IP Library Granted Patent US 7,465,497
Granted Patent B2
US 7,465,497 · App. 11/286,096 · Granted Dec 16, 2008

High dielectric constant nanocomposites, methods of manufacture thereof, and articles comprising the same

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Quick Facts
Patent No.
US 7,465,497
App. No.
11/286,096
Granted
Dec 16, 2008
Kind
B2
Abstract

Disclosed herein is a composition comprising thermoplastic polymers; and nanoparticles; wherein the nanoparticles comprise a substrate upon which is disposed a coating composition; and wherein the substrate has a different dielectric constant from that of the coating composition. Disclosed herein too is a composition comprising a polymeric material; and nanoparticles; wherein the nanoparticles comprise a substrate upon which is disposed a coating composition comprising a plurality of layers; and wherein at least one layer has a dielectric constant that is different from the remaining layers. Disclosed herein too is a method comprising blending a polymeric resin with nanoparticles to form a composition; wherein the nanoparticles comprise a substrate upon which is disposed a coating composition comprising a plurality of layers; and wherein at least one layer has a dielectric constant that is different from the remaining layers.

Claims (59)

1. A composition comprising:

a thermoplastic polymer, wherein the thermoplastic polymer has a glass transition temperature greater than or equal to about 100° C.; and

nanoparticles; wherein the nanoparticles comprise a substrate upon which is disposed a coating composition; wherein the substrate has a different dielectric constant from that of the coating composition; and

wherein the composition has a breakdown resistance of greater than or equal to about 200 volts/micrometer.

2. The composition of claim 1 , wherein the coating composition comprises one or more layers.

3. The composition of claim 2 , wherein a dielectric constant of an innermost layer is greater than a dielectric constant of an outermost layer.

4. The composition of claim 1 , wherein each layer has a lower dielectric constant than a dielectric constant of a preceding inner layer that is closer to the center of the nanoparticle.

5. The composition of claim 1 , wherein the substrate has a higher dielectric constant than the dielectric constant of the coating composition.

6. The composition of claim 1 , wherein the coating composition comprises a plurality of layers with progressively decreasing dielectric constants from an innermost layer to an outermost layer.

7. The composition of claim 1 , wherein the substrate comprises metals, ceramics, borides, carbides, silicates, chalcogenides, hydroxides, metals, metal oxides, nitrides, perovskites and perovskites derivatives, phosphides, sulfides, silicides, or a combination comprising at least one of the foregoing.

8. The composition of claim 1 , wherein the coating composition comprises ceramics, borides, carbides, silicates, chalcogenides, hydroxides, metals, metal oxides, nitrides, perovskites and perovskites derivatives, phosphides, sulfides, suicides, or a combination comprising at least one of the foregoing.

9. The composition of claim 8 , wherein the metal oxides comprise zirconates, titanates, aluminates, silicates, stannates, niobates, tantalates, rare earth oxides or a combination comprising at least one of the foregoing metal oxides.

10. The composition of claim 8 , wherein the perovskites comprise calcium-copper-titanium-oxides having the formula (I):

ACu 3 Ti 4 O 12   (I)

where A is calcium or cadmium.

11. The composition of claim 8 , wherein the perovskites have the formula (II):

A′ 2/3 Cu 3 Ti 3 FeO 12   (II)

where A′ is bismuth or yttrium.

12. The composition of claim 8 , wherein the perovskites are lithium and titanium co-doped nickel oxide (LTNOs) having the general formula (III):

Li x Ti y Ni 1-x-y O  (III)

where x is less than or equal to about 0.3 and y is less than or equal to about 0.1.

13. The composition of claim 1 , wherein the thermoplastic polymer has a glass transition temperature of greater than or equal to about 150° C.

14. The composition of claim 1 , wherein the thermoplastic polymer comprises polyetherimides, polyphenylene ethers, polyethylene terephthalates, polyethylenes, polypropylenes, polyimides, polyvinylidene fluorides, or a combination comprising at least one of the foregoing polymers.

15. An article comprising the composition of claim 1 .

16. The article of claim 15 , wherein the article is a capacitor or a component for a spark plug.

17. A composition comprising:

a polymeric material; wherein the polymeric material has a glass transition temperature greater than or equal to about 100° C.; and

nanoparticles; wherein the nanoparticles comprise a substrate upon which is disposed a coating composition comprising a plurality of layers; wherein at least one layer has a dielectric constant that is different from the remaining layers; and

wherein the composition has a breakdown resistance of greater than or equal to about 200 volts/micrometer.

