IP Library Granted Patent US 8,114,222
Granted Patent B2
US 8,114,222 · App. 11/257,874 · Granted Feb 14, 2012

Method for cleaning industrial equipment with pre-treatment

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Quick Facts
Patent No.
US 8,114,222
App. No.
11/257,874
Granted
Feb 14, 2012
Kind
B2
Abstract

A method of cleaning equipment such as heat exchangers, evaporators, tanks and other industrial equipment using clean-in-place procedures and a pre-treatment solution prior to the conventional CIP cleaning process. The pre-treatment step improves the degree of softening of the soil, and thus facilitates its removal. The pre-treatment solution can be a strong acidic solution, a strong alkaline solution, or comprise a penetrant. A preferred strong acidic solution is an acid peroxide solution. In some embodiments, the pre-treatment may include no strong alkali or acid ingredient; rather, the penetrant provides acceptable levels of pre-treatment.

Claims (13)

1. A method of cleaning soils from industrial equipment using a CIP process, the method comprising:

(a) applying a liquid acidic pre-treatment solution to the soil, the solution comprising at least 0.25 wt-% active ingredients, the active ingredients comprising:

a surfactant penetrant comprising a C 6 -C 12 fatty acid;

and an oxidizer selected from the group consisting of hydrogen peroxide, peroxycarboxylic acid compounds and mixtures thereof;

(b) allowing the pretreatment solution to remain on the soil for a period of time sufficient to facilitate soil removal;

(c) circulating a liquid CIP solution through the equipment after the pre-treatment solution, the CIP solution comprising about 0.5 to 3% of a dilute alkaline detergent wherein there is not a rinse step between the pre-treatment solution and the CIP solution; and then

(c) rinsing the equipment.

2. The method according to claim 1 , wherein the pre-treatment solution further comprises 0.25 to 1.5 wt-% acid.

3. The method according to claim 2 , wherein the pre-treatment solution comprises 0.25 to 1.5 wt-% acid and 0.4 to 8 wt-% penetrant.

4. The method according to claim 2 , wherein the pre-treatment solution comprises:

(a) 0.25 to 1.5 wt-% acid, selected from the group consisting of phosphoric acid, nitric acid, sulfuric acid, lactic acid, acetic acid, hydroxyacetic acid citric acid, and mixtures thereof; and

(b) 0.01 to 1 wt-% oxidizer comprising a peroxycarboxylic acid.

5. The method according to claim 1 , wherein the oxidizer is present at a level of 0.05 to 0.5 wt-%.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 30, 2011
From: ECOLAB INC.
To: ECOLAB USA INC.
Reel/Frame 027462/0681 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 25, 2005
From: FERNHOLZ, PETER J.; HERDT, BRANDON L.
To: ECOLAB INC.
Reel/Frame 017134/0335 →