IP Library Granted Patent US 7,348,062
Granted Patent B2
US 7,348,062 · App. 11/423,435 · Granted Mar 25, 2008

Interlayers comprising modified fumed silica

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Quick Facts
Patent No.
US 7,348,062
App. No.
11/423,435
Granted
Mar 25, 2008
Kind
B2
Abstract

The present invention includes polymer interlayers that are used in multiple layer glazing panels. Interlayers of the present invention comprise a thermoplastic polymer, a plasticizer, and a fumed silica that has been modified to impart hydrophobic character. Interlayers incorporating such components have improved tensile modulus, moisture resistance, creep performance, anticorrosion effect, glass adhesion, and are well suited to a variety of applications, including, but not limited to, acoustic applications.

Claims (31)

1. An interlayer for use in a multiple layer glazing, comprising:

a thermoplastic polymer; and,

fumed silica, wherein said fumed silica is alkylated and wherein said interlayer comprises more than one polymer sheet.

2. The interlayer of claim 1 , wherein said fumed silica has a carbon content of at least 0.5 weight percent.

3. The interlayer of claim 1 , wherein said fumed silica is methylated.

4. The interlayer of claim 1 , wherein said fumed silica has an average aggregate length of 0.15 to 0.35 microns.

5. The interlayer of claim 1 , wherein said fumed silica has an average aggregate length of 0.2 to 0.3 microns.

6. The interlayer of claim 1 , wherein said interlayer comprises a polymer sheet having 10 to 70 parts per hundred resin of said plasticizer and 0.05 to 15 parts per hundred resin of said fumed silica.

7. The interlayer of claim 1 , wherein said interlayer comprises a polymer sheet having 20 to 60 parts per hundred resin of said plasticizer and 0.1 to 10 parts per hundred resin of said fumed silica.

8. The interlayer of claim 1 , wherein said thermoplastic polymer comprises a polymer selected from the group consisting of poly(vinyl butyral), poly(vinyl chloride), poly(ethylene-co-vinyl acetate), poly(ethylene-co-ethyl acrylate), ionomers of partially neutralized ethylene/(meth)acrylic acid copolymer, polyethylene, polyethylene copolymers, polyurethane, and poly(cyclohexanedimethylene terephthalate-co-ethylene terephthalate) copolyester.

9. An interlayer for use in a multiple layer glazing, comprising:

a polymer sheet comprising:

poly(vinyl butyral);

plasticizer; and,

fumed silica, wherein said fumed silica is alkylated, wherein said interlayer comprises more than one polymer sheet, and wherein said interlayer comprises a polymer sheet having a glass transition temperature of less than 40° C.

10. The interlayer of claim 9 , wherein said fumed silica has a carbon content of at least 0.5 weight percent.

11. The interlayer of claim 9 , wherein said fumed silica is methylated.

12. The interlayer of claim 9 , wherein said fumed silica has an average aggregate length of 0.15 to 0.35 microns.

13. The interlayer of claim 9 , wherein said fumed silica has an average aggregate length of 0.2 to 0.3 microns.

14. The interlayer of claim 9 , wherein said interlayer comprises a polymer sheet having 10 to 70 parts per hundred resin of said plasticizer and 0.05 to 15 parts per hundred resin of said fumed silica.

15. The interlayer of claim 9 , wherein said interlayer comprises a polymer sheet having 20 to 60 parts per hundred resin of said plasticizer and 0.1 to 10 parts per hundred resin of said fumed silica.

16. A multiple layer glass panel comprising an interlayer, wherein said interlayer comprises:

a thermoplastic polymer; and,

fumed silica, wherein said fumed silica is alkylated and wherein said interlayer comprises more than one polymer sheet.

