IP Library Granted Patent US 7,601,858
Granted Patent B2
US 7,601,858 · App. 11/122,859 · Granted Oct 13, 2009

Method of processing ethanol byproducts and related subsystems

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Quick Facts
Patent No.
US 7,601,858
App. No.
11/122,859
Granted
Oct 13, 2009
Kind
B2
Abstract

In one aspect of the invention, a method recovers oil from a concentrated byproduct, such as evaporated thin stillage formed during a dry milling process used for producing ethanol. The method includes forming a concentrate from the byproduct and recovering oil from the concentrate. The step of forming the concentrate may comprise evaporating the byproduct. Further, the step of separating the oil from the concentrate may comprise using a centrifuge and, in particular, a disk stack centrifuge. Other aspects of the invention include related methods and subsystems for recovering oil from thin stillage.

Claims (18)

1. A method of recovering oil from thin stillage, the method comprising, in sequence:

evaporating the thin stillage to remove water and form a concentrated byproduct; and

recovering oil from the concentrated byproduct by heating and mechanically processing the concentrated byproduct to separate the oil from the concentrated byproduct, wherein the concentrated byproduct has a moisture content of greater than 30% and less than 90% by weight.

2. The method of claim 1 , wherein the mechanical processing comprises separating the oil from the concentrated byproduct using a disk stack centrifuge.

3. The method of claim 1 , wherein the recovering step is performed on the concentrated byproduct at a temperature of between about 150 and 212° F.

4. The method of claim 1 , wherein the recovering step is performed on the concentrated byproduct at a temperature of about 180° F.

5. The method of claim 1 , wherein the recovering step is performed on the concentrated byproduct having a pH of between about 3 and 6.

6. The method of claim 1 , wherein the recovering step is performed on the concentrated byproduct having a pH of between about 3.5 and 4.5.

7. The method of claim 1 , wherein the concentrated byproduct has a moisture content between about 60-85%.

8. A method of recovering oil from thin stillage, comprising, in sequence: evaporating the thin stillage to create a concentrate having a moisture content of greater than 30% by weight and less than about 90% by weight; and centrifuging the concentrate to recover oil.

9. The method according to claim 8 , wherein the step of centrifuging the concentrate comprises using a disk stack centrifuge.

10. A method of processing whole stillage, comprising: recovering thin stillage from the whole stillage, the thin stillage including oil and solids; concentrating the thin stillage including the solids to produce a thin stillage concentrate, wherein the thin stillage concentrate has a moisture content of greater than 30% and less than 90% by weight; and recovering oil from the concentrate by a process consisting essentially of heating and mechanically processing the concentrate to separate the oil from the concentrate.

11. The method of claim 10 , wherein the step of recovering the thin stillage includes using a separator selected from the group consisting of a press, extruder, a decanter centrifuge, and a screen centrifuge.

12. The method of claim 10 , wherein the concentrating step comprises processing the thin stillage to a temperature of between about 150 and 212° F., a pH of between about 3 and 6.

13. The method of claim 10 , wherein the step of recovering oil comprises separating the oil from the concentrate using a centrifuge.

14. The method of claim 10 , wherein the recovering and concentrating steps are performed in a continuous fashion.

15. The method of claim 10 , further including the step of drying the concentrate after the step of recovering the oil.

16. In a method for processing corn to produce ethanol and concentrated thin stillage, the improvement comprising the step of recovering a product consisting essentially of oil from the concentrated thin stillage by heating and mechanically processing the concentrated thin stillage to separate the oil from the concentrated thin stillage.

