IP Library Granted Patent US 7,687,648
Granted Patent B2
US 7,687,648 · App. 11/375,461 · Granted Mar 30, 2010

Biomass extracts with protein and nutritional value

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 7,687,648
App. No.
11/375,461
Granted
Mar 30, 2010
Kind
B2
Abstract

Biomass extracts with high protein and nutritional value and methods for making the same are disclosed. Such extracts may include cakes with low residual oil and high levels of desirable constituents and oils that require little to no downstream processing upon extraction from the biomass. Also includes methods of extracting desirable products from an oil bearing biomass.

Claims (41)

1. A method of producing an organic defatted cake and an oil, the method comprising:

a. dehulling a whole bean or whole grain feedstock to provide an oil bearing biomass from which the hulls have been removed:

b. feeding the oil bearing biomass to a continuous screw press extractor;

c. compressing the biomass in the screw press extractor to form a cake plug that is essentially impermeable to fluids;

d. relieving the pressure on the biomass in the screw press extractor;

e. feeding an organic solvent to the screw press extractor and into the biomass;

f. compressing the biomass in the screw press extractor to extract oil and solvent from the biomass to create the organic defatted cake having a residual oil content of less than 6%;

g. separating the extracted oil and solvent from the defatted biomass; and

h. recovering the extracted oil, the oil having an average of less than 50 parts per million phosphorous.

2. The method of claim 1 , wherein the temperature within the extractor is maintained below 260° F.

3. The method of claim 1 , wherein the temperature within the extractor is maintained below 220° F.

4. The method of claim 1 , wherein the extracted oil has less than 35 parts per million phosphorous.

5. The method of claim 1 , wherein the extracted oil has less than 20 parts per million phosphorous.

6. An organic defatted biomass product having less than 6% residual oil and a PDI of greater than 60%, the defatted biomass product being produced by a process comprising:

a. feeding a raw biomass comprised of dehulled whole beans or dehulled whole grain or of germ to a compression zone of a screw press extraction unit;

b. compressing the raw biomass in the extraction unit to form a cake plug that is essentially impermeable to fluids;

c. relieving the pressure on the cake plug in the screw press extraction unit to make it permeable to fluids;

d. injecting an organic solvent selected from the group consisting of non-toxic alcohols and gases into the extraction unit to form a mixture of solvent, oil and biomass; and

e. compressing the mixture in the extraction unit to form a second cake plug and to push solvent and oil from the biomass, the second cake plug from which solvent and oil has been pushed being the organic defatted biomass product having a residual oil content of less than 6% and a PDI of greater than 60%; and wherein

the organic defatted biomass product is hexane free.

7. The method of claim 1 , wherein the feedstock is soybean.

8. The method of claim 1 , further comprising the step of further processing the dehulled feedstock to provide a germ fraction as the oil bearing biomass.

9. A method of producing an organic defatted cake and an oil, the method comprising:

a. providing a continuous screw press extractor for compression of a biomass and extraction of oil and solvent from the biomass;

b. feeding a dehulled oil bearing biomass to the continuous screw press extractor;

c. compressing the biomass in the screw press extractor to form a cake plug that is essentially impermeable to fluids;

d. relieving the pressure on the biomass in the screw press extractor;

e. feeding an organic solvent to the screw press extractor and into the biomass;

f. compressing the biomass in the screw press extractor to extract oil and solvent from the biomass to create the organic defatted cake wherein the organic defatted cake has a residual oil content of less than 6%, a PDI of greater than 60%;

g. separating the extracted oil and solvent from the defatted biomass; and

h. recovering the extracted oil, the oil having an average of less than 100 parts per million phosphorous.

10. A method of producing an organic defatted cake and oil, the method comprising:

a. feeding a raw dehulled biomass to a compression zone of a screw press extraction unit;

b. compressing the raw dehulled biomass in the screw press extraction unit to form a cake plug that is essentially impermeable to fluids;

c. relieving the pressure on the cake plug in the screw press extraction unit to make the cake plug permeable to fluids;

d. injecting organic solvent into the screw press extraction unit at a point where the pressure on the cake plug has been relieved to create a mixture of solvent and biomass;

e. compressing the mixture in the screw press extraction unit to extract the solvent and the oil from the biomass to form the organic defatted cake, the organic defatted cake having a residual oil content of less than 6% and a PDI of greater than 60%;

f. separating the extracted oil and solvent from the defatted cake; and

g. recovering the extracted oil, the oil having an average of less than 100 parts per million phosphorous.

