Methods for monitoring binder mix loading of fiber glass mats
View Patent ↗Process and apparatus for non-invasive measuring of binder mix loading of glass fibers for monitoring production of construction insulation product, such as roofing and wall insulation. The process utilizes visible (VIS) and near infrared (NIR) spectroscopy; and, is particularly advantageous when utilized in an on-line production processing following binder mix loading of glass fibers and prior to curing treatment of the binder mix loaded glass fibers. Such spectroscopic analyses can be carried out on a static or moving support substrate. The blend is then conveyed to and through curing treatment to form insulation product. The blend is exposed to VIS-NIR radiant energy, and a radiant energy sensor collects resulting data as to absorption following penetration of the VIS-NIR radiant energy. The spectroscopic instrumentation is calibrated to determine to facilitate accuracy; and, can be used to verify load following curing. The amount of binder mix, in the binder mix/fiber blend, is adjusted if the blend is outside of desired loading specifications.
1. Process for monitoring binder mix loading of glass fibers comprising
(a) providing a first blend combining glass fibers and binder mix, each in an amount suitable for forming insulation product;
(b) exposing samples of said first blend, while on a static support substrate or on a moving support substrate, to radiant energy in a wavelength region of about 350-2500 nm, and spectroscopically collecting data resulting from penetration of such energy into said first blend of such samples; for
(c) providing calibration of spectroscopic instrumentation, based on the data collected in (b), so as to enable reflecting binder mix content of such samples;
(d) placing a second blend of glass fibers and binder mix on a predetermined support substrate;
(e) subjecting, free of mechanical contact with said second blend, at least a portion of said second blend to radiant energy in a wavelength spectrum of about 350-2500 nm, for measuring absorption data reflecting absorbed energy into said second blend; in which
(f) such measured absorption data of (e) is correlated with said calibration of (c) for verifying quantitative measurement of hinder mix content of said second blend.
2. The invention of claim 1 , wherein steps (e) and (f) are conducted on a periodic or a continuous basis.
3. The invention of claim 1 , wherein said second blend is provided as a mat.
4. The invention of claim 1 , wherein said calibration of said spectroscopic instrumentation is carried out by multivariate calibration.
5. The invention of claim 1 , wherein said second blend is subjected to radiant energy, has an area of at least about 3 inches in diameter.
6. A process for spectroscopically monitoring binder mix loading of glass fibers, comprising
(1) providing calibration for spectroscopic instrumentation based on binder mix content of reference samples of known blends of glass fibers and binder mix, by measuring radiant energy penetration of said reference samples in a wavelength spectrum of about 350-2500 nm;
(2) exposing at least a portion of a blend of fiber glass and binder mix, while said blend is on a static support substrate or a moving support substrate, to radiant energy in a wavelength spectrum of about 350-2500 nm and measuring absorption of such energy as a result of penetration of said blend;
(3) monitoring measured absorbed radiant energy as a result of penetrating said reference samples, to obtain relative peak intensity of binder mix, as present in each reference sample and processing to convert peak shape to a level of analyte to obtain a value of binder mix content, and
(4) correlating said value of binder mix content of said blend with said calibrated reference sample to determine differences, if any, between said values and said calibrated reference samples.
7. The invention of claim 6 , wherein steps (3) and (4) are conducted on a periodic or continuous basis.
8. The invention of claim 6 , wherein said blend of glass fibers and binder mix is provided as a mat.
9. The invention of claim 6 , wherein calibration of such spectroscopic instrumentation is carried out by multivariate calibration.
10. The invention of claim 4 or 9 , wherein said multivariate calibration utilizes a Partial Least Squares (PLS) algorithm.
11. The invention of claim 4 or 9 , wherein said multivariate calibration utilizes a Principle Component Regression (PCR) algorithm.
12. The invention of claim 4 or 9 , wherein said multivariate calibration utilizes a Multiple Linear Regression (MLR) algorithm.
13. The invention of claim 1 or 6 , wherein said radiant energy wavelength region is 400-2500 nm.
14. The invention of claim 1 or 6 , wherein said radiant energy wavelength region is 400-1800 nm.
15. The invention of claim 1 or 6 , wherein said radiant energy wavelength region is 400-1000 nm.
16. The invention of claim 1 or 6 , wherein said radiant energy wavelength region is 350-1050 nm.
17. The invention of claim 1 or 6 , comprising selecting an on-line support substrate conveying system.
18. The invention of claim 1 or 6 , comprising selecting a support substrate which is a rotating turntable.
19. The invention of claim 6 , wherein said portion of such blend of fiber glass and binder mix subjected to said radiant energy, has an area of at least about 3 inches in diameter.