IP Library Granted Patent US 8,192,759
Granted Patent B2
US 8,192,759 · App. 11/179,425 · Granted Jun 5, 2012

Matrix made of polyester polymers entangled with hyaluronic polymers useful for supporting tissue repair

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Quick Facts
Patent No.
US 8,192,759
App. No.
11/179,425
Granted
Jun 5, 2012
Kind
B2
Abstract

The present application discloses matrix compositions to support the repair of tissue defects such as an osteochondral injury. A matrix described herein comprises a polyester polymer entangled with a polysaccharide polymer. Also disclosed are methods of preparing a matrix, and methods of using a matrix in the repair of tissue. In certain configurations, a matrix can comprise a polyester cross-linked with a polysaccharide, which can be an oxidized polysaccharide. In some configurations, a matrix can further comprise one or more additional components, such as a growth factor.

Claims (17)

1. A matrix for supporting repair of bone or cartilage comprising polyester polymers entangled with hyaluronic acid polymers, said matrix being formed by the steps of:

(i) dissolving polyester polymers in an organic solvent;

(ii) blending the polyester polymers with hyaluronic acid polymers contained in an aqueous medium to form an emulsified mixture;

(iii) pouring the emulsified mixture of the two polymers into a mold, and

(iv) successively removing the organic solvent and water from the mold; wherein said matrix is characterized by (i) retention of pore structure and shape when hydrated and (ii) the ability to support the growth of cells in vivo or ex vivo.

2. A matrix in accordance with claim 1 , wherein the polyester polymers are selected from the group consisting of polylactic acid, polyglycolic acid, and a co-polymer comprising polylactic acid and polyglycolic acid.

3. A matrix in accordance with claim 1 , wherein the polyester polymers comprise a co-polymer comprising polylactic acid and polyglycolic acid.

4. A matrix in accordance with claim 3 , wherein the polylactic acid and the polyglycolic acid are in a weight ratio of about 5:1 to about 2:1.

5. A matrix in accordance with claim 4 , wherein the weight ratio of polylactic acid to polyglycolic acid is about 3:1.

6. A matrix in accordance with claim 1 , wherein the hyaluronic acid polymers are oxidized.

7. A matrix in accordance with claim 1 , wherein the hyaluronic acid polymers are covalently crosslinked.

8. A matrix in accordance with claim 1 , wherein the polyester polymers and the hyaluronic acid polymers are in a weight ratio of from 99:1 to 1:99.

9. A matrix in accordance with claim 8 , wherein the polyester polymers comprise a co-polymer comprising polylactic acid and polyglycolic acid, wherein the weight ratio of the co-polymer to the hyaluronic acid polymers is from about 9:1 to about 1:9.

10. A matrix in accordance with claim 1 , further comprising at least one growth factor.

11. A matrix in accordance with claim 10 , wherein the at least one growth factor is selected from the group consisting of a TGF-β, a bone morphogenetic protein, a growth differentiation factor, ADMP-1, a fibroblast growth factor, a hedgehog protein, an insulin-like growth factor, a platelet-derived growth factor, an interleukin, a colony-stimulating factor, and an activin.

12. A matrix in accordance with claim 10 , wherein the at least one growth factor is a bone morphogenetic protein.

13. A matrix in accordance with claim 1 , further comprising at least one collagen.

Assignments (10)
SECURITY INTEREST Recorded Sep 18, 2025
From: ISTO TECHNOLOGIES II, LLC; ADVANCED BIOLOGICS LLC,; ARTERIOCYTE MEDICAL SYSTEMS, INC.; THERACELL, LLC
To: GOLUB CAPITAL MARKETS LLC
Reel/Frame 072300/0216 →
RELEASE OF SECURITY INTEREST Recorded Sep 16, 2025
From: BARINGS FINANCE LLC, AS COLLATERAL AGENT
To: ARTERIOCYTE MEDICAL SYSTEMS, INC.; ISTO TECHNOLOGIES II, LLC; THERACELL, LLC; ADVANCED BIOLOGICS, LLC; BIOLOGICA TECHNOLOGIES, LLC
Reel/Frame 072274/0408 →
RELEASE OF SECURITY INTEREST Recorded Oct 18, 2023
From: TWIN BROOK CAPITAL PARTNERS, LLC
To: ISTO TECHNOLOGIES II, LLC
Reel/Frame 065269/0604 →
SECURITY INTEREST Recorded Oct 18, 2023
From: ARTERIOCYTE MEDICAL SYSTEMS, INC.; ISTO TECHNOLOGIES II, LLC; THERACELL, LLC; ADVANCED BIOLOGICS, LLC; BIOLOGICA TECHNOLOGIES, LLC
To: BARINGS FINANCE LLC, AS COLLATERAL AGENT
Reel/Frame 065271/0059 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 9, 2018
From: ISTO TECHNOLOGIES, INC.
To: ISTO TECHNOLOGIES II, LLC
Reel/Frame 045478/0013 →
SECURITY INTEREST Recorded Jun 15, 2017
From: ISTO TECHNOLOGIES II, LLC
To: TWIN BROOK CAPITAL PARTNERS, LLC, AS AGENT
Reel/Frame 042727/0459 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2016
From: MIDCAP FUNDING XVIII TRUST, AS SUCCESSOR IN INTEREST TO MIDCAP FINANCIAL SBIC, LP
To: ISTO TECHNOLOGIES, INC.
Reel/Frame 038903/0645 →
SECURITY INTEREST Recorded Jan 23, 2015
From: ISTO TECHNOLOGIES, INC.
To: MIDCAP FINANCIAL SBIC, LP
Reel/Frame 034805/0001 →
RELEASE OF SECURITY INTEREST Recorded Jun 22, 2010
From: VELOCITY VENTURE FUNDING, L.L.C.
To: ISTO TECHNOLOGIES, INC.
Reel/Frame 024563/0606 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 10, 2008
From: ISTO TECHNOLOGIES, INC., A DELAWARE CORP.
To: VELOCITY FINANCIAL GROUP INC., ITS SUCCESSORS AND ASSIGNS
Reel/Frame 021805/0354 →