IP Library Granted Patent US 7,247,632
Granted Patent B2
US 7,247,632 · App. 11/151,897 · Granted Jul 24, 2007

N-sulfonyl-4-methyleneamino-3-hydroxy-2-pyridones

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Quick Facts
Patent No.
US 7,247,632
App. No.
11/151,897
Granted
Jul 24, 2007
Kind
B2
Abstract

Compounds of Formula (I) are effective in the treatment of a microbial infection.

Claims (31)

1. A compound of formula (I):

wherein:

a. R 1 is aryl, optionally substituted with one or more hydrogen, halo, cyano, hydroxy, carboxy, keto, thioketo, amino, acylamino, acyl, amido, phenyl, aryloxy, alkyl, alkenyl, alkynyl, heteroalkyl, haloalkyl, alkoxy, aryl, cycloalkyl, spirocycloalkyl or combinations thereof;

b. each R 2 is independently chosen from hydrogen, halo, cyano, hydroxy, carboxy, keto, thioketo, amino, acylamino, acyl, amido, phenyl, aryloxy, alkyl, alkenyl, alkynyl, beteroalkyl, haloalkyl, alkoxy, aryl, and cycloalkyl;

c. R 3 and R 4 , together with the nitrogen atom to which they are bonded, join to form a piperazine ring substituted with a pyridazine ring or one or more hydrogen, halo, cyano, hydroxy, carboxy, keto, thioketo, amino, acylamino, acyl, amido, alkyl, alkenyl, alkynyl, heteroalkyl, haloalkyl, alkoxy, or combinations thereof; and

d. R 5 and R 6 are each independently chosen from hydrogen, halo, cyano, hydroxy, carboxy, keto, thioketo, amino, acylamino, acyl, amido, phenyl, aryloxy, alkyl, alkenyl, alkynyl, heteroalkyl, haloalkyl, alkoxy, aryl, and cycloalkyl; or

optical isomers, diastereomers and enantiomers of the formula above, or a pharmaceutically-acceptable salt thereof.

2. The compound of claim 1 , wherein R 1 is substituted or unsubstituted phenyl.

3. The compound of claim 2 , wherein the phenyl group of R 1 is substituted with an alkyl.

4. The compound of claim 1 , wherein R 1 is aryl substituted with a heteroalkyl.

5. The compound of claim 1 , wherein R 1 is aryl substituted with an aryl.

6. The compound of claim 1 , wherein R 1 is aryl substituted with an aryloxy.

7. The compound of claim 1 , wherein R 2 is hydrogen.

8. The compound of claim 1 , wherein R 5 and R 6 are hydrogen.

9. The compound of claim 1 , chosen from:

3-Hydroxy-4-(4-phenylpiperazin-1-ylmethyl)-1-(toluene-4-sulfonyl)-1H-pyridin-2-one; and

4-[4-(6-Chloropyridazin-3-yl)piperazin-1-ylmethyl]-3-hydroxy-1-(toluene-4-sulfonyl)-1H-pyridin-2-one.

10. A method of treating a microbial infection comprising administering a safe and effective of amount of a compound according to claim 1 , in a subject in need thereof.

11. A method of treating a microbial infection comprising administering a safe and effective of amount of a compound according to claim 9 , in a subject in need thereof.

12. A pharmaceutical composition comprising:

a. a safe and effective of amount of a compound according to claim 1 ;

b. a pharmaceutically-acceptable excipient.

13. A pharmaceutical composition comprising:

a. a safe and effective of amount of a compound according to claim 9 ;

b. a pharmaceutically-acceptable excipient.

14. The compound of claim 1 , wherein R 1 , R 2 , R 5 , and R 6 are hydrogen.

15. The compound of claim 9 , which is 4-[4-(6-Chloropyridazin -3-yl)piperazin-1-ylmethyl]-3-hydroxy-1-(toluene-4-sulfonyl) -1H-pyridin-2-one.

16. A method of treating a microbial infection comprising administering a safe and effective of amount of a compound according to claim 15 , in a subject in need thereof.

17. A pharmaceutical composition comprising:

a. a safe and effective of amount of a compound according to claim 15 ;

b. a pharmaceutically-acceptable excipient.

Assignments (8)
RELEASE OF SECURITY INTEREST Recorded Oct 31, 2013
From: BANK OF AMERICA, N.A., AS COLLATERAL AGENT
To: WARNER CHILCOTT COMPANY, LLC
Reel/Frame 031531/0538 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 2, 2012
From: AKEBIA THERAPEUTICS, INC.
To: AERPIO THERAPEUTICS, INC.
Reel/Frame 027801/0378 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 27, 2011
From: WARNER CHILCOTT COMPANY, LLC
To: AKEBIA THERAPEUTICS INC.
Reel/Frame 027445/0100 →
PATENT RELEASE Recorded Dec 23, 2011
From: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
To: WARNER CHILCOTT COMPANY, LLC
Reel/Frame 027443/0164 →
SECURITY AGREEMENT Recorded Mar 30, 2011
From: WARNER CHILCOTT COMPANY LLC
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 026064/0607 →
RELEASE - REEL 023456, FRAME 0052 Recorded Mar 29, 2011
From: CREDIT SUISSSE AG, CAYMAN ISLANDS BRANCH, AS ADMINISTRATIVE AGENT
To: WARNER CHILCOTT COMPANY LLC
Reel/Frame 026042/0046 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 8, 2010
From: PROCTER & GAMBLE COMPANY, THE
To: WARNER CHILCOTT COMPANY, LLC
Reel/Frame 023796/0417 →
SECURITY AGREEMENT Recorded Nov 2, 2009
From: WARNER CHILCOTT COMPANY, LLC
To: CREDIT SUISSE, CAYMAN ISLANDS BRANCH, AS ADMINISTRATIVE AGENT
Reel/Frame 023456/0052 →