IP Library Granted Patent US 7,422,644
Granted Patent B2
US 7,422,644 · App. 11/366,606 · Granted Sep 9, 2008

Thin parts made of β or quasi-β titanium alloys; manufacture by forging

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Quick Facts
Patent No.
US 7,422,644
App. No.
11/366,606
Granted
Sep 9, 2008
Kind
B2
Abstract

The present invention provides non-axially symmetrical manufactured parts of thickness less than 10 mm, made of β or quasi-β titanium alloy, having a core microstructure constituted by whole grains presenting a slenderness ratio greater than 4 and an equivalent diameter lying in the range 10 μm to 300 μm. The invention also provides a method of manufacturing the parts by forging.

Claims (40)

1. A method of manufacturing a non-axially symmetrical part having a thickness less than 10 mm, and made of “quasi-β” titanium alloy, said method comprising:

obtaining an enameled blank;

transforming the blank into a long part of equivalent diameter less than 100 mm;

forging the long part with a final heating operation carried out at a temperature above a β transition;

quenching the forged long part; and

tempering the quenched forged long part.

2. The method according to claim 1 , wherein the part has a core microstructure comprising whole grains having a slenderness ratio greater than 4 and an equivalent diameter lying in the range of 10 μm to 300 μm.

3. The method according to claim 1 , wherein the part is a part selected from the group consisting of a compressor blade, a single-piece bladed disk, a single-piece bladed ring, a propeller, a fan blade, and a mixer blade.

4. The method according to claim 2 , wherein the quasi-β titanium alloy is a Ti 17 alloy (TA 5 CD 4 or TiAl 5 Cr 2 Mo 4 ).

5. The method according to claim 1 , wherein the forging comprises at least two heating operations, the first to a temperature that is below or above the β transition, and the last to a temperature that is above the β transition, a reduction ratio on each heating operation being greater than or equal to 2, and a forging speed lying in the range of 1s −1 to 1×10 −5 s −1 .

6. The method according to claim 5 , wherein the forging comprises first and second heating operations that are independently above or below the β transition, and a third heating operation that is above the β transition.

7. The method according to claim 5 , further comprising:

re-enameling the part between two heating operations.

8. The method according to claim 1 , wherein a forging matrix is maintained at a temperature lying in the range of 100° C. to 700° C.

9. The method according to claim 1 , wherein quenching is implemented under conditions which induce a cooling speed that is less than or equal to the speed induced by quenching in a bath of oil.

10. The method according to claim 1 , wherein the tempering is implemented at a temperature lying in the range 620° C. to 750° C. for a period lying in the range 3 h to 5 h.

11. The method according to claim 1 , wherein the blank is made of Ti 17 alloy (TA 5 CD 4 or TiAl 5 Cr 2 Mo 4 ).

12. The method according to claim 1 , wherein the forging comprises a first heating operation at a temperature less than or equal to 840° C ±10° C or at a temperature greater than or equal to 940° C ±10° C and a second heating operation at a temperature of 940° C ±10° C.

13. The method according to claim 12 , wherein the quenching is implemented on a matrix and then in still air.

14. The method according to claim 13 , wherein the tempering is implemented at 630° C for 4 h.

15. The method according to claim 1 , wherein the whole grains comprise lens-shaped forms and non β-parts within the whole grains comprising α-needles.

16. A method of manufacturing a non-axially symmetrical part having a thickness less than 10 mm, made of a quasi-β titanium alloy, and having a core microstructure comprising whole grains having a slenderness ratio greater than 4 and an equivalent diameter lying in the range of 10 μm to 300 μm, the method comprising:

obtaining an enameled blank;

transforming the blank into a long part of equivalent diameter less than 100 mm;

forging the long part with a final heating operation carried out at a temperature above a β transition;

quenching the forged long part; and

tempering the quenched forged long part.

17. The method according to claim 16 , wherein the forging comprises homogeneously forging the entire long part.

18. The method according to claim 16 , wherein the part is a part selected from the group consisting of a compressor blade, a single-piece bladed disk, a single-piece bladed ring, a propeller, a fan blade, and a mixer blade.

19. The method according to claim 16 , wherein the quasi-β titanium alloy is a Ti 17 alloy (TA 5 CD 4 or TiAl 5 Cr 2 Mo 4 ).

20. The method according to claim 16 , wherein the forging comprises at least two heating operations, the first to a temperature that is below or above the β transition, and the last to a temperature that is above the β transition, a reduction ratio on each heating operation being greater than or equal to 2, and a forging speed lying in the range of 1 s −1 to 1×10 −5 s −1 .

21. The method according to claim 20 , wherein the forging comprises first and second heating operations that are independently above or below the β transition, and a third heating operation that is above the β transition.

22. The method according to claim 20 , further comprising:

re-enameling the part between two heating operations.

23. The method according to claim 16 , wherein the obtaining comprises extruding a bar so as to obtain the enameled blank.

24. The method according to claim 16 , wherein a forging matrix is maintained at a temperature lying in the range of 100° C. to 700° C.

25. The method according to claim 16 , wherein quenching is implemented under conditions which induce a cooling speed that is less than or equal to the speed induced by quenching in a bath of oil.

26. The method according to claim 16 , wherein the tempering is implemented at a temperature lying in the range 620° C. to 750° C. for a period lying in the range 3 h to 5 h.

27. The method according to claim 16 , wherein the blank is made of Ti 17 alloy (TA 5 CD 4 or TiAl 5 Cr 2 Mo 4 ), the forging comprises a first heating operation at a temperature less than or equal to 840° C.±10° C. or at a temperature greater than or equal to 940° C.±10° C. and a second heating operation at a temperature of 940° C.±10° C., the quenching is implemented on a matrix and then in still air, and the tempering is implemented at 630° C. for 4 h.

28. The method according to claim 16 , wherein the whole grains comprise lens-shaped forms and non β-parts within the whole grains comprising α-needles.

Assignments (2)
CORRECTIVE ASSIGNMENT TO CORRECT THE COVER SHEET TO REMOVE APPLICATION NOS. 10250419, 10786507, 10786409, 12416418, 12531115, 12996294, 12094637 12416422 PREVIOUSLY RECORDED ON REEL 046479 FRAME 0807. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF NAME. Recorded Aug 24, 2018
From: SNECMA
To: SAFRAN AIRCRAFT ENGINES
Reel/Frame 046939/0336 →
CHANGE OF NAME Recorded May 23, 2018
From: SNECMA
To: SAFRAN AIRCRAFT ENGINES
Reel/Frame 046479/0807 →