N-(2((4-Hydroxyphenyl)amino)pyridin-3-yl)-4-methoxybenzenesulfonamide Crystalline Form 1
View Patent ↗N-(2-((4-Hydroxyphenyl)amino)pyridin-3-yl)-4-methoxybenzenesulfonamide Crystalline Form 1, ways to make it, compositions containing it and methods of treatment of diseases using it are disclosed.
1. A process for making N-(2-((4-Hydroxyphenyl)amino)pyridin-3-yl)-4-methoxybenzenesulfonamide Crystalline Form 1, said processes comprising:
causing nucleation in mixture of N-(2-((4-hydroxyphenyl)amino)pyridin-3 -yl)-4-methoxybenzenesulfonamide and solvent between about 60° C. and 100° C., wherein the N-(2-((4-hydroxyphenyl)amino)pyridin-3 -yl)-4-methoxybenzenesulfonamide is completely dissolved in the solvent and the solvent is supersaturated with the N-(2-((4-hydroxyphenyl)amino)pyridin-3 -yl)-4-methoxybenzenesulfonamide and isolating said N-(2-((4-Hydroxyphenyl)amino)pyridin-3 -yl)-4-methoxybenzenesulfonamide Crystalline Form 1.