IP Library Granted Patent US 7,622,610
Granted Patent B2
US 7,622,610 · App. 11/354,486 · Granted Nov 24, 2009

Crystalline ACAT inhibitor

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Quick Facts
Patent No.
US 7,622,610
App. No.
11/354,486
Granted
Nov 24, 2009
Kind
B2
Abstract

The invention is directed to the Form A polymorph of N-benzyl-N′-(2,6-diisopropyl-phenyl)-N-isopropyl-malonamide and its use as a therapeutic/cosmetic agent.

Claims (10)

1. Form A polymorph of N-benzyl-N′-(2,6-diisopropyl-phenyl)-N-isopropyl-malonamide.

2. A crystalline polymorph of N-benzyl-N′-(2,6-diisopropyl-phenyl)-N-isopropyl-malonamide that exhibits an X-ray powder diffraction pattern having at least one characteristic peak expressed in degrees 2θ at approximately 16.0, 19.6, or 28.1.

3. A crystalline polymorph of N-benzyl-N′-(2,6-diisopropyl-phenyl)-N-isopropyl-malonamide that exhibits an X-ray powder diffraction pattern having characteristic peaks expressed in degrees 2θ at approximately 16.0, 19.6, and 28.1.

4. The crystalline polymorph according to claim 2 which exhibits at least one additional peak, expressed in degrees 2θ, at approximately 7.3, 10.3, 16.5, 17.9, 19.1, 20.7, or 25.

5. The crystalline polymorph according to claim 3 which exhibits at least one additional peak, expressed in degrees 2θ, at approximately 7.3, 10.3, 16.5, 17.9, 19.1, 20.7, or 25.0.

6. The crystalline polymorph according to claim 2 which exhibits at least two additional peaks, expressed in degrees 2θ, at approximately 7.3, 10.3, 10.8, 11.3, 12.1, 14.6, 14.9, 16.5, 17.9, 18.1, 18.9, 19.1, 20.7, 21.8, 22.9, 23.2, 25.0, or 26.0.

7. The crystalline polymorph according to claim 3 which exhibits at least two additional peaks, expressed in degrees 2θ, at approximately 7.3, 10.3, 10.8, 11.3, 12.1, 14.6, 14.9, 16.5, 17.9, 18.1, 18.9, 19.1, 20.7, 21.8, 22.9, 23.2, 25.0, or 26.0.

8. A pharmaceutical composition comprising a polymorph according to claim 1 in admixture with at least one pharmaceutically acceptable excipient.

9. A topical pharmaceutical composition manufactured using a polymorph according to claim 4 .

10. A topical pharmaceutical composition manufactured using a polymorph according to claim 5 .

Assignments (4)
RELEASE OF SECURITY INTEREST Recorded Apr 8, 2025
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: SOLTA MEDICAL, INC.; PRECISION DERMATOLOGY, INC.; BAUSCH HEALTH IRELAND LIMITED (F/K/A/ VALEANT PHARMACEUTICALS IRELAND LIMITED); SALIX PHARMACEUTICALS, INC.; SALIX PHARMACEUTICALS, LTD; SANTARUS, INC.; MEDICIS PHARMACEUTICAL CORPORATION; HUMAX PHARMACEUTICAL S.A.; SOLTA MEDICAL IRELAND LIMITED; BAUSCH & LOMB MEXICO, S.A. DE C.V.; BAUSCH+LOMB OPS B.V.; BAUSCH HEALTH AMERICAS, INC.; BAUSCH HEALTH COMPANIES INC.; BAUSCH HEALTH HOLDCO LIMITED; BAUSCH HEALTH MAGYARORSZAG KFT (A/K/A BAUSCH HEALTH HUNGARY LLC); BAUSCH HEALTH POLAND SPOLKA Z OGRANICZONA ODPOWIEDZIALNOSCIA (F/K/A VALEANT PHARMA POLAND SPOLKA Z OGRANICZONA ODPOWIEDZIALNOSCIA); BAUSCH HEALTH US, LLC; BAUSCH HEALTH, CANADA INC. / SANTE BAUSCH, CANADA INC.; ICN POLFA RZESZOW SPOLKA AKCYJNA (A/K/A ICN POLFA RZESZOW S.A.); ORAPHARMA, INC.; PRZEDSIEBIORSTWO FARMACEUTYCZNE JELFA SPOLKA AKCYJNA (A/K/A PRZEDSIEBIORSTWO FARMACEUTYCZNE JELFA S.A.); SOLTA MEDICAL DUTCH HOLDINGS B.V.; V-BAC HOLDING CORP.; VRX HOLDCO LLC; 1261229 B.C. LTD.; 1530065 B.C. LTD.
Reel/Frame 070778/0199 →
NOTICE OF SUCCESSION OF AGENCY Recorded Jan 9, 2015
From: GOLDMAN SACHS LENDING PARTNERS, LLC
To: BARCLAYS BANK PLC, AS SUCCESSOR AGENT
Reel/Frame 034749/0689 →
RELEASE OF SECURITY INTEREST Recorded Jan 10, 2014
From: GOLDMAN SACHS LENDING PARTNERS LLC
To: MEDICIS PHARMACEUTICAL CORPORATION
Reel/Frame 031944/0190 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 25, 2013
From: MEDICIS PHARMACEUTICAL CORPORATION
To: THESAN PHARMACEUTICALS, INC.
Reel/Frame 031280/0766 →