IP Library Granted Patent US 7,803,855
Granted Patent B2
US 7,803,855 · App. 11/437,018 · Granted Sep 28, 2010

Wood composites, methods of production, and methods of manufacture thereof

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Quick Facts
Patent No.
US 7,803,855
App. No.
11/437,018
Filed
May 18, 2006
Granted
Sep 28, 2010
Kind
B2
Art Unit
1796
USPC
524/14
Abstract

An adhesive binder comprising a phenol-formaldehyde resin, polyvinyl ester resin, and a protein is disclosed. The adhesive binder is useful for preparing wood composites.

Claims (32)

1. A wood composite comprising the cure product of an adhesive binder composition comprising a wood material and a thermosetting composition comprising,

a phenol-formaldehyde resin,

a polyvinyl ester resin, and

a protein;

provided, however, the wood composite does not contain any added urea-formaldehyde resin.

2. The wood composite of claim 1 wherein the protein is a vegetable protein.

3. The wood composite of claim 2 wherein the vegetable protein comprises a soy protein.

4. The wood composite of claim 3 wherein the soy protein is a soy flour.

5. The wood composite of claim 1 wherein the wood material is hardwood for plywood.

6. The wood composite of claim 1 wherein the wood material is selected from the group consisting of wood flakes, wood fibers, wood particles, wood wafers, wood strips, wood strands, wood veneer and combinations thereof.

7. The wood composite of claim 1 wherein the phenol-formaldehyde resin has a formaldehyde to phenol mole ratio of about 0.7:1 to about 4:1.

8. The wood composite of claim 1 wherein the ratio of the combined weights of the phenol-formaldehyde and polyvinyl ester resin solids to the protein is about 90:10 to about 50:50 in the thermosetting compound.

9. The wood composite of claim 1 wherein the polyvinyl ester resin is a polyvinyl acetate.

10. The wood composite of claim 1 wherein the adhesive binder further comprises additives selected from the group consisting of formaldehyde scavengers, plasticizers, thickeners, fillers, flame retardants, lubricants, softening agents, pigments, biocides, wax, acidic cure catalysts, and combinations thereof.

11. A process for making the wood composite of claim 1 comprising combining a wood material with an adhesive binder comprising a thermosetting composition comprising

a phenol-formaldehyde resin,

a polyvinyl ester resin, and

a protein;

consolidating the combined adhesive binder and wood material, and curing the combined adhesive binder and wood material.

12. The process of claim 11 wherein the protein is a vegetable protein.

13. The process of claim 12 wherein the vegetable protein comprises a soy protein.

14. The process of claim 13 wherein the soy protein is a soy flour.

15. The process of claim 11 wherein the wood material is selected from the group consisting of wood flakes, wood fibers, wood particles, wood wafers, wood strips, wood strands, wood veneer, and combinations thereof.

16. The process of claim 11 wherein the wood material is hardwood for plywood.

17. The process of claim 11 wherein the adhesive binder composition has a formaldehyde to phenol mole ratio of about 0.7:1 to about 4:1.

18. The process of claim 11 wherein the ratio of the combined weights of the phenol-formaldehyde and polyvinyl ester resin solids to the protein is about 90:10 to about 50:50 in the thermosetting compound.

19. The process of claim 11 wherein the adhesive binder further comprises additives selected from the group consisting of formaldehyde scavengers, plasticizers, thickeners, fillers, flame retardants, lubricants, softening agents, pigments, biocides, wax, acidic cure catalysts, and combinations thereof.

20. An adhesive binder, comprising a thermosetting composition comprising a

phenol-formaldehyde resin,

a polyvinyl ester resin, and

a protein;

provided, however, the adhesive binder contains no urea-formaldehyde resin.

