IP Library Granted Patent US 7,524,363
Granted Patent B2
US 7,524,363 · App. 11/435,382 · Granted Apr 28, 2009

Gas chromatograph column assembly

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Quick Facts
Patent No.
US 7,524,363
App. No.
11/435,382
Granted
Apr 28, 2009
Kind
B2
Abstract

A separation column assembly for a gas chromatograph and the like is provided. The assembly is a self contained unit which allows very rapid heating and cooling of the column.

Claims (43)

1. A chromatograph column assembly comprising:

a first housing, the first housing defining a first chamber;

a column support, wherein the column support is ring-shaped about an axis and comprises a circumferential outer surface oriented about the axis and a plurality of axially oriented bridges, the bridges extending radially from the outer surface of the column support, and wherein the column support is positioned within the first chamber; and

column tubing wound around the column support, wherein the column tubing is in contact with the plurality of bridges and is separated from the outer surface of the column support,

the chromatograph column assembly further comprising an intake port and an exhaust port, wherein the intake port is in fluid communication with the exhaust port along a fluid communication path within the chromatograph column assembly and wherein the column tubing is between the intake port and the exhaust port along the fluid communication path,

the first housing comprising a column housing having an inner side wall, wherein the column tubing is between the inner side wall of the column housing and the outer surface of the column support and wherein the fluid communication path passes between the column tubing and the inner wall of the column housing and the column tubing and outer surface of the column support.

2. The chromatograph column assembly of claim 1 , further comprising a heating element, the heating element being in communication with an energy source, wherein the heating element is in direct contact with the column tubing.

3. The chromatograph column assembly of claim 2 , wherein the portions of the column tubing that are wound around the column support are only in contact with the heating element and the bridges.

4. The chromatograph column assembly of claim 1 , wherein the column support is made from low density rigid foam.

5. The chromatograph column assembly of claim 4 , wherein the low density rigid foam is light weight polymethacrylimide.

6. The chromatograph column assembly of claim 5 , wherein the first housing is made from light weight polymethacrylimide.

7. The chromatograph column assembly of claim 1 , wherein the first housing further comprises a bottom plate, the column housing having a top plate connected to the side wall of the column housing, wherein the bottom plate and the column housing define the first chamber.

8. The chromatograph column assembly of claim 7 , wherein the bottom plate, the column support and the top plate of column housing define an inner chamber, wherein the inner chamber is between the column tubing and the exhaust port along the fluid communication path.

9. The chromatograph column assembly of claim 8 , further comprising a plurality of exhaust vents formed between the bottom plate and the column support, wherein the fluid communication path travel through the exhaust vents into the inner chamber.

10. The chromatograph column assembly of claim 9 , the top plate of the column housing further comprising a central opening, wherein the fluid communication path exits from the inner chamber through the central opening.

11. The chromatograph column assembly of claim 10 , the top plate of the column housing further comprising a plurality of intake vents, wherein the column tubing is in fluid communication with the intake port through the plurality of intake vents.

12. The chromatograph column assembly of claim 11 , the first housing further comprising a port plate, wherein the column housing is between the port plate and the bottom plate and wherein the top plate of the column housing and the port plate define an intake chamber, the intake chamber being between the intake port and the intake vents along the fluid communication path.

13. The chromatograph column assembly of claim 12 , wherein the intake chamber and plurality of intake vents extend 360° around and separated from the central opening of the top plate of the column housing.

14. The chromatograph column assembly of claim 13 , the port plate comprising the intake port and the exhaust ports, wherein the fluid communication path begins at the intake port and travels into the intake chamber, through the intake vents, over the column tubing, through the exhaust vents, into the inner chamber, through the central opening in the top plate, and out of the exhaust port.

15. The chromatograph column assembly of claim 14 , the assembly further comprising an internal fan, wherein the fan draws air into the intake port and along the fluid communication path and out of the exhaust port.

16. The chromatograph column assembly of claim 1 , the upper surface of the column support having a first side edge and an axially opposite second side edge and the bridges having a first lateral end and a second lateral end, wherein the first lateral end of the bridges extend axially beyond the first side edge of the upper surface forming lateral posts.

17. The chromatograph column assembly of claim 16 , the bridges having a first radial post extending radially from the first lateral end and a second radial post extending radially from the second lateral end, wherein the first and second radial posts extend beyond the wound column tubing relative to the outer surface of the column support and wherein the column tubing is wound on the column support between the first and second radial posts.

18. A chromatograph column assembly comprising:

a first housing, the first housing defining a first chamber;

a column support, wherein the column support is ring-shaped about an axis and comprises a circumferential outer surface oriented about the axis and a plurality of axially oriented bridges, the bridges extending radially from the outer surface of the column support, and wherein the column support is positioned within the first chamber, the bridges having a first lateral end and a second lateral end and a first radial post extending radially from the first lateral end and a second radial post extending radially from the second lateral end; and

column tubing wound around the column support, wherein the column tubing is in contact with the plurality of bridges and is separated from the outer surface of the column support and wherein the first and second radial posts extend beyond the wound column tubing relative to the outer surface of the column support.

