IP Library Granted Patent US 7,507,972
Granted Patent B2
US 7,507,972 · App. 11/247,016 · Granted Mar 24, 2009

Compact ionization source

Assignee: Owlstone Nanotech, Inc.
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Quick Facts
Patent No.
US 7,507,972
App. No.
11/247,016
Granted
Mar 24, 2009
Kind
B2
Abstract

A compact ionization source includes first and second electrodes, each having a plurality of fingers that are interdigitated with each other. The spacing between the first and second electrode, preferably less than 1 mm, creates a large electric field when a potential is applied across the first and second electrodes. The large electric field creates an ionization volume between the fingers of the first and second electrode and ionizes a portion of the molecules occupying the ionization volume. The interdigitated fingers of the first and second electrodes allow for a narrow gap separating the electrodes while presenting a large flow area for ionizing molecules for downstream analysis.

Claims (28)

1. An ionization source comprising:

a first electrode having a plurality of fingers;

a second electrode having a plurality of fingers, the plurality of fingers of the second electrode disposed between the plurality of fingers of the first electrode; and

a generator for applying a signal between the first and second electrodes, the signal generating an ionization volume between the first and second electrode; and

a diamond-like coating (DLC) layer deposited on the first and second electrodes wherein the DLC layer comprises n-doped tetrahedral amorphous carbon.

2. The ionization source of claim 1 , wherein a distance between the first electrode and the second electrode is between 100 μm and 1 μm.

3. The ionization source of claim 2 , wherein the distance between the first electrode and the second electrode is between 60 μm and 5 μm.

4. The ionization source of claim 3 , wherein the distance between the first electrode and the second electrode is between 40 μm and 10 μm.

5. The ionization source of claim 1 , further comprising a carbon nanotube layer disposed on a side of the first electrode facing a side of the second electrode.

6. The ionization source of claim 5 , wherein the carbon nanotube layer comprises a plurality of carbon nanotubes characterized by a longitudinal axis, the longitudinal axis parallel to a surface normal of the side of the first electrode.

7. The ionization source of claim 1 , wherein the DLC layer is deposited using a filtered cathodic vacuum arc (FCVA).

8. The ionization source of claim 1 , wherein the gap between the first and second electrodes forms a channel that is serpentine in cross-section.

9. An ionization source comprising:

a first electrode having a plurality of fingers, said electrode appearing comb shaped when seen from above; and

a second electrode having a plurality of fingers, said electrode appearing comb shaped when seen from above, the fingers of the second electrode interdigitated with the fingers of the first electrode with a gap between the first and second electrodes that is serpentine in cross-section;

wherein the first and second comb-shaped electrodes are oriented in a flow stream so that they are transverse to the direction of flow of the stream.

10. The ionization source of claim 9 , further comprising a deflector electrode disposed above and/or below the gap between the first and second electrodes to drive ions from between the electrodes to another location for analysis.

11. The ionization source of claim 9 , further comprising a voltage source which applies a voltage potential across the first and second electrodes.

12. The ionization source of claim 9 , further comprising a carbon nanotube layer disposed on a side of the first electrode facing a side of the second electrode.

13. The ionization source of claim 12 , wherein the carbon nanotube layer comprises a plurality of carbon nanotubes characterized by a longitudinal axis, the longitudinal access parallel to a surface normal of the side of the first electrode.

14. An ionization source comprising:

a first electrode having a plurality of substantially parallel planar fingers interconnected at one end; and

a second electrode having a plurality of substantially parallel planar fingers interconnected at one end, the fingers of the second electrode interdigitated with the fingers of the first electrode with a gap between the first and second electrodes;

wherein the first and second electrodes are oriented in a flow stream so that they are transverse to the direction of flow of the stream.

15. The ionization source of claim 14 , further comprising a deflector electrode disposed above and/or below the first and second electrodes to drive ions from between the electrodes to another location for analysis.

16. The ionization source of claim 14 , further comprising a voltage source which applies a voltage potential across the first and second electrodes.

17. The ionization source of claim 14 , further comprising a carbon nanotube layer disposed on a side of the first electrode facing a side of the second electrode.

18. The ionization source of claim 17 , wherein the carbon nanotube layer comprises a plurality of carbon nanotubes characterized by a longitudinal axis, the longitudinal access parallel to a surface normal of the side of the first electrode.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 30, 2016
From: OWLSTONE INC.
To: OWLSTONE MEDICAL LIMITED
Reel/Frame 038139/0701 →
RELEASE OF SECURITY INTEREST Recorded Mar 30, 2016
From: INGALLS & SNYDER LLC
To: OWLSTONE INC.
Reel/Frame 038140/0594 →
SECURITY AGREEMENT Recorded Apr 9, 2013
From: OWLSTONE INC.
To: INGALLS & SNYDER LLC, AS COLLATERAL AGENT
Reel/Frame 030175/0367 →
CHANGE OF NAME Recorded Mar 29, 2013
From: OWLSTONE NANOTECH INC.
To: OWLSTONE INC.
Reel/Frame 030112/0955 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 10, 2005
From: RUSH, MARTYN; BOLE, PAUL; RUIZ-ALONSO, DAVID; KOEHL, ANDREW; PARRIS, RUSSELL; WILKS, ASHLEY
To: OWISTONE NANOTECH, INC.
Reel/Frame 017112/0402 →
Continuity (1)
Related Publication 20070080304A1 · Apr 12, 2007