17. The panel of claim 16 , wherein said fumed silica has a carbon content of at least 0.5 weight percent.

18. The panel of claim 16 , wherein said fumed silica is methylated.

19. The panel of claim 16 , wherein said fumed silica has an average aggregate length of 0.15 to 0.35 microns.

20. The panel of claim 16 , wherein said fumed silica has an average aggregate length of 0.2 to 0.3 microns.

21. The panel of claim 16 , wherein said interlayer comprises a polymer sheet having 10 to 70 parts per hundred resin of plasticizer and 0.05 to 15 parts per hundred resin of said fumed silica.

22. The panel of claim 16 , wherein said interlayer comprises a polymer sheet having 20 to 60 parts per hundred resin of plasticizer and 0.1 to 10 parts per hundred resin of said fumed silica.

23. The panel of claim 16 , wherein said thermoplastic polymer comprises a polymer selected from the group consisting of poly(vinyl butyral), poly(vinyl chloride), poly(ethylene-co-vinyl acetate), poly(ethylene-co-ethyl acrylate), ionomers of partially neutralized ethylene/(meth)acrylic acid copolymer, polyethylene, polyethylene copolymers, polyurethane, and poly(cyclohexanedimethylene terephthalate-co-ethylene terephthalate) copolyester.

Assignments (11)
RELEASE OF SECURITY INTEREST Recorded Jul 17, 2012
From: DEUTSCHE BANK TRUST COMPANY AMERICAS, AS COLLATERAL AGENT
To: SOLUTIA INC.; CPFILMS INC.; FLEXSYS AMERICA L.P.
Reel/Frame 028563/0241 →
SECURITY AGREEMENT Recorded May 17, 2010
From: SOLUTIA INC.; CP FILMS INC.; FLEXSYS AMERICA L.P.
To: DEUTSCHE BANK TRUST COMPANY AMERICAS, AS COLLATERAL AGENT
Reel/Frame 024390/0281 →
RELEASE OF TERM LOAN SECURITY INTEREST IN PATENTS - REEL/FRAME 022610/0697 Recorded Mar 30, 2010
From: CITIBANK, N.A.
To: SOLUTIA INC.; CPFILMS INC.; FLEXSYS AMERICA L.P.
Reel/Frame 024151/0513 →
RELEASE OF ABL SECURITY INTEREST IN PATENTS - REEL/FRAME 022610/0495 Recorded Mar 30, 2010
From: CITIBANK, N.A.
To: SOLUTIA INC.; CPFILMS INC.; FLEXSYS AMERICA L.P.
Reel/Frame 024151/0469 →
RELEASE OF TERM LOAN SECURITY INTEREST IN PATENTS RECORDED AT REEL/FRAME 022043/0533 Recorded Mar 23, 2010
From: CITIBANK, N.A.
To: SOLUTIA INC.
Reel/Frame 024120/0461 →
RELEASE OF ABL SECURITY INTEREST IN PATENTS - REEL/FRAME 022043/0539 Recorded Mar 23, 2010
From: CITIBANK, N.A.
To: SOLUTIA INC.
Reel/Frame 024120/0499 →
ABL PATENT SECURITY AGREEMENT Recorded Apr 29, 2009
From: SOLUTIA INC.; CPFILMS INC.; FLEXSYS AMERICA L.P.
To: CITIBANK, N.A.
Reel/Frame 022610/0495 →
TERM LOAN PATENT SECURITY AGREEMENT Recorded Apr 29, 2009
From: SOLUTIA INC.; CPFILMS INC.; FLEXSYS AMERICA L.P.
To: CITIBANK, N.A.
Reel/Frame 022610/0697 →
TERM LOAN PATENT SECURITY AGREEMENT Recorded Dec 31, 2008
From: SOLUTIA INC.
To: CITIBANK, N.A.
Reel/Frame 022043/0533 →
ABL PATENT SECURITY AGREEMENT Recorded Dec 31, 2008
From: SOLUTIA INC.
To: CITIBANK, N.A.
Reel/Frame 022043/0539 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 10, 2006
From: YUAN, PING
To: SOLUTIA, INC.
Reel/Frame 017760/0270 →