IP Library Granted Patent US 7,931,701
Granted Patent B2
US 7,931,701 · App. 11/338,346 · Granted Apr 26, 2011

Composition for dyeing of cellulosic fabric

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Quick Facts
Patent No.
US 7,931,701
App. No.
11/338,346
Granted
Apr 26, 2011
Kind
B2
Abstract

The present invention provides a composition that permits spray dyeing of a cellulosic, such as cotton, fabric or garment. The composition includes a wetter, an alkali, a reactive dye, and water, and preferably a thickener. The present compositions are made by first mixing together the wetter, reactive dye and water to form a first solution, then mixing the thickener into the first solution to form a second solution, and thereafter mixing or merging the alkali to the second solution within five minutes prior to spray application onto the cellulosic fabric or garment.

Claims (27)

1. A spray composition for dyeing a cotton fabric having fibers, consisting essentially of:

a wetter, wherein the wetter is a blend of one or more surfactants includes sulfuric acid disodium salt and phosphoric acid trisodium salt;

an alkali, wherein the alkali is a combination of sodium silicate and a caustic;

a reactive dye;

water; and

the wetter, the alkali and the reactive dye are anionic ingredients for application of the spray composition onto surfaces of the cotton fabric.

2. The composition of claim 1 , further comprising a thickener.

3. The composition of claim 2 , wherein the thickener is an acrylic acid copolymer.

4. The composition of claim 3 , wherein the acrylic acid copolymer has 2% to 3% naphthol spirits.

5. The composition of claim 2 , wherein the thickener is present in an amount between 5 g/l and 50 g/l based on the total g/l of the composition.

6. The composition of claim 1 , wherein the wetter is present in an amount between 5 g/l and 40 g/l based on the total g/l of the composition.

7. The composition of claim 1 , wherein the alkali is present in an amount between 3 g/l and 20 g/l based on the total g/l of the composition.

8. The composition of claim 7 , wherein the sodium silicate to the caustic is in a ratio of about 2 to about 1.

9. The composition of claim 1 , wherein the reactive dye is present in an amount between 10 g/l and 80 g/l based on the total g/l of the composition.

10. The composition of claim 1 , further comprising a chelator.

11. The composition of claim 10 , wherein the chelator is present in an amount between 1 g/l and 40 g/l based on the total g/l of the composition.

12. The composition of claim 1 , further comprising one or more ingredients selected from the group consisting of a defoamer, an anti-reducing agent, and sodium chloride.

13. The composition of claim 1 , wherein the cotton fabric forms a garment that is selected from the group consisting essentially a brassiere, shirt, pants, underwear, panty, sock, skirt, dress, shorts, coat, suit, scarf, glove, and hat.

14. A spray dye composition for spray dyeing a cotton fabric having fibers comprising:

a wetter wherein the wetter is a blend of one or more surfactants includes sulfuric acid disodium salt and phosphoric acid trisodium salt in an amount between 5 g/l and 20 g/l;

an alkali wherein the alkali is a combination of sodium silicate and a caustic in an amount between 3 g/l and 20 g/l;

a reactive dye in an amount between 10 g/l and 80 g/l based on the total g/l of the composition;

water; and

the wetter, the alkali, and the reactive dye are anionic ingredients for application of the spray composition onto surfaces of the cotton fabric.

15. The composition of claim 14 , further comprising a thickener in an amount between 5 g/l and 50 g/l based on the total g/l of the composition.

16. The composition of claim 15 , further comprising a chelator in an amount between 1 g/l and 40 g/l based on the total g/l of the composition.

17. The composition of claim 14 , wherein the alkali is a combination of a sodium silicate and a caustic.

Assignments (10)
RELEASE OF PATENT SECURITY INTEREST RECORDED AT R/F 45029/0132 Recorded Dec 15, 2025
From: JPMORGAN CHASE BANK, N.A.
To: MAIDENFORM LLC; HBI BRANDED APPAREL ENTERPRISES, LLC
Reel/Frame 074166/0114 →
RELEASE OF PATENT SECURITY INTEREST RECORDED AT R/F 59910/0685 Recorded Dec 15, 2025
From: JPMORGAN CHASE BANK, N.A.
To: MAIDENFORM LLC; HBI BRANDED APPAREL ENTERPRISES, LLC
Reel/Frame 074165/0634 →
FOURTH AMENDED AND RESTATED PATENT SECURITY AGREEMENT Recorded May 9, 2022
From: HANESBRANDS INC.; ALTERNATIVE APPAREL, INC.; BA INTERNATIONAL, L.L.C.; CC PRODUCTS LLC; CEIBENA DEL, INC.; EVENT 1 LLC; GEARCO LLC; GFSI HOLDINGS LLC; GFSI LLC; GTM RETAIL, INC.; HANES GLOBAL HOLDINGS U.S. INC.; HANES JIBOA HOLDINGS, LLC; HANES MENSWEAR, LLC; HANESBRANDS DIRECT, LLC; HANESBRANDS EXPORT CANADA LLC; HBI BRANDED APPAREL ENTERPRISES LLC; HBI INTERNATIONAL HOLDINGS U.S., INC.; HBI SOURCING, LLC; INNER SELF LLC; IT'S GREEK TO ME, INC.; KNIGHTS APPAREL, LLC; KNIGHTS HOLDCO, LLC; MAIDENFORM (BANGLADESH) LLC; MAIDENFORM (INDONESIA) LLC; MAIDENFORM BRANDS LLC; MAIDENFORM INTERNATIONAL LLC; MAIDENFORM LLC; MF RETAIL LLC; PLAYTEX DORADO, LLC; PLAYTEX INDUSTRIES, INC.; SEAMLESS TEXTILES LLC
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 059910/0685 →
SECURITY INTEREST Recorded Jan 9, 2018
From: HBI BRANDED APPAREL ENTERPRISES, LLC; IT'S GREEK TO ME, INC.; MAIDENFORM LLC
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 045029/0132 →
AMENDED AND RESTATED PATENT SECURITY AGREEMENT Recorded Dec 15, 2009
From: HBI BRANDED APPAREL ENTERPRISES, LLC
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT AND COLLATERAL AGENT
Reel/Frame 023649/0812 →
RELEASE OF SECOND LIEN SECURITY INTEREST RECORDED AT REEL/FRAMES 018367/0353, 018367/0312, AND 018545/0521 Recorded Dec 10, 2009
From: CITIBANK, N.A., AS COLLATERAL AGENT
To: HBI BRANDED APPAREL ENTERPRISES, LLC
Reel/Frame 023627/0842 →
PATENT SECURITY AGREEMENT (FIRST LIEN) Recorded Oct 10, 2006
From: HBI BRANDED APPAREL ENTERPRISES, LLC
To: CITIBANK, N.A., AS THE COLLATERAL AGENT
Reel/Frame 018367/0333 →
PATENT SECURITY AGREEMENT (SECOND LIEN) Recorded Oct 10, 2006
From: HBI BRANDED APPAREL ENTERPRISES, LLC
To: CITIBANK, N.A., AS THE COLLATERAL AGENT
Reel/Frame 018367/0353 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 21, 2006
From: SARA LEE CORPORATION
To: HBI BRANDED APPAREL ENTERPRISES, LLC
Reel/Frame 018279/0527 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 31, 2006
From: MAY, RUTH E.; BENTHAM, MARTIN
To: SARA LEE CORPORATION
Reel/Frame 018144/0267 →