Assignments (22)
SECURITY INTEREST Recorded Mar 18, 2022
From: HEXION INC.; HEXION INVESTMENTS INC.
To: GOLDMAN SACHS BANK USA, AS ADMINISTRATIVE AGENT
Reel/Frame 059436/0823 →
RELEASE OF SECURITY INTEREST IN PATENTS (ABL) RECORDED AT REEL/FRAME 049740/0770 Recorded Mar 18, 2022
From: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
To: HEXION INC.
Reel/Frame 059435/0490 →
SECURITY INTEREST Recorded Mar 18, 2022
From: HEXION INC.; HEXION INVESTMENTS INC.
To: GOLDMAN SACHS BANK USA, AS ADMINISTRATIVE AGENT
Reel/Frame 059436/0748 →
SECURITY INTEREST Recorded Mar 18, 2022
From: HEXION INC.; HEXION INVESTMENTS INC.
To: ROYAL BANK OF CANADA, AS ADMINISTRATIVE AGENT
Reel/Frame 059436/0842 →
RELEASE OF SECURITY INTEREST IN PATENTS (TERM LOAN) RECORDED AT REEL/FRAME 049741/0425 Recorded Mar 18, 2022
From: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
To: HEXION INC.
Reel/Frame 059435/0473 →
PATENT SECURITY INTEREST (TERM LOAN) Recorded Jul 12, 2019
From: HEXION INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 049741/0425 →
PATENT SECURITY INTEREST (ABL) Recorded Jul 12, 2019
From: HEXION INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 049740/0770 →
RELEASE OF SECURITY INTEREST IN PATENTS PREVIOUSLY RECORDED AT REEL/FRAME (030146/0970) Recorded Jul 9, 2019
From: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT AND COLLATERAL AGENT
To: HEXION INC. (FORMERLY KNOWN AS MOMENTIVE SPECIALTY CHEMICALS INC.)
Reel/Frame 049706/0264 →
PATENT SECURITY INTEREST ASSIGNMENT AGREEMENT Recorded Apr 3, 2019
From: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS THE PRIOR COLLATERAL AGENT
To: WILMINGTON SAVINGS FUND SOCIETY, FSB, AS THE CURRENT COLLATERAL AGENT
Reel/Frame 048788/0617 →
RELEASE OF SECURITY INTEREST Recorded Feb 23, 2017
From: WILMINGTON TRUST, NATIONAL ASSOCIATION (SUCCESSOR BY MERGER TO WILMINGTON TRUST FSB), AS COLLATERAL AGENT
To: HEXION INC. (FORMERLY KNOWN AS HEXION SPECIALTY CHEMICALS INC.); BORDEN CHEMICAL FOUNDRY, LLC; HEXION INVESTMENTS INC. (FORMERLY KNOWN AS BORDEN CHEMICAL INVESTMENTS, INC.); HEXION U.S. FINANCE CORP.; HSC CAPITAL CORPORATION; LAWTER INTERNATIONAL INC.; HEXION INTERNATIONAL INC. (FORMERLY KNOWN AS BORDEN CHEMICAL INTERNATIONAL INC.); OILFIELD TECHNOLOGY GROUP, INC.; HEXION CI HOLDING COMPANY (CHINA) LLC
Reel/Frame 041793/0001 →
SECURITY INTEREST Recorded Feb 13, 2017
From: HEXION INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 041693/0888 →
CHANGE OF NAME Recorded Feb 3, 2015
From: MOMENTIVE SPECIALTY CHEMICALS INC.
To: HEXION INC.
Reel/Frame 034882/0127 →
PATENT SECURITY AGREEMENT Recorded Apr 3, 2013
From: MOMENTIVE SPECIALTY CHEMICALS INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 030146/0946 →
PATENT SECURITY AGREEMENT Recorded Apr 3, 2013
From: MOMENTIVE SPECIALTY CHEMICALS INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 030146/0970 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENT RIGHTS Recorded Mar 28, 2013
From: JPMORGAN CHASE BANK, N.A.
To: MOMENTIVE SPECIALTY CHEMICALS INC. (F/K/A HEXION SPECIALTY CHEMICALS, INC.)
Reel/Frame 030111/0021 →
CHANGE OF NAME Recorded Apr 15, 2011
From: HEXION SPECIALTY CHEMICALS, INC.
To: MOMENTIVE SPECIALTY CHEMICALS INC.
Reel/Frame 026138/0817 →
CORRECTIVE ASSIGNMENT TO CORRECT THE APPLICATION NUMBER FROM 11/487,018 TO 11/437,018 PREVIOUSLY RECORDED ON REEL 018379 FRAME 0576. ASSIGNOR(S) HEREBY CONFIRMS THE CORRECT APPLICATION NUMBER IS 11/437,018. Recorded Jan 10, 2011
From: KINTZLEY, TOM G; HELKEY, JOHN; HOLTE, IVAN; JOHNSON, LEE ROY; MILLER, TODD R
To: HEXION SPECIALTY CHEMICALS, INC.
Reel/Frame 025608/0107 →
SECURITY AGREEMENT Recorded Feb 5, 2010
From: HEXION LLC; HEXION SPECIALTY CHEMICALS, INC.; BORDEN CHEMICAL FOUNDRY, LLC; BORDEN CHEMICAL INVESTMENTS, INC.; HEXION U.S. FINANCE CORP.; HSC CAPITAL CORPORATION; LAWTER INTERNATIONAL INC.; BORDEN CHEMICAL INTERNATIONAL, INC.; OILFIELD TECHNOLOGY GROUP, INC.; HEXION CI HOLDING COMPANY (CHINA) LLC
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 023905/0451 →
SECURITY INTEREST Recorded Jan 29, 2010
From: HEXION SPECIALTY CHEMICALS, INC.; BORDEN CHEMICAL FOUNDRY, LLC; BORDEN CHEMICAL INVESTMENTS, INC.; HEXION U.S. FINANCE CORP.; HSC CAPITAL CORPORATION; LAWTER INTERNATIONAL INC.; BORDEN CHEMICAL INTERNATIONAL, INC.; OILFIELD TECHNOLOGY GROUP, INC.; HEXION CI HOLDING COMPANY (CHINA) LLC
To: WILMINGTON TRUST FSB, AS COLLATERAL AGENT
Reel/Frame 023963/0038 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 26, 2007
From: KINTZLEY, TOM G.; HELKEY, JOHN; HOLTE, IVAN; JOHNSON, LEE ROY; MILLER, TODD R.
To: HEXION SPECIALTY CHEMICALS, INC.
Reel/Frame 018820/0730 →
SECURITY AGREEMENT Recorded Nov 21, 2006
From: HEXION SPECIALTY CHEMICALS, INC.
To: JPMORGAN CHASE BANK, N.A. AS ADMINISTRATIVE AGENT
Reel/Frame 018535/0556 →
SECURITY AGREEMENT Recorded Nov 21, 2006
From: HEXION SPECIALTY CHEMICALS, INC.
To: WILMINGTON TRUST COMPANY, AS COLLATERAL AGENT
Reel/Frame 018535/0701 →