IP Library Granted Patent US 7,918,293
Granted Patent B1
US 7,918,293 · App. 11/370,425 · Granted Apr 5, 2011

Method and system for perceiving a boundary between a first region and a second region of a superabrasive volume

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Quick Facts
Patent No.
US 7,918,293
App. No.
11/370,425
Granted
Apr 5, 2011
Kind
B1
Abstract

Methods of evaluating a superabrasive volume or a superabrasive compact are disclosed. One method may comprise exposing a superabrasive volume to beta particles and detecting a quantity of scattered beta particles. Further, a boundary may be perceived between a first region and a second region of the superabrasive volume in response to detecting the quantity of scattered beta particles. In another embodiment, a boundary between a catalyst-containing region and a catalyst-diminished region of a polycrystalline diamond volume may be perceived. In a further embodiment, a boundary may be perceived between a catalyst-containing region and a catalyst-diminished region of a polycrystalline diamond compact. Additionally, a depth to which a catalyst-diminished region extends within a polycrystalline diamond volume of a polycrystalline diamond compact may be measured in response to detecting a quantity of scattered beta particles. A system configured to evaluate a superabrasive volume is disclosed.

Claims (43)

1. A method of evaluating a superabrasive volume, the method comprising:

providing a superabrasive volume comprising a plurality of superabrasive grains bonded to one another forming a coherent matrix;

exposing a superabrasive volume to beta particles;

detecting a quantity of scattered beta particles;

perceiving a boundary between a first region of the superabrasive volume and a second region of the superabrasive volume in response to detecting the quantity of scattered beta particles wherein each of the first volume and the second volume include a portion of the coherent matrix, and wherein perceiving the boundary between the first region and the second region of the superabrasive volume comprises perceiving a boundary between a catalyst-containing region and a catalyst-diminished region of the superabrasive volume.

2. The method of claim 1 , wherein perceiving the boundary comprises perceiving an arcuate boundary.

3. The method of claim 1 , wherein exposing the superabrasive volume to beta particles comprises exposing a polycrystalline diamond volume to beta particles.

4. The method of claim 3 , wherein a catalyst used for forming the polycrystalline diamond volume is substantially removed from the first region of the polycrystalline diamond volume.

5. The method of claim 4 , wherein perceiving the boundary between the first region of the superabrasive volume and the second region of the superabrasive volume comprises measuring a depth of the first superabrasive region from an exterior surface of the polycrystalline diamond volume.

6. The method of claim 4 , wherein cobalt is substantially removed from the first region of the polycrystalline diamond volume.

7. The method of claim 1 , wherein perceiving the boundary between the first region and the second region of the superabrasive volume comprises perceiving a boundary between a cobalt-containing region and a cobalt-diminished region of the superabrasive volume.

8. A method of evaluating a polycrystalline diamond volume, the method comprising:

exposing a polycrystalline diamond volume to beta particles;

detecting a quantity of scattered beta particles;

perceiving a boundary between a catalyst-containing region of the polycrystalline diamond volume and a catalyst-diminished region of the polycrystalline diamond volume in response to detecting the quantity of scattered beta particles.

9. The method of claim 8 , wherein perceiving the boundary comprises perceiving an arcuate boundary.

10. The method of claim 8 , wherein perceiving the boundary comprises measuring a depth of the catalyst-diminished region from an exterior surface of the polycrystalline diamond volume.

11. The method of claim 8 , wherein cobalt is substantially removed from the catalyst-diminished region of the polycrystalline diamond volume.

12. The method of claim 8 , wherein perceiving the boundary between the catalyst-diminished region and the catalyst-containing region of the polycrystalline diamond volume comprises perceiving a boundary between a cobalt-containing region and a cobalt-diminished region of the polycrystalline diamond volume.

13. A method of evaluating a polycrystalline diamond compact, the method comprising:

providing a polycrystalline diamond compact comprising a polycrystalline diamond volume bonded to a substrate;

exposing the polycrystalline diamond volume to beta particles;

detecting a quantity of scattered beta particles;

perceiving a boundary between a catalyst-containing region of the polycrystalline diamond volume and a catalyst-diminished region of the polycrystalline diamond volume in response to detecting the quantity of scattered beta particles.

