IP Library Granted Patent US 7,501,106
Granted Patent B2
US 7,501,106 · App. 10/994,408 · Granted Mar 10, 2009

Denitrification catalyst regeneration method

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Quick Facts
Patent No.
US 7,501,106
App. No.
10/994,408
Granted
Mar 10, 2009
Kind
B2
Abstract

A denitrification catalyst regeneration method comprises heat-treating a used denitrification catalyst, then cleaning the denitrification catalyst with an aqueous solution of oxalic acid, and then finish washing the denitrification catalyst with water to regenerate the denitrification catalyst.

Claims (12)

1. A denitrification catalyst regeneration method, comprising:

denitrifying exhaust gas produced by the combustion of ultraheavy oil with the sulfur content of 1% or higher by a denitrification catalyst;

then applying heat-treatment to the used denitrification catalyst to transform substantially all vanadium oxysulfate deposited on the denitrification catalyst into vanadium pentoxide;

then cleaning said denitrification catalyst with an aqueous solution of oxalic acid; and

then finish washing said denitrification catalyst with water to regenerate said denitrification catalyst.

2. The denitrification catalyst regeneration method according to claim 1 , further comprising:

performing said heat-treatment;

then roughly washing said denitrification catalyst with water; and

then cleaning said denitrification catalyst with an aqueous solution of oxalic acid.

3. The denitrification catalyst regeneration method according to claim 1 , wherein an oxalic acid concentration of said aqueous solution of oxalic acid is 4 to 25% by weight.

4. The denitrification catalyst regeneration method according to claim 2 , wherein an oxalic acid concentration of said aqueous solution of oxalic acid is 0.5 to 25% by weight.

5. The denitrification catalyst regeneration method according to claim 1 , wherein a temperature of said heat-treatment is 450 to 600° C.

Assignments (3)
CORRECTIVE ASSIGNMENT TO CORRECT THE REMOVING PATENT APPLICATION NUMBER 11921683 PREVIOUSLY RECORDED AT REEL: 054975 FRAME: 0438. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded May 26, 2023
From: MITSUBISHI HITACHI POWER SYSTEMS, LTD.
To: MITSUBISHI POWER, LTD.
Reel/Frame 063787/0867 →
CHANGE OF NAME Recorded Jan 13, 2021
From: MITSUBISHI HITACHI POWER SYSTEMS, LTD.
To: MITSUBISHI POWER, LTD.
Reel/Frame 054975/0438 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 26, 2015
From: MITSUBISHI HEAVY INDUSTRIES, LTD.
To: MITSUBISHI HITACHI POWER SYSTEMS, LTD.
Reel/Frame 035101/0029 →