IP Library Granted Patent US 7,670,506
Granted Patent B1
US 7,670,506 · App. 11/321,784 · Granted Mar 2, 2010

Photoactive compositions for liquid deposition

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Quick Facts
Patent No.
US 7,670,506
App. No.
11/321,784
Granted
Mar 2, 2010
Kind
B1
Abstract

Compositions are provided, comprising a host and a dopant, wherein the weight:weight ratio of host:dopant is about 10:1 to about 40:1, and a solvent, and methods for making the same, as well as devices and sub-assemblies including the same.

Claims (39)

1. A composition comprising:

(i) a distyrylarylene or mixtures of a distyrylarylene and a diarylantracene; and

(ii) an arylamine;

in a concentration of about 1.0% w/v in a solvent, wherein the weight:weight ratio of (i):(ii) is about 10:1 to about 40:1;

wherein said distyrylarylene is of the formula

wherein R 1 to R 30 are, independently, hydrogen, alkyl, alkoxy, or aryl.

2. The composition of claim 1 , wherein the weight ratio of distyrylarylene:arylamine is 13:1.

3. The composition of claim 1 , wherein the weight ratio of distyrylarylene:arylamine is 30:1.

4. The composition of claim 1 , wherein the solvent is an aromatic hydrocarbon.

5. The composition of claim 1 , wherein the solvent is toluene, xylene, mesitylene, anisole, chlorobenzene, cyclohexanone, gamma-valerolactone, chloroform, tetrachloroethane, tetrachloroethylene, trifluorotoluene, methylbenzoate, N,N-dimethylformamide or derivatives thereof.

6. The composition of claim 1 , wherein the solvent is toluene, xylene, mesitylene, anisole, chlorobenzene, cyclohexanone, gamma-valerolactone, or chloroform, or derivatives thereof, or mixtures thereof.

7. The composition of claim 1 , wherein the solvent is toluene.

8. The composition of claim 7 , wherein the solvent is trifluorotoluene.

9. The composition of claim 1 , wherein the solvent is toluene and trifluorotoluene.

10. The composition of claim 9 , wherein the toluene and trifluorotoluene are in a 1:1 volume:volume ratio.

11. The composition of claim 1 , wherein the solvent further includes esters, ketones, and alcohols.

12. A composition comprising:

a host and a dopant, wherein the weight:weight ratio of host:dopant is about 10:1 to about 40:1, wherein said host is a distyrylarylene or mixtures of a distyrylarylene and a diarylantracene; and

a solvent;

wherein said distyrylarylene is of the formula

wherein R 1 to R 30 are, independently, hydrogen, alkyl, alkoxy, or aryl.

13. The composition of claim 12 , wherein the solvent is organic and nonreactive with the host and dopant.

14. The composition of claim 12 , wherein the host and dopant are present in a concentration of about 1.0% w/v in the solvent.

15. The composition of claim 12 , wherein the weight ratio of host:dopant is about 13:1.

16. A method for forming an organic electronic device, comprising:

providing the composition of claim 12 ; and

depositing the composition as a liquid.

17. The method of claim 16 , wherein the depositing step is spin-coating.

18. A composition including the composition of claim 12 .

19. An organic electronic device having an active layer including the composition of claim 12 .

20. An article useful in the manufacture of an organic electronic device, comprising the composition of claim 12 .

21. A composition comprising:

(i) a distyrylarylene, a diarylanthracene, or mixtures thereof; and

(ii) an arylamine;

in a concentration of about 1.0% w/v in a solvent, wherein the weight:weight ratio of (i):(ii) is about 10:1 to about 40:1, wherein the solvent comprises trifluorotoluene.

22. The composition of claim 21 wherein said solvent additionally comprises toluene.

23. The composition of claim 22 , wherein the toluene and trifluorotoluene are in a 1:1 volume:volume ratio.

24. The composition of claim 21 , wherein the weight ratio of distyrylarylene:arylamine is 13:1.

25. The composition of claim 21 , wherein the weight ratio of distyrylarylene:arylamine is 30:1.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 22, 2019
From: E. I. DU PONT DE NEMOURS AND COMPANY
To: LG CHEM, LTD.
Reel/Frame 050150/0482 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 30, 2006
From: LECLOUX, DANIEL DAVID; SMITH, ERIC MAURICE
To: E. I. DU PONT DE NEMOURS AND COMPANY
Reel/Frame 017690/0792 →