14. The method of claim 13 , wherein perceiving the boundary comprises perceiving an arcuate boundary.

15. The method of claim 13 , wherein perceiving the boundary between the catalyst-containing region of the polycrystalline diamond volume and the catalyst-diminished region of the polycrystalline diamond volume comprises measuring a depth of the catalyst-diminished region from an exterior surface of the polycrystalline diamond volume.

16. The method of claim 13 , wherein a catalyst used for forming the polycrystalline diamond volume is substantially removed from the catalyst-diminished region of the polycrystalline diamond volume.

17. The method of claim 13 , wherein cobalt is substantially removed from the catalyst-diminished region of the polycrystalline diamond volume.

18. The method of claim 13 , wherein perceiving the boundary between the catalyst-containing region and the catalyst-diminished region of the polycrystalline diamond volume comprises perceiving a boundary between a cobalt-containing region and a cobalt-diminished second of the polycrystalline diamond volume.

19. A method of evaluating a polycrystalline diamond compact, the method comprising:

providing a polycrystalline diamond compact comprising a polycrystalline diamond volume bonded to a substrate, the polycrystalline diamond volume including a coherent matrix of mutually bonded diamond grains and a catalyst material in a portion of the polycrystalline diamond volume;

exposing the polycrystalline diamond volume to beta particles;

detecting a quantity of scattered beta particles;

measuring a depth to which a catalyst-diminished region of the polycrystalline diamond extends within the polycrystalline diamond volume in response to detecting the quantity of scattered beta particles.

20. The method of claim 19 , wherein measuring the depth to which the catalyst-diminished region of the polycrystalline diamond extends within the polycrystalline diamond volume comprises measuring a depth to which cobalt has been at least partially removed from the polycrystalline diamond volume.

21. A system configured to evaluate a superabrasive volume, the system comprising:

a beta particle source;

a beta particle detector;

calibration data for correlating a quantity of detected beta particles to an indicated depth of a first region of a coherent matrix of a superabrasive volume, the indicated depth being less than a total thickness of the coherent matrix.

22. The system of claim 21 , wherein the calibration data comprises a first measured quantity of beta particles associated with a first depth and at least a second measured quantity of beta particles associated with a second depth.

23. The system of claim 21 , wherein the calibration data is designed to correlate the quantity of detected beta particles to the indicated depth of a first region of a polycrystalline diamond volume.

24. The system of claim 23 , wherein the calibration data is designed to correlate the quantity of detected beta particles to the indicated depth of a catalyst-diminished region of the polycrystalline diamond volume.

25. The system of claim 23 , wherein the calibration data is designed to correlate the quantity of detected beta particles to the indicated depth of a cobalt-diminished region of the polycrystalline diamond volume.

Assignments (6)
SECURITY INTEREST Recorded Jul 18, 2025
From: US SYNTHETIC CORPORATION
To: KEYBANK NATIONAL ASSOCIATION
Reel/Frame 074973/0089 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 17, 2025
From: JPMORGAN CHASE BANK, N.A.
To: CHAMPIONX LLC; APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP; HARBISON-FISCHER, INC.; NORRIS RODS, INC.,; NORRIS RODS, INC.,; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; US SYNTHETIC CORPORATION
Reel/Frame 072004/0019 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2022
From: BANK OF AMERICA, N.A.
To: ACE DOWNHOLE, LLC; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; APERGY BMCS ACQUISITION CORP.; NORRISEAL-WELLMARK, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
Reel/Frame 060305/0001 →
SECURITY INTEREST Recorded Jun 5, 2020
From: ACE DOWNHOLE, LLC; APERGY BMCS ACQUISITION CORP.; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 053790/0001 →
SECURITY AGREEMENT Recorded May 9, 2018
From: APERGY (DELAWARE) FORMATION, INC.; APERGY BMCS ACQUISITION CORP.; APERGY ENERGY AUTOMATION, LLC; HARBISON-FISCHER, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 046117/0015 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 8, 2006
From: VAIL, MICHAEL A.
To: US SYNTHETIC CORPORATION
Reel/Frame 017665/0271 →