IP Library Granted Patent US 8,309,061
Granted Patent B2
US 8,309,061 · App. 11/078,263 · Granted Nov 13, 2012

Formulations and methods for treating rhinosinusitis

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Quick Facts
Patent No.
US 8,309,061
App. No.
11/078,263
Granted
Nov 13, 2012
Kind
B2
Abstract

The invention involves methods and formulations for treating or preventing rhinosinusitis, including but not limited to, bacterial-induced, viral-induced and/or fungus-induced rhinosinusitis in mammals, and/or rhinosinusitis not induced by an infective agent, such as bacteria, fungus or virus. In one embodiment, the formulation of the present invention comprises an anti-inflammatory agent (e.g. fluticasone propionate) having a specific particle size distribution profile. The formulation may also comprise an antifungal agent, antibiotic or antiviral agent.

Claims (51)

1. A formulation for the treatment of symptoms associated with rhinosinusitis in a mammal suffering from rhinosinusitis, the formulation comprising an aqueous suspension comprising:

(a) about 10 mcg to about 2000 mcg of an anti-inflammatory agent, the anti-inflammatory agent comprises suspended solid particles of fluticasone or pharmaceutically acceptable salt thereof, said suspended solid particles of fluticasone comprise the following particle size distribution profile:

i. about 10% of the anti-inflammatory particles has an average particle size of less than 0.40 microns;

ii. about 25% of the anti-inflammatory particles have an average particle size of less than 0.8 microns;

iii. about 50% of the anti-inflammatory particles have an average particle size of less than 1.5 microns;

iv. about 75% of the anti-inflammatory particles have an average particle size of less than 3.0 microns; and

v. about 90% of the anti-inflammatory particles have an average particle size distribution of less than 5.3 microns; and

(b) an antifungal agent, wherein the formulation is suitable for administration by the intranasal route of the mammal; wherein the formulation is sterile and free of benzalkonium chloride.

2. A formulation for the treatment of symptoms associated with rhinosinusitis in a mammal suffering from said rhinosinusitis, the formulation comprising an aqueous suspension comprising:

(a) about 10 mcg to about 2000 mcg of an anti-inflammatory agent, the anti-inflammatory agent comprises suspended solid particles of beclomethasone or pharmaceutically acceptable salt thereof, said suspended solid particles of beclomethasone comprise the following particle size distribution profile:

i. about 10% of the anti-inflammatory particles has an average particle size of less than 0.30 microns;

ii. about 25% of the anti-inflammatory particles have an average particle size of less than 0.55 microns;

iii. about 50% of the anti-inflammatory particles have an average particle size of less than 1.1 microns; and

iv. about 75% of the anti-inflammatory particles have an average particle size of less than 1.8 microns; and

v. about 90% of the anti-inflammatory particles have an average particle size distribution of less than 2.7 microns; and

(b) an antifungal agent, wherein the formulation is suitable for administration by the intranasal route of the mammal; wherein the formulation is sterile and free of benzalkonium chloride.

3. The formulation of claims 1 or 2 , comprising about 25 mcg to about 400 mcg of the anti-inflammatory agent.

4. The formulation of claims 1 or 2 , comprising about 75 to about 300 mcg of the anti-inflammatory agent.

5. The formulation of claims 1 or 2 , comprising about 200 mcg of the anti-inflammatory agent, and wherein the formulation is sterile and free of benzalkonium chloride yet has a relatively long period of stability such that after storage for 12 months at a temperature between 15 to 30° C., greater than 80% of the anti-inflammatory agent and greater than 80% of the antifungal agent originally present in the formulation still remains in the formulation.

6. A formulation for the treatment of symptoms associated with rhinosinusitis in a mammal suffering thereof, the formulation comprises an aqueous suspension that comprises an anti-inflammatory agent, the anti-inflammatory agent comprises 0.04% to 0.06% by weight of suspended solid particles of fluticasone or pharmaceutically acceptable salt thereof, said suspended solid particles of fluticasone comprise the following particle size distribution profile:

i. about 10% of the anti-inflammatory particles have an average particle size of less than 0.40 microns;

ii. about 25% of the anti-inflammatory particles have an average particle size of less than 0.8 microns;

iii. about 50% of anti-inflammatory particles have an average particle size of less than 1.5 microns;

iv. about 75% of the anti-inflammatory particles have a particle size of less than 3.0 microns;

v. about 90% of the anti-inflammatory particles have a particle size of less than 5.3 microns;

an antifungal agent, wherein the formulation is suitable for the administration by the intranasal route of the mammal; wherein the formulation is sterile and free of benzalkonium chloride.