Assignments (9)
SECURITY AGREEMENT Recorded Jan 8, 2013
From: ECOSYSTEM TECHNOLOGIES, LLC; GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS AGRIFUELS CORPORATION; GS BIG MANAGEMENT, LLC; GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS COES (ADRIAN I), LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS GLOBAL BIODIESEL, LLC; GS RENTALS, LLC (F/K/A WARNECKE RENTALS, LLC); GS TECHNOLOGY, LLC; GREENSHIFT ENGINEERING, INC. (F/K/A GS CARBON DIOXIDE TECHNOLOGIES, INC.); NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL, INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS, LLC; VIRIDIS CAPITAL LLC
To: YA GLOBAL INVESTMENTS, L.P., AS COLLATERAL AGENT
Reel/Frame 029588/0092 →
SECURITY AGREEMENT Recorded Nov 16, 2009
From: VIRIDIUS CAPITAL LLC; CARBONICS CAPITAL CORPORATION; GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS RENTAL, LLC (F/K/A WARNECKE RENTALS, LLC); GS CARBON DIOXIDE TECHNOLOGIES, INC.; GS AGRIFUELS CORPORATION; NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS LLC; GS GLOBAL BIODIESEL, LLC; BOLLHEIMER & ASSOCIATES, INC.; GS BIG MANAGEMENT, LLC; GS COES (ADRIAN I), LLC; GS TECHNOLOGY, LLC; ECOSYSTEM TECHNOLOGIES, LLC
To: YA GLOBAL INVESTMENTS, L.P.
Reel/Frame 023524/0728 →
CORRECTIVE ASSIGNMENT TO CORRECT THE SERIAL NUMBER PREVIOUSLY RECORDED ON REEL 023163 FRAMAE 0954. Recorded Sep 15, 2009
From: VIRIDIS CAPITAL LLC; CARBONICS CAPITAL CORPORATION; GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS GLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE), LLC; GS CARBON DIOXIDE TECHNOLOGIES, INC.; GS GLOBAL BIODIESEL, LLC; GS AGRIFUELS CORPORATION; NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEM LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS RENTAL LLC (F/K/A WARNECKE RENTALS, LLC); BOLLHEIMER & ASSOCIATES, INC.; ECOSYSTEM TECHNOLOGIES, LLC; GS BIG MANAGEMENT LLC; GS COES (ADRIAN I), LLC; GS TECHNOLOGY, LLC
To: YA GLOBAL INVESTMENTS, L.P.
Reel/Frame 023232/0189 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 15, 2009
From: GS ETHANOL TECHNOLOGIES, INC.
To: GS CLEANTECH CORPORATION
Reel/Frame 022691/0639 →
SECURITY AGREEMENT Recorded Feb 5, 2008
From: VIRIDIS CAPITAL LLC; GREENSHIFT CORPORATION; GS AGRIFUELS CORPORATION; GS CLEANTECH CORPORATION (F/K/A VERIDIUM CORPORATION); GS ETHANOL TECHNOLOGIES, INC.; GS COES (YORKVILLE I), LLC; GS ENERGY CORPORATION; WARNECKE DESIGN SERVICE, INC.; WARNECKE RENTALS, LLC; GS CARBON DIOXIDE TECHNOLOGIES, INC.; GS ENVIROSERVICES, INC.; ENVIRO-SAFE CORP.; ENVIRO-SAFE CORPORATION (NE); NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS LLC
To: YA GLOBAL INVESTMENTS, L.P. (F/K/A CORNELL CAPITAL PARTNERS, L.P.)
Reel/Frame 020462/0956 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 17, 2007
From: MEAN GREEN BIOFUELS OF GEORGIA, LLC
To: GS ETHANOL TECHNOLOGIES, INC.
Reel/Frame 019308/0266 →
CHANGE OF NAME Recorded Apr 25, 2007
From: CANTRELL WINSNESS TECHNOLOGIES, LLC
To: MEAN GREEN BIOFUELS OF GEORGIA, LLC
Reel/Frame 019250/0160 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 13, 2007
From: ETHANOL OIL RECOVERY SYSTEMS LLC
To: CANTRELL WINSNESS TECHNOLOGIES, LLC
Reel/Frame 019002/0374 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 13, 2005
From: WINSNESS, DAVID J.; CANTRELL, DAVID FRED
To: ETHANOL OIL RECOVERY SYSTEMS LLC
Reel/Frame 016252/0954 →