11. The method of any one of claims 1 , 9 and 10 wherein the organic solvent is a gas or a non-toxic alcohol.

12. The method of any one of claims 1 , 9 and 10 wherein the organic solvent is carbon dioxide.

Assignments (17)
RELEASE OF SECOND LIEN PATENT SECURITY AGREEMENT Recorded Sep 28, 2023
From: JEFFERIES FINANCE LLC, AS COLLATERAL AGENT
To: CROWN IRON WORKS COMPANY; CPM WOLVERINE PROCTOR, LLC; CPM ACQUISITION CORP.
Reel/Frame 065081/0848 →
RELEASE OF FIRST LIEN PATENT SECURITY AGREEMENT Recorded Sep 28, 2023
From: JEFFERIES FINANCE LLC, AS COLLATERAL AGENT
To: CROWN IRON WORKS COMPANY; CPM WOLVERINE PROCTOR, LLC; CPM ACQUISITION CORP.
Reel/Frame 065081/0860 →
SECURITY INTEREST Recorded Dec 4, 2018
From: CROWN IRON WORKS COMPANY; CPM ACQUISITION CORP.; CPM WOLVERINE PROCTOR, LLC
To: JEFFERIES FINANCE LLC, AS COLLATERAL AGENT
Reel/Frame 047671/0986 →
SECURITY INTEREST Recorded Dec 4, 2018
From: CROWN IRON WORKS COMPANY; CPM ACQUISITION CORP.; CPM WOLVERINE PROCTOR, LLC
To: JEFFERIES FINANCE LLC, AS COLLATERAL AGENT
Reel/Frame 047671/0974 →
TERMINATION AND RELEASE OF FIRST LIEN SECURITY INTEREST IN PATENTS RECORDED AT REEL 043598, FRAME 0448 Recorded Nov 15, 2018
From: BANK OF MONTREAL, AS COLLATERAL AGENT
To: CROWN IRON WORKS COMPANY; CPM ACQUISITION CORP.
Reel/Frame 047579/0742 →
TERMINATION AND RELEASE OF SECOND LIEN SECURITY INTEREST IN PATENTS, RECORDED AT REEL 043533, FRAME 0369 Recorded Nov 15, 2018
From: BANK OF MONTREAL, AS COLLATERAL AGENT
To: CROWN IRON WORKS COMPANY; CPM ACQUISITION CORP.
Reel/Frame 047580/0169 →
ASSIGNMENT OF SECOND LIEN PATENT SECURITY AGREEMENT RECORDED AT REEL/FRAME 035397/0972 AND 035398/0015 Recorded Aug 11, 2017
From: COÖPERATIEVE RABOBANK U.A., NEW YORK BRANCH (F/K/A COÖPERATIEVE CENTRALE RAIFFEISEN-BOERENLEENBANK B.A., "RABOBANK NEDERLAND", NEW YORK BRANCH), AS THE ORIGINAL COLLATERAL AGENT
To: BANK OF MONTREAL, AS THE SUCCESSOR COLLATERAL AGENT
Reel/Frame 043533/0369 →
ASSIGNMENT OF FIRST LIEN PATENT SECURITY AGREEMENT RECORDED AT REEL/FRAME 035397/0888 AND 035397/0924 Recorded Aug 11, 2017
From: COÖPERATIEVE RABOBANK U.A., NEW YORK BRANCH (F/K/A COÖPERATIEVE CENTRALE RAIFFEISEN-BOERENLEENBANK B.A., "RABOBANK NEDERLAND", NEW YORK BRANCH), AS THE ORIGINAL COLLATERAL AGENT
To: BANK OF MONTREAL, AS THE SUCCESSOR COLLATERAL AGENT
Reel/Frame 043598/0448 →
SECURITY INTEREST Recorded Apr 13, 2015
From: CROWN IRON WORKS COMPANY
To: COOPERATIEVE CENTRALE RAIFFEISEN-BOERENLEENBANK B.A., "RABOBANK NEDERLAND", NEW YORK BRANCH
Reel/Frame 035398/0015 →
SECURITY INTEREST Recorded Apr 13, 2015
From: CROWN IRON WORKS COMPANY
To: COOPERATIEVE CENTRALE RAIFFEISEN-BOERENLEENBANK B.A., "RABOBANK NEDERLAND", NEW YORK BRANCH
Reel/Frame 035397/0924 →
RELEASE OF SECURITY INTEREST Recorded Apr 10, 2015
From: JEFFERIES FINANCE LLC
To: CROWN IRON WORKS COMPANY
Reel/Frame 035381/0001 →
RELEASE OF SECURITY INTEREST Recorded Apr 10, 2015
From: JEFFERIES FINANCE LLC
To: CROWN IRON WORKS COMPANY
Reel/Frame 035381/0148 →
RELEASE OF SECURITY INTEREST IN PATENTS AT REEL/FRAME NO. 023556/0913 Recorded Aug 31, 2012
From: BMO HARRIS BANK N.A. (FORMERLY KNOWN AS HARRIS N.A.)
To: CROWN IRON WORKS COMPANY
Reel/Frame 028885/0622 →
FIRST LIEN PATENT SECURITY AGREEMENT Recorded Aug 31, 2012
From: CROWN IRON WORKS COMPANY
To: JEFFERIES FINANCE LLC, AS COLLATERAL AGENT
Reel/Frame 028886/0600 →
SECOND LIEN PATENT SECURITY AGREEMENT Recorded Aug 31, 2012
From: CROWN IRON WORKS COMPANY
To: JEFFERIES FINANCE LLC, AS COLLATERAL AGENT
Reel/Frame 028886/0910 →
SECURITY AGREEMENT Recorded Nov 24, 2009
From: CPM HOLDINGS, INC.; CPM ACQUISITION CORP.; CROWN ACQUISITION CORP.; CPM WOLVERINE PROCTOR, LLC; CROWN IRON WORKS COMPANY; CROWN BIOFUELS, LLC; CPM SA LLC
To: HARRIS N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 023556/0913 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 2, 2006
From: SMALLRIDGE, LON E.; TEETER JR., FLOYD C.
To: CROWN IRON WORKS COMPANY
Reel/Frame 017938/0420 →