IP Library Granted Patent US 8,008,516
Granted Patent B2
US 8,008,516 · App. 11/241,231 · Granted Aug 30, 2011

Method of processing ethanol byproducts and related subsystems

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Quick Facts
Patent No.
US 8,008,516
App. No.
11/241,231
Granted
Aug 30, 2011
Kind
B2
Abstract

In one aspect of the invention, a method recovers oil from a concentrated byproduct, such as evaporated thin stillage formed during a dry milling process used for producing ethanol. The method includes forming a concentrate from the byproduct and recovering oil from the concentrate. The step of forming the concentrate may comprise evaporating the byproduct. Further, the step of separating the oil from the concentrate may comprise using a centrifuge and, in particular, a disk stack centrifuge. Other aspects of the invention include related methods and subsystems for recovering oil from thin stillage.

Claims (17)

1. A method of recovering oil from thin stillage; the method consisting essentially of, in sequence:

evaporating water from the thin stillage to form a thin stillage concentrate, wherein the thin stillage concentrate has a moisture content of greater than 30% and less than 90% by weight before the recovering step;

mechanically processing the thin stillage concentrate to separate oil from the thin stillage concentrate; and

recovering the separated oil.

2. The method of claim 1 , wherein the thin stillage concentrate has a moisture content of greater than 60% and less than 85% by weight before the recovering step.

3. The method of claim 1 , wherein the thin stillage concentrate has a pH of between about 3 and 6.

4. The method of claim 1 , wherein the thin stillage concentrate has a pH of between about 3.5 and 4.5.

5. The method of claim 1 , wherein mechanically processing further comprises heating the thin stillage concentrate to a temperature between 150° F. and 212° F.

6. The method of claim 1 , wherein mechanically processing further comprises heating the thin stillage concentrate to a temperature between 150° F. and 212° F. and a pH between 3 and 6.

7. A method of processing whole stillage, comprising, in sequence:

separating distiller wet grains and thin stillage from the whole stillage, the thin stillage including oil and solids;

concentrating the thin stillage including the solids to form a concentrate having a moisture content of greater than 30% and less than 90% by weight; and

disc stack centrifuging oil from the thin stillage concentrate to form a substantially oil free concentrate.

8. The method of claim 7 , wherein the concentrating step comprises processing the thin stillage a pH of between about 3 and 6, and a moisture content of less than 90%.

9. The method of claim 7 , wherein the recovering and concentrating steps are performed in a continuous fashion.

10. The method of claim 7 , further including the step of drying the concentrate after the step of recovering the oil.

11. The method of recovering oil from thin stillage of claim 1 , wherein mechanically processing comprises disc stack centrifuging the thin stillage concentrate.

Assignments (6)
SECURITY AGREEMENT Recorded Jan 8, 2013
From: ECOSYSTEM TECHNOLOGIES, LLC; GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS AGRIFUELS CORPORATION; GS BIG MANAGEMENT, LLC; GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS COES (ADRIAN I), LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS GLOBAL BIODIESEL, LLC; GS RENTALS, LLC (F/K/A WARNECKE RENTALS, LLC); GS TECHNOLOGY, LLC; GREENSHIFT ENGINEERING, INC. (F/K/A GS CARBON DIOXIDE TECHNOLOGIES, INC.); NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL, INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS, LLC; VIRIDIS CAPITAL LLC
To: YA GLOBAL INVESTMENTS, L.P., AS COLLATERAL AGENT
Reel/Frame 029588/0092 →
SECURITY AGREEMENT Recorded Mar 16, 2012
From: VIRIDIUS CAPITAL LLC; GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS RENTALS, LLC (F/K/A WARNECKE RENTALS, LLC); GREENSHIFT ENGINEERING, INC.; GS AGRIFUELS CORPORATION; NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS LLC; GS GLOBAL BIODIESEL, LLC; GS BIG MANAGMENT, LLC; GS COES (ADRIAN I), LLC; GS TECHNOLOGY, LLC; ECOSYSTEM TECHNOLOGIES, LLC
To: YA GLOBAL INVESTMENTS, L.P.
Reel/Frame 027876/0153 →
SECURITY AGREEMENT Recorded Aug 31, 2010
From: VIRIDIUS CAPITAL LLC; CARBONICS CAPITAL CORPORATION (F/K/A GREENSHIFT CORPORATION); GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS RENTALS, LLC (F/K/A WARNECKE RENTALS, LLC); GS CARBON DIOXIDE TECHNOLOGIES, INC.; GS AGRIFUELS CORPORATION; NEXTGEN, ACQUISITION, INC.; NEXTGEN FUEL INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS, LLC; GS GLOBAL BIODIESEL, LLC; GS BIG MANAGEMENT, LLC; GS COES (ADRIAN I), LLC; GS TECHNOLOGY, LLC; ECOSYSTEM TECHNOLOGIES, LLC
To: YA GLOBAL INVESTMENTS, L.P.
Reel/Frame 024920/0795 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 14, 2009
From: WINSNESS, DAVID J.; CANTRELL, DAVID FRED
To: GS CLEANTECH CORPORATION
Reel/Frame 023225/0020 →
SECURITY AGREEMENT Recorded Sep 1, 2009
From: VIRIDIS CAPITAL LLC; CARBONICS CAPITAL CORPORATION (F/K/A GREENSHIFT CORPORATION); GREENSHIFT CORPORATION (F/K/A GS CLEANTECH CORPORATION); GS CLEANTECH CORPORATION (F/K/A GS ETHANOL TECHNOLOGIES, INC.); GS COES (YORKVILLE I), LLC; GS CARBON DIOXIDE TECHNOLOGIES, INC.; GS GLOBAL BIODIESEL, LLC; GS AGRIFUELS CORPORATION; NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS LLC; GS DESIGN, INC. (F/K/A WARNECKE DESIGN SERVICE, INC.); GS RENTALS LLC (F/K/A WARNECKE RENTALS, LLC); BOLLHEIMER & ASSOCIATES, INC.; ECOSYSTEM TECHNOLOGIES, LLC; GS BIG MANAGEMENT, LLC; GS COES (ADRIAN I), LLC; GS TECHNOLOGY, LLC
To: YA GLOBAL INVESTMENTS, L.P.
Reel/Frame 023163/0954 →
SECURITY AGREEMENT Recorded Feb 5, 2008
From: VIRIDIS CAPITAL LLC; GREENSHIFT CORPORATION; GS AGRIFUELS CORPORATION; GS CLEANTECH CORPORATION (F/K/A VERIDIUM CORPORATION); GS ETHANOL TECHNOLOGIES, INC.; GS COES (YORKVILLE I), LLC; GS ENERGY CORPORATION; WARNECKE DESIGN SERVICE, INC.; WARNECKE RENTALS, LLC; GS CARBON DIOXIDE TECHNOLOGIES, INC.; GS ENVIROSERVICES, INC.; ENVIRO-SAFE CORP.; ENVIRO-SAFE CORPORATION (NE); NEXTGEN ACQUISITION, INC.; NEXTGEN FUEL INC.; SUSTAINABLE SYSTEMS, INC.; SUSTAINABLE SYSTEMS LLC
To: YA GLOBAL INVESTMENTS, L.P. (F/K/A CORNELL CAPITAL PARTNERS, L.P.)
Reel/Frame 020462/0956 →