IP Library Granted Patent US 7,601,294
Granted Patent B2
US 7,601,294 · App. 11/415,840 · Granted Oct 13, 2009

High volume production of nanostructured materials

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 7,601,294
App. No.
11/415,840
Granted
Oct 13, 2009
Kind
B2
Abstract

A system and method for high volume production of nanoparticles, nanotubes, and items incorporating nanoparticles and nanotubes. Microwave, radio frequency, or infrared energy vaporizes a metal catalyst which, as it condenses, is contacted by carbon or other elements such as silicon, germanium, or boron to form agglomerates. The agglomerates may be annealed to accelerate the production of nanotubes. Magnetic or electric fields may be used to align the nanotubes during their production. The nanotubes may be separated from the production byproducts in aligned or non-aligned configurations. The agglomerates may be formed directly into tools, optionally in compositions that incorporate other materials such as abrasives, binders, carbon-carbon composites, and cermets.

Claims (18)

1. An apparatus for manufacturing nanostructure material, the apparatus comprising:

a catalyst feeder for introducing metal catalyst feed material into the apparatus;

a nano-element feeder for introducing nano-element feed material into the apparatus;

a vaporizer having a heat source selected from the group consisting of (a) a microwave plasma generator and (b) a hollow cathode glow discharge system, the vaporizer (i) to form metal catalyst vapor from the metal catalyst feed material and (ii) to establish atomic nano-element from the nano-element feed material;

a condenser comprising a condensation region for condensing the metal catalyst vapor into metal catalyst particles and for consolidating the atomic nano-element into nano-element nano-particle clusters and comprising an aggregation region for aggregating the metal catalyst particles and the nano-element nano-particle clusters as metal nano-element agglomerates.

2. The apparatus of claim 1 wherein the catalyst feeder and the nano-element feeder are combined as one apparatus for feeding a mixture of metal catalyst feed material and nano-element feed material into the apparatus.

3. An apparatus for manufacturing nanostructure material, the

apparatus comprising:

a fluid feed stream;

a catalyst feeder for introducing metal catalyst feed material into the fluid feed stream;

a nano-element feeder for introducing nano-element feed material into the fluid feed stream;

a vaporizer to (a) form metal catalyst vapor from the metal catalyst feed material and (b) establish atomic nano-element from the nano-element feed material;

a condenser comprising a condensation region for condensing the metal catalyst vapor into metal catalyst particles and comprising an aggregation region for consolidating the atomic nano-element into nano-element nano-particle clusters and for aggregating the metal catalyst particles and nano-element nano-particle clusters as metal nano-element agglomerates.

4. The apparatus of claim 3 wherein the metal catalyst feeder introduces the metal catalyst feed material into the fluid feed stream upstream from where the nano-element feeder introduces the nano-element feed material into the apparatus.

5. The apparatus of claim 4 in which the vaporizer comprises a microwave plasma generator.

6. The apparatus of claim 3 in which the vaporizer comprises a microwave plasma generator.

7. The apparatus of claim 3 in which the vaporizer comprises a hollow cathode glow discharge system.

8. The apparatus of claim 3 in which the metal catalyst feeder and the nano-element feeder are combined as one apparatus for feeding a mixture of metal catalyst feed material and nano-element feed material into the fluid feed stream.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 17, 2014
From: BABCOCK & WILCOX TECHNICAL SERVICES Y-12, LLC
To: CONSOLIDATED NUCLEAR SECURITY, LLC
Reel/Frame 033756/0649 →
CONFIRMATORY LICENSE Recorded Feb 8, 2011
From: UT-BATTELLE, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 025757/0611 →
CONFIRMATORY LICENSE Recorded Jun 5, 2007
From: BWXT Y-12, LLC
To: ENERGY, U.S. DEPARTMENT OF
Reel/Frame 019380/0831 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 2, 2006
From: RIPLEY, EDWARD B.; MORRELL, JONATHAN S.; SEALS, ROLAND D.
To: BWXT Y-12, L.L.C.
Reel/Frame 017862/0447 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 2, 2006
From: LUDTKA, GERARD M.
To: UT-BATTELLE, L.L.C.
Reel/Frame 017865/0648 →