Method for using divider rods for separating superconducting regions in fine filament internal tin wire
View Patent ↗A method for decreasing the effective magnetic filament sizes for high current internal tin Nb 3 Sn superconductors. During processing composite rods preferably comprised of copper clad Ta rods of approximately the same dimensions as the hexes in the designed filament billet stack are used as dividers in the subelement. Along with the Ta rods, Ta strips are strategically situated against the Nb or Nb alloy barrier tube which surrounds the subelement. The use of Ta as a spacer instead of copper prevents any reasonable likelihood of bridging of the superconducting phases formed after final reaction.
1. A method for producing a multifilament Nb 3 Sn superconducting wire comprising the steps of:
a) packing a plurality of Nb or Nb alloy rods within a copper containing matrix to form a packed subelement for said superconducting wire;
b) packing divider rods amongst the Nb or Nb alloy rods in the copper containing matrix along with Ta divider strips to thereby divide said subelement into regions bounded by said divider rods and strips; said divider strips further being positioned within a Nb or Nb alloy diffusion barrier which surrounds said subelement as to prevent the Nb or Nb alloy barrier from reacting during a subsequent diffusion step for forming said Nb 3 Sn;
c) providing sources of Sn within said subelement;
d) assembling a plurality of said subelements within a further copper containing matrix;
e) reducing said assemblage of step(d) to wire form; and
f) diffusing the said Sn into the Nb or Nb alloy rods to form Nb 3 Sn regions separated by said divider rods and strips.
2. A method in accordance with claim 1 wherein in step a) said Nb or Nb alloy rods are ensheathed in a copper or copper alloy.
3. A method in accordance with claim 2 , wherein the encased Nb or Nb alloy rods are formed into hexed cross sectioned rods for use in packing the subelement.
4. A method in accordance with claim 1 , wherein said divider rods comprise Ta or Ta alloy rods in copper or copper alloy foils or sheaths.
5. A method in accordance with claim 4 , wherein the Ta divider rods are formed into a hexagonal cross section to enable their packing among the hexed cross section Nb or Nb alloy rods.
6. A method in accordance with claim 4 , wherein the Ta divider rods are formed into a round cross section.
7. A method in accordance with claim 4 wherein said Ta divider rods are strategically placed along with the Ta strips so as to subdivided the subelement into the desired number of sections.
8. A method in accordance with claim 1 , wherein the Sn is diffused into said Nb or Nb alloy rods by an internal Sn process.
9. A method in accordance with claim 8 , wherein the subelement from step ( 1 d ) is extruded gundrilled and the resulting holes filled with said Sn or Sn alloy.
10. A method in accordance with claim 8 wherein the subelements from step ( 1 d ) is extruded, gundrilled, filled with salt, restacked, extruded again, and the salt replaced with Sn or Sn alloy.
11. A method in accordance with claim 1 , wherein said divider rods comprise Ti or Ti alloy rods in copper or copper alloy sheaths.
12. A method in accordance with claim 11 , wherein the Ti or Ti alloy rods are placed in the subelement to separate superconducting regions to reduce the effective filament diameter and AC losses.
13. A method in accordance with claim 1 , wherein in step (d) the subelements are hexed in cross-section.