IP Library Granted Patent US 8,680,357
Granted Patent B1
US 8,680,357 · App. 10/968,456 · Granted Mar 25, 2014

Dehydrogenation catalyst

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Quick Facts
Patent No.
US 8,680,357
App. No.
10/968,456
Granted
Mar 25, 2014
Kind
B1
Abstract

A process for the dehydrogenation of a hydrocarbon feed stream, wherein the hydrocarbon feed stream substantially includes hydrocarbons containing 3 to 5 carbon atoms, wherein the process includes passing the hydrocarbon feed stream over a dehydrogenation catalyst containing from about 50 to about 90 percent by weight of an eta alumina carrier, about 10 to about 30 percent by weight of chromia and from about 0.1 to about 5 percent by weight of zirconia added as a stabilizing material.

Claims (23)

1. A process for the dehydrogenation of a C 3 -C 5 hydrocarbon feed stream comprising

providing a dehydrogenation catalyst where the dehydrogenation catalyst comprises from about 70 to about 90 percent of eta alumina formed carrier, from about 15 to about 25 percent of a chromium compound and from about 0.1 to about 5 percent, by weight, of a zirconium compound, wherein the chromium compound and zirconium compound are impregnated on the eta alumina formed carrier;

passing an aliphatic hydrocarbon feed stream comprising C 3 -C 5 compounds over the dehydrogenation catalyst; and

producing a dehydrogenated unsaturated C 3 -C 5 hydrocarbon product.

2. The process of claim 1 wherein the hydrocarbon feed stream comprises isobutane.

3. The process of claim 1 wherein the hydrocarbon feed stream comprises propanes and pentanes.

4. The process of claim 1 wherein the zirconium compound comprises from about 0.1 to about 1 percent of the dehydrogenation catalyst, by weight.

5. The process of claim 1 wherein the dehydrogenation catalyst has a surface area from about 60 m 2 /g to about 120 m 2 /g.

6. The process of claim 1 wherein the dehydrogenation catalyst further comprises an additive selected from the group consisting of silica, lanthanum compounds, alkali metal additive and mixtures thereof.

7. The process of claim 1 wherein the dehydrogenation catalyst further comprises an alkali metal additive selected from the group consisting of potassium, sodium and cesium compounds and mixtures thereof.

8. The process of claim 1 wherein the dehydrogenation catalyst is prepared by impregnating the eta alumina formed carrier with the chromium compound and with the zirconium compound in separate steps.

9. The process of claim 1 wherein the dehydrogenation catalyst is prepared by co-impregnating the eta alumina formed carrier with the chromium compound and the zirconium compound in a single step.

10. A process for the dehydrogenation of a C 3 -C 5 hydrocarbon feed stream comprising

providing a dehydrogenation catalyst where the dehydrogenation catalyst comprises from about 70 to about 90 percent, by weight, of eta alumina formed carrier, from about 15 to about 25 percent, by weight, of a chromium compound, from about 0.1 to about 1 percent by weight of a zirconium compound, and an additive selected from the group consisting of silica, lanthanum compounds, and alkali metal additives and mixtures thereof, wherein the chromium compound and zirconium compound are impregnated on the eta alumina formed carrier;

passing an aliphatic hydrocarbon feed stream comprising C 3 -C 5 compounds over the dehydrogenation catalyst; and

producing a dehydrogenated unsaturated C 3 -C 5 hydrocarbon product.

11. The process of claim 10 wherein the hydrocarbon feed stream comprises isobutane.

12. The process of claim 10 wherein the hydrocarbon feed stream comprises propanes and pentanes.

13. The process of claim 10 wherein the zirconium compound comprises from about 0.1 to about 1 percent of the dehydrogenation catalyst, by weight.

14. The process of claim 10 wherein the dehydrogenation catalyst has a surface area from about 60 m 2 /g to about 120 m 2 /g.

15. The process of claim 10 wherein the alkali metal additive is selected from the group consisting of potassium, sodium and cesium compounds and mixtures thereof.

16. The process of claim 10 wherein the dehydrogenation catalyst is prepared by impregnating the eta alumina formed carrier with the chromium compound and with the zirconium compound in separate steps.

17. The process of claim 10 wherein the dehydrogenation catalyst is prepared by co-impregnating the eta alumina formed carrier with the chromium compound and the zirconium compound in a single step.

Assignments (3)
CONFIRMATORY DEED OF ASSIGNMENT EFFECTIVE DEC. 31, 2017 Recorded Sep 14, 2021
From: CLARIANT CORPORATION
To: CLARIANT INTERNATIONAL LTD
Reel/Frame 057499/0988 →
MERGER Recorded Jan 13, 2014
From: SUD-CHEMIE INC.
To: CLARIANT CORPORATION
Reel/Frame 031951/0466 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 4, 2011
From: ROKICKI, ANDRZEJ; FRIDMAN, VLADIMIR
To: SUD-CHEMIE INC.
Reel/Frame 025747/0494 →