7. A formulation for the treatment of symptoms associated with rhinosinusitis in a mammal suffering thereof, the formulation comprises an aqueous suspension that comprises an anti-inflammatory agent, the anti-inflammatory agent comprises 0.04% to 0.05% by weight of suspended solid particles of beclomethasone or pharmaceutically acceptable salt thereof, said suspended solid particles of beclomethasone comprise the following particle size distribution profile:

i. about 10% of the anti-inflammatory particles have an average particle size of less than 0.30 microns;

ii. about 25% of anti-inflammatory particles have an average particle size of less than 0.55 microns;

iii. about 50% of the anti-inflammatory particles have an average particle size of less than 1.1 microns;

iv. about 75% of the anti-inflammatory particles have a particle size of less than 1.8 microns;

v. about 90% of the anti-inflammatory particles have a particle size of less than 2.7 microns;

an antifungal agent, wherein the formulation is suitable for the administration by the intranasal route of the mammal; wherein the formulation is sterile and free of benzalkonium chloride.

8. The formulations of claims 6 or 7 , comprising about 25 mcg to about 400 mcg of the anti-inflammatory agent.

9. The formulation of claims 6 or 7 , comprising about 75 mcg to about 300 mcg of the anti-inflammatory agent.

10. The formulations of claims 6 or 7 , comprising about 200 mcg of said anti-inflammatory agent.

11. The formulations of claims 9 or 10 , wherein the formulation is sterile and free of benzalkonium chloride yet has a relatively long period of stability such that after storage for 12 months at a temperature between 15 to 30° C., greater than 95% of the anti-inflammatory agent and greater than 95% of the antifungal agent originally present in the formulation still remains in the formulation.

12. The formulations of claims 9 or 10 , wherein the formulation is suitable for intranasal administration by a spray pump, by nebulization or metered dose spray pump.

13. The formulation of claims 1 , 2 , 9 or 10 , further comprising about 0.01% to about 90% by weight on a dried weight basis of one or more of the following compounds:

(a) polysorbate 80;

(b) disodium edetate dihydrate, USP;

(c) sodium citrate dihydrate, USP;

(d) sodium chloride, USP; and

(e) purified water, USP.

14. The formulation of claim 13 , wherein the:

(a) polysorbate 80 is present in an amount of about 0.4 mg/ml;

(b) disodium edetate dihydrate, USP is present in an amount of about 1 mg/ml;

(c) sodium citrate dihydrate, USP is present in an amount of about 0.065 mg/ml; and

(d) sodium chloride, USP is present in an amount of about 8.8 mg/ml.

15. The formulation of claim 13 , wherein said formulation is a sterile aqueous suspension suitable for administration to the nasal-paranasal mucosa.

16. The formulations of claims 9 or 10 , further comprising an antiviral agent.

Assignments (7)
ADDRESS CHANGE Recorded Mar 15, 2022
From: MYLAN SPECIALTY L.P.
To: MYLAN SPECIALTY L.P.
Reel/Frame 059366/0851 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 24, 2013
From: DEY PHARMA, L.P.
To: MYLAN SPECIALTY L.P.
Reel/Frame 030482/0242 →
PATENT RELEASE Recorded Dec 10, 2012
From: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
To: DEY PHARMA L.P. (F/K/A DEY, L.P.); MYLAN PHARMACEUTICALS, INC.; MYLAN BERTEK PHARMACEUTICALS INC.; MYLAN TECHNOLOGIES, INC.; SOMERSET PHARMACEUTICALS, INC.; MYLAN INSTITUTIONAL INC. (F/K/A UDL LABORATORIES, INC.); MYLAN INC.
Reel/Frame 029440/0967 →
CHANGE OF NAME Recorded Dec 8, 2011
From: DEY, L.P.
To: DEY PHARMA, L.P.
Reel/Frame 027351/0334 →
SECURITY AGREEMENT Recorded Nov 21, 2011
From: MYLAN PHARMACEUTICALS, INC.; MYLAN BERTEK PHARMACEUTICALS INC.; MYLAN TECHNOLOGIES, INC.; MYLAN INSTITUTIONAL INC. (F/K/A UDL LABORATORIES, INC.); SOMERSET PHARMACEUTICALS, INC.; DEY PHARMA, L.P. (F/K/A DEY L.P.)
To: BANK OF AMERICA, N.A., AS COLLATERAL AGENT
Reel/Frame 027270/0799 →
RELEASE OF SECURITY INTEREST Recorded Nov 18, 2011
From: JPMORGAN CHASE BANK, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
To: MYLAN TECHNOLOGIES, INC.; DEY, INC. (F/K/A DEY LABORATORIES, INC.); MYLAN BERTEK PHARMACEUTICALS INC.; MYLAN PHARMACEUTICALS, INC.; DEY PHARMA, L.P. (F/K/A DEY L.P.); MYLAN INSTITUTION INC. (F/K/A UDL LABORATORIES, INC.); MYLAN INC. (F/K/A MYLAN LABORATORIES INC.)
Reel/Frame 027261/0928 →
SECURITY AGREEMENT Recorded Oct 24, 2007
From: MYLAN LABORATORIES INC.; DEY, L.P.; DEY, INC.; MYLAN PHARMACEUTICALS, INC.; MYLAN TECHNOLOGIES, INC.; MYLAN BERTEK PHARMACEUTICALS INC.; UDL LABORATORIES, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 020004/0404 →