18. The composition of claim 17 , wherein a dielectric constant of an innermost layer is greater than a dielectric constant of an outermost layer.

19. The composition of claim 17 , wherein each layer has a lower dielectric constant than a dielectric constant of a preceding inner layer that is closer to the center of the nanoparticle.

20. The composition of claim 17 , wherein the substrate has a higher dielectric constant than the dielectric constant of the coating composition.

21. The composition of claim 17 , wherein the plurality of layers have a progressively decreasing dielectric constant from an innermost layer to an outermost layer.

22. The composition of claim 17 , wherein the substrate comprises metals, ceramics, borides, carbides, silicates, chalcogenides, hydroxides, metals, metal oxides, nitrides, perovskites and perovskites derivatives, phosphides, sulfides, silicides, or a combination comprising at least one of the foregoing.

23. The composition of claim 22 , wherein the metal oxides comprise zirconates, titanates, aluminates, silicates, stannates, niobates, tantalates, rare earth oxides or a combination comprising at least one of the foregoing metal oxides.

24. The composition of claim 22 , wherein the perovskites comprise calcium-copper-titanium-oxides having the formula (I):

ACu 3 Ti 4 O 12   (I)

where A is calcium or cadmium.

25. The composition of claim 22 , wherein the perovskites have the formula (II):

A′ 2/3 Cu 3 Ti 3 FeO 12   (II)

where A′ is bismuth or yttrium.

26. The composition of claim 22 , wherein the perovskites are lithium and titanium co-doped nickel oxide (LTNOs) having the general formula (III):

Li x Ti y Ni 1-x-y O  (III)

where x is less than or equal to about 0.3 and y is less than or equal to about 0.1.

27. The composition of claim 17 , wherein the coating composition comprises ceramics, borides, carbides, silicates, chalcogenides, hydroxides, metals, metal oxides, nitrides, perovskites and perovskites derivatives, phosphides, sulfides, silicides, or a combination comprising at least one of the foregoing.

28. The composition of claim 17 , wherein the polymeric material has a glass transition temperature of greater than or equal to about 150° C.

29. The composition of claim 17 , wherein the polymeric material comprises a thermosetting polymer.

30. The composition of claim 17 , wherein the polymeric material comprises polyetherimides, polyphenylene ethers, polyethylene terephthalates, polyimides, polyvinylidene fluorides, or a combination comprising at least one of the foregoing polymers.

31. The composition of claim 17 , wherein the nanoparticle comprises a passivated metal.

32. An article comprising the composition of claim 17 .

33. A method comprising:

blending a polymeric resin with nanoparticles to form a composition;

wherein the polymeric resin has a glass transition temperature greater than or equal to about 100° C.

wherein the nanoparticles comprise a substrate upon which is disposed a coating composition comprising a plurality of layers; wherein at least one layer has a dielectric constant that is different from the remaining layers; and

wherein the composition has a breakdown resistance of greater than or equal to about 200 volts/micrometer.

34. The method of claim 33 , further comprising casting the composition.

35. The method of claim 33 , further comprising molding the composition

36. The method of claim 35 , wherein the molding comprises injection molding.

37. An article manufactured by the method of claim 33 .

Assignments (5)
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE TO GENERAL ELECTRIC COMPANY & CORRECT CORRESPONDENCE STREET ADDRESS TO: 1 RESEARCH CIRCLE PREVIOUSLY RECORDED ON REEL 027518 FRAME 0803. ASSIGNOR(S) HEREBY CONFIRMS THE CLARIFICATION OF OWNERSHIP. Recorded Jan 13, 2012
From: GENERAL ELECTRIC COMPANY
To: GENERAL ELECTRIC COMPANY
Reel/Frame 027531/0149 →
CLARIFICATION OF OWNERSHIP Recorded Jan 11, 2012
From: GENERAL ELECTRIC COMPANY
To: GENEFRAL ELECTRIC COMPANY
Reel/Frame 027518/0803 →
RELEASE OF SECURITY INTEREST Recorded Jun 19, 2009
From: CITIBANK, N.A.
To: SABIC INNOVATIVE PLASTICS IP B.V.
Reel/Frame 022846/0411 →
SECURITY AGREEMENT Recorded Aug 18, 2008
From: SABIC INNOVATIVE PLASTICS IP B.V.
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 021423/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 23, 2005
From: TAN, QI; IRWIN, PATRICIA CHAPMAN; CAO, YANG
To: GENERAL ELECTRIC COMPANY
Reel/Frame 017277/0066 →