19. A portable multi-dimensional gas chromatograph, the gas chromatograph comprising:

a first pre-concentrator;

a first chromatograph column assembly comprising:

a first housing, the first housing defining a first chamber;

a column support, wherein the column support is ring-shaped about an axis and comprises a circumferential outer surface oriented about the axis and a plurality of axially oriented bridges, the bridges extending radially from the outer surface of the column support, and wherein the column support is positioned within the first chamber; and

column tubing wound around the column support, wherein the column tubing is in contact with the plurality of bridges and is separated from the outer surface of the column support,

the chromatograph column assembly further comprising an intake port and an exhaust port, wherein the intake port is in fluid communication with the exhaust port along a fluid communication path within the chromatograph column assembly and wherein the column tubing is between the intake port and the exhaust port along the fluid communication path,

the first housing comprising a column housing having an inner side wall, wherein the column tubing is between the inner side wall of the column housing and the outer surface of the column support and wherein the fluid communication path passes between the column tubing and the inner wall of the column housing and the column tubing and outer surface of the column support;

a first detector; and

a reference chemical.

20. The portable multi-dimensional gas chromatograph of claim 19 , further comprising:

a second pre-concentrator;

a second chromatograph column assembly comprising:

a first housing, the first housing defining a first chamber;

a column support, wherein the column support is ring-shaped about an axis and comprises a circumferential outer surface oriented about the axis and a plurality of axially oriented bridges, the bridges extending radially from the outer surface of the column support, and wherein the column support is positioned within the first chamber; and

column tubing wound around the column support, wherein the column tubing is in contact with the plurality of bridges and is separated from the outer surface of the column support; and

a second detector.

Assignments (11)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 6, 2023
From: VISIONARY PRODUCTS, INC.; VPI ENGINEERING, INC.; VPI MANUFACTURING, INC.; VPI LABORATORIES, INC.; D-TECT SYSTEMS, INC.
To: LUDLUM MEASUREMENTS, INC.
Reel/Frame 062604/0271 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 15, 2022
From: ALLIANT TECHSYSTEMS INC.
To: VPI ENGINEERING
Reel/Frame 061774/0203 →
RELEASE OF SECURITY INTEREST Recorded Oct 7, 2015
From: BANK OF AMERICA, N.A.
To: ALLIANT TECHSYSTEMS INC.
Reel/Frame 036807/0671 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 12, 2015
From: VPI ENGINEERING, INC.
To: D-TECT SYSTEMS, INC.
Reel/Frame 035621/0585 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 26, 2011
From: ALLIANT TECHSYSTEMS INC.
To: VPI ENGINEERING, INC.
Reel/Frame 026816/0018 →
PARTIAL INTELLECTUAL PROPERTY SECURITY RELEASE AGREEMENT Recorded May 31, 2011
From: BANK OF AMERICA, N.A.
To: ALLIANT TECHSYSTEMS INC.
Reel/Frame 026363/0854 →
PARTIAL INTELLECTUAL PROPERTY SECURITY RELEASE AGREEMENT Recorded May 31, 2011
From: BANK OF AMERICA, N.A.
To: ALLIANT TECHSYSTEMS INC.
Reel/Frame 026360/0973 →
SECURITY AGREEMENT Recorded Nov 4, 2010
From: ALLIANT TECHSYSTEMS INC.; AMMUNITION ACCESSORIES INC.; ATK COMMERCIAL AMMUNITION COMPANY INC.; ATK COMMERCIAL AMMUNITION HOLDINGS COMPANY; ATK LAUNCH SYSTEMS INC.; ATK SPACE SYSTEMS INC.; FEDERAL CARTRIDGE COMPANY; EAGLE INDUSTRIES UNLIMITED, INC.; EAGLE MAYAGUEZ, LLC; EAGLE NEW BEDFORD, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 025321/0291 →
SECURITY AGREEMENT Recorded Aug 24, 2007
From: AMMUNITION ACCESSORIES INC.; ATK COMMERCIAL AMMUNITION COMPANY INC.; ATK COMMERCIAL AMMUNITION HOLDINGS COMPANY INC.; ATK LAUNCH SYSTEMS INC.; ATK SPACE SYSTEMS INC.; FEDERAL CARTRIDGE COMPANY; MICRO CRAFT INC.; ALLIANT TECHSYSTEMS INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 019733/0757 →
OTHER:TO CORRECT THE SPELLING OF THE 1ST INVENTOR NAME Recorded Aug 21, 2006
From: BENTLEY, JAMES; BLANKEVOORT, JOHN; LEWIS, COLLIN; WUNNER, KEN
To: ALLIANT TECHSYSTEMS INC.
Reel/Frame 018149/0549 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 24, 2006
From: BENTLY, JAMES; BLANKEVOORT, JOHN; LEWIS, COLLIN; WUNNER, KEN
To: ALLIANT TECHSYSTEMS INC.
Reel/Frame 017999/0933 →