crystallinity of the release agent within the toner is within a range from 35 to 80; and

R/D is within a range from 0.2 to 0.6, where R denotes a domain average longitudinal diameter of the release agent within the toner and D denotes the volume average particle size of the toner.

14. A method for manufacturing an electrostatic latent image developing toner including a binder resin, a colorant, and a release agent, the method comprising a process of granulating particles of the toner, the granulating process including:

a step of heating to or above glass transition temperature of the binder resin; and

a step of cooling performed after the heating step by speedily cooling at a cooling rate of 10°C./minute or faster from the temperature of the heating step, wherein:

the toner obtained as a result of the granulating process is such that:

shape factor SF1 of the toner is within a range from 110 to 140, where SF1=(ML 2 /A)·(π/4)·100, ML denoting an absolute maximum length of a toner particle and A denoting a projected area of a toner particle;

volume average particle size of the toner is within a range from 1.2 μm to 4.8 μm;

crystallinity of the release agent within the toner is within a range from 35 to 80; and

R/D is within a range from 0.2 to 0.6, where R denotes a domain average longitudinal diameter of the release agent within the toner and D denotes the volume average particle size of the toner.

15. A method for manufacturing an electrostatic latent image developing toner as defined in claim 14 , wherein the cooling step includes adding, into a tank in which the granulating process is performed, a cooled solvent or a solid obtained by cooling and solidifying the solvent.

16. A method for manufacturing an electrostatic latent image developing toner as defined in claim 14 , wherein the cooling step includes adding, into a tank in which the granulating process is performed, a liquid or solid form of a cooling substance that is in gas phase at room temperatures.

17. A method for manufacturing an electrostatic latent image developing toner as defined in claim 14 , wherein

the heating step includes heating to or above a temperature value that is 1.6 times greater than the glass transition temperature of the binder resin, and

the cooling step includes cooling, after the heating step, to a temperature below a value that is 1.4 times greater than the glass transition temperature of the binder resin.

18. A method for manufacturing an electrostatic latent image developing toner as defined in claim 17 , wherein the cooling step includes adding, into a tank in which the granulating process is performed, a cooled solvent or a solid obtained by cooling and solidifying the solvent.

19. A method for manufacturing an electrostatic latent image developing toner as defined in claim 17 , wherein the cooling step includes adding, into a tank in which the granulating process is performed, a liquid or solid form of a cooling substance that is in gas phase at room temperatures.

Assignments (1)
CHANGE OF NAME Recorded Aug 12, 2021
From: FUJI XEROX CO., LTD.
To: FUJIFILM BUSINESS INNOVATION CORP.
Reel/Frame 